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Analytical Instrumentation

This document outlines the course content for Analytical Instrumentation at Gujarat Technological University. The course covers various analytical techniques including analysis using mechanical, thermal, electrical, and radiant energy properties. Specific topics include viscosity and density measurement, pH and conductivity analysis, X-ray diffraction, gas chromatography, NMR, ESR, ultrasonics, and refractometers. The course also discusses online analyzers and their application guidelines. An industrial visit is recommended to complement the theoretical concepts taught in this subject.

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Mahavirsinh Gohil
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4K views2 pages

Analytical Instrumentation

This document outlines the course content for Analytical Instrumentation at Gujarat Technological University. The course covers various analytical techniques including analysis using mechanical, thermal, electrical, and radiant energy properties. Specific topics include viscosity and density measurement, pH and conductivity analysis, X-ray diffraction, gas chromatography, NMR, ESR, ultrasonics, and refractometers. The course also discusses online analyzers and their application guidelines. An industrial visit is recommended to complement the theoretical concepts taught in this subject.

Uploaded by

Mahavirsinh Gohil
Copyright
© Attribution Non-Commercial (BY-NC)
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd

GUJARAT TECHNOLOGICAL UNIVERSITY

Diploma in Instrumentation & Control Engineering


Semester: V

Subject Name: Analytical Instrumentation

Sr. No. Course Content

1. Analysis Using Different Properties :

1.1 Analysis Using Mechanical Properties


1.1.1 Viscosity
• Definitions
• Viscometers : Efflux Cup Type ,Say bolt, Ford cup, Zahn Cup, Automatic Efflux Cup,
Diff. Pressure Type, Magnetically Coupled Type.
1.1.2 Density and specific gravity
• Definitions
• Displacement type density meter,
• Buoyancy effect densitometer, Radio active densitometer.
• Vibrating U Tube type, Oscillating Coriolis Type, Liquid Densitometer,
• Straight Tube Pneumatic Densitometer,
• Thermal conductivity type Densitometer
1.2 Analysis Using Thermal Properties
• Thermal conductivity analysis
• Construction of hotwire thermal conductivity cell
1. 3 Analysis Using Electrical Properties :
1.3.1 pH analysers
• Introduction of pH
• Principles of pH measurement
• Electrodes of pH measurement
• Construction and Working of pH meters
1.3.2 Conductivity analyser
• Introduction and applications
• Methods of Measurement of Conductance : Null method and Direct reading method
• Conductivity cell
• Temperature compensation in Conductivity Measurement
1.4 Analysis Using Radiant Energy Property :
• X-Ray techniques of analysis by diffraction method.
• Geiger Muller (G.M.) counter and its measuring circuit.

2. O2 Analyzer
• Heat of reaction method, oxygen analyser.
• Paramagnetic O2 analyzer

3. Polarography
• Types & Theory of polarography

4. Flourescence Spectrography:
• Absorption spectrography, Scheme of X-Ray absorption spectrography.
5. Ionization Radiation:
• Properties of Cesium-134 and Cobalt-60

6. Spectrometer:
• Nuclear Magnetic Resonance Spectrometer (NMR)
• Principles and Constructional details of NMR
• Electron Spin Resonance Spectrometer (ESR)
• Principles and Constructional details of ESR

7. Gas Chromatographs:
• Chromatography
• Basic Parts of a Gas Chromatograph
• Carrier gas supply
• Sample Injection System
• Chromatographic Column
• Thermal compartment
• The detection system (Thermal Conductivity Detector, Flame Ionisation Detector)
• Recorders

8. Ultrasonics :
• Properties
• Applications of ultrasonic transducer
• Ultrasonic flaw detector
• Pulse eco method

9. Refractometers:
• Theory of operation
• Single pass & double pass method
• Critical angle type
• Applications

10. Application Guidelines for Analytical Systems:


Online Analysers
• Sample conditioning (Inlet/Exhaust)
• Housing of online analyzer
• Sample injection methods

Reference Books:
1. Handbook of Analytical Instruments by R S Khandpur (Tata McGraw-Hill Company Limited).
2. Process Instruments and Controls Handbook by Douglas M Considine (McGraw Hill Book
Company).
3. Analytical Instrumentation by B G Liptak.
4. Instrumental methods of Analysis by Willard.

Note:
An industrial visit is essential for this subject.

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