Telford Test House
( Water Quality Laboratory)
Azad Vihar Colony ,Miranpur-Pinvat
Kanpur Road –Lucknow-226401
Email:[email protected]
M-8934092044
1.0 WATER FOR DRINKING TEST (IS:10500)
S.NO Test Description Method Range
1 Colour IS:3025. pt-4-2002 2-70, Hazen Units
2 Odour IS:3025, pt-5 –2002 –
3 Taste IS:3025, pt-7-2002 –
4 Turbidity, NTU IS:3025, pt-10-2002 1-1000NTU
5 pH IS:3025, pt-11-2002 1-14
6 Total Hardness IS:3025, pt-21-2002 1-10000,mg/l
7 Iron APHA, 21st Ed.3111 0.01-50,mg/l
8 Chlorides IS:3025, pt-32-2003 1-10000,mg/l
9 Total Dissolved Solids (Residue on IS:3025, pt-16-2002 1-10000,mg/l
Evaporation)
10 Calcium IS:3025, pt-40-2003 1-10000mg/l
11 Magnesium .IS:3025-pt-46-2005 1-10000, mg/l
12 Manganese APHA 21st Ed.,3111 0.01-50,mg/l
13 Sulfates IS:3025, pt-24-2003 1-1000, mg/l
14 Nitrate IS:3025, pt-34-2003/ 1-100, mg/l
APHA, 21st Ed, 4500 NO3
15 Fluoride APHA, 21st Ed.,4500F 0.1-100,mg/l
16 Phenol IS:3025, pt-43,-2003 0.01-100, mg/l
APHA, 21st Ed. 5530
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17 Mercury APHA, 21st Ed.,3112 0.01-100, mg/l
18 Cadmium IS:3025, pt-41-2003/ 0.01-50, mg/l
APHA, 21st Ed.,3111
19 Selenium APHA, 21st Ed.,3114 0.05-50, mg/l
20 Arsenic IS:3025, pt-37-2003/ 0.05-50, mg/l
APHA, APHA, 21stEd. 3114
21 Cyanide IS:3025, pt-27-2003/ 0.01-100, mg/l
APHA, APHA, 21stEd.,4500CN
22 Lead IS:3025, pt-47-2003 / 0.01-50, mg/l
APHA, 21stEd.,3111
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2.0 PHYSICAL AND CHEMICAL PARAMETERS
Description I II III Analytical
(6) (25) (41) Instrument
Physical Temp, Temp, Temp, EC/TDS, pH Digital thermometer,
Parameters Colour, EC/TDS, pH pH meter, Conductivity
Odour, / TDS meter, Oven,
EC/TDS, Nepheloturbidit meter
pH
Chemical Carbonate, Similar to Level-II Lab Digital Burette, Ion
Parameters Bicarbonate, + Meter & Visible
(Cations) Chloride, Ammonia (N), Cynide, Spectrophotometer
Fluoride, Total Kjeldhal
Nitrate, Nitrite, Nitrogen
Sulphate,
Phosphate
Chemical Sodium, Similar to Level-II Lab Digital Burette, Flame
Parameters Calcium, Photometer & Visible
(Anions) Magnesium, Spectrophotometer,
Potassium, Water bath
Sillicate, Boron
Biological D.O. D.O., B.O.D & Similar to Level-II Lab DO Meter / Burette,
Parameters C.O.D In addition BOD Incubator & COD
(Oxygen Total Organic Carbon Digester & Total
Demand) carbon Analyser
Microbiological Total Colliform, Test tube with plastic
Total Plate cap, Bacteriological
Count, F. Incubator, Water Bath
Colliform, E.
Colliform
Trace/Toxic Iron In addition, Atomic Absorption
Metals Arsenic, Cadmium, Spectrophotometer
Mercury, Chromium, (AAS) / Inductively
Lead, Zinc, Nickel
coupled plasma mass
spectrometry (ICP-
MS)
Pesticides Chloro-hydrocarbons Gas chromatography–
(6nos) Mass Spectrometry
Alpha BHC, Beta (GC-MS)
BHC, Gama BHC
(Lindane), OP-DDT,
PP-DDT, Alpha
Endosulphan, Beta
Endosulpham, Aldrin,
Dieldrin, 2, 4-D,
Carbaryl
(Carbamate),
Malathian, Methyl
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Parathian, Anilphos
3.0 EQUIPMENT LIST
SL.No.
Name of the Instrument Quantity
1 Balance, Analytical (Electronic) 1
2 Electronic Pipette Controller 1
3 Magnetic Stirrer 1
4 Refrigerator 1
5 Dispensor 1
6 Ultra Water Purification System 1
7 pH Meter 1
8 Conductivity Meter 1
9 Turbidity Meter 1
10 Hot Air Oven 1
11 Digital Burette 1
12 Ion Meter 1
13 UV Visible Spectrophotometer 1
14
Flame Photometer microprocessor based with PC controlled 1
15 DO Meter 1
16 BOD Incubator PSD controller 1
17 Colorimeter 1
18 COD Digistor 1
19 Bacteriological incubator 1
20 Laminar Air Flow 1
21 Fume Hood in SS 1
22 Auto Clave 1
23 Water Bath PSD controller 1
24 Ion Chromatograph 1
25
Atomic Absorption Spectrophotometer (AAS) with GTA and
VGA 1
26
Total Organic Carbon Analyser (TOC) 1
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27
Inductively coupled plasma mass spectrometry (ICP-MS) 1
28
Gas chromatography–Mass Spectrometry (GC-MS) with Head
Space and Purge & Trap with Auto sampler 1
29 Air Conditioner 1
30 Water Geyser (Heater) 1
31 Software (Aqua Chem etc) 1
32 Reagent and chemical ( Total) 1
4.0 EQUIPMENT SPECIFICATIONS
(A)-pH Meter
Bench top pH meter with pH, mV meter for routine application microprocessor based,
Mains / Battery or Dual power supply (AC: 220V ±10%; 50Hz.)
pH combined electrode with milli Volt and temperature probe,
Temperature range 0 to 600C;
pH range between –2.000 to 16.000
Resolution: 0.001pH,
Accuracy : ± 0.001pH;
pH calibration up to 3 point Calibration with 2 custom and 7 standard buffers;
Beakers, stand and other standard accessories.
(B)-Conductivity Meter (EC)
Bench top conductivity meter with for routine application, microprocessor based.
Mains / Battery or Dual power supply (AC: 220V ±10%; 50Hz.)
Conductivity Cell : 1.00 & 0.5 cell constant
Electrode with temperature probe, temperature range 0 to 800C;
Conductivity range: 0 to 19.99, 199.9, 1999; 0 to19.99 micro Siemens /cm and 0 to199.9 milli
Siemens /cm,
Accuracy : ± 1% full scale,
Temperature compensation :0 to 80 0C .
Display: large LED
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99 data memory with real time clock and data
Stand and other standard accessories.
(C)-Dissolved OXYGEN KIT
Display : LCD
Range: D.O.: 0 to 20.0 mg/l and Temp: 0 to 500C
Accuracy: Dissolved Oxygen: ±0.4 mg/L, Oxygen in Air: ±0.7% O2 (for reference only),
Temperature: ±0.8 ºC/1.5 ºF
Power Off: Auto shut-off
Data Hold: Holds the current displayed Reading
Operating Temp: 0 to 50 ºC, 32 to 122 ºF
Sample Time: Approx. One (1) Second
Operating Humidity: Less Than 80% RH
Power Supply: 4-AAA Alkaline Batteries
(D)-DIGITAL BURETTE & PIPETTE
Burette
Recirculation valve for priming without loss of reagent
Dispensing range from 0.01 to 999.9 ml
Simple calibration program Discharge tube rotation 3600
Adjustable filling tube horizontal 142-220 mm vertical 10-200 mm
Telescopic filling tube for Automatic setting the length from 210 to 370 mm
Pipette
Circulation valve for priming without loss of reagent
Dispensing range from 0.01 to 10.00 ml
(E)-PORTABLE WATER ANALYSIS KIT
Compact in a Briefcase, operational both on AC mains/Rechargeable battery 6V/12V for
measurement of pH, EC, ORP, DO &Temperature, have LCD display & temp. compensation.
pH
Range: 0-14 pH
Resolution: 0.01pH
Accuracy: + 0.01 PH
EC
Range: 0.5 µS/cm to 100mS/cm (5 ranges)
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Resolution: 1 mV
Accuracy: + 1%
Oxidation Reduction Potential (ORP)
Range: 0-1999 mV
Resolution: 1 mV
Accuracy: + 1mV + 1 digit
DO
Range: 0.1 to 20 ppm
Resolution: 0.1 to 0.2 ppm
Accuracy: + 0.2 ppm + 1 digit or 1% full scale deflection
Temperature
Range: -5.0-99.9 0C
Resolution: 0.10C
Accuracy: + 1% 0C
Accessories: Electrodes for pH and EC measurements, cell holder, all standard buffers for 2
years, DO prove with membranes, temperature probe, one rechargeable compatible battery,
instruction manual.
(F)- FLAME PHOTOMETER
Flame photometer for routine application, microprocessor based with two filter for Sodium and
Potassium ; Flame Atomization
4 Line 20 Character Alphanumeric LCD Display
Analysis of 1 to max. 4 elements in single aspiration
Automatic filter selection
Sensitivity: 2.0 ppm for Na, 1.0 ppm for K, 1.0 ppm for Li and 30.0 ppm for Ca
Facility for Re-standardization, Sample Data storage in memory and recall and Print out
Data transfer to Computer through RS-232 (PC-Link) (Optional)
(G)-ION METER
Micro processor controlled multi-channel ion meter with LED display for menu, capable of
measuring pH, milli volt, ORP (Oxidation Reduction Potential), Cations and anions, built in
software
pH range: -2.000 to 19.999, Resolution: 0.001/0.01/0.1, Relative Accuracy: ± 0.005
Calibration point : 1-6 point Concentration range-0.000 to 19900.
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Milli volt range : 1600 mV, milli volt accuracy: ±0.2 mV or ± 0.05 % of reading whichever is
greater.
Working temperature: -50C to 105 0C and 5 to 85 % relative humidity, non-condensing.
Specific ion electrodes of Fluoride, Nitrate, Br etc. Fluoride electrode should have capability of
measuring in conc. Range of saturated to 0.02 ppm at temp range 0 to 800C.
(H)-PC based UV-VIS SPECTROPHOTOMETER
Double beam, fully automatic UV-VIS Spectrophotometer and should also have a facility to
connect with latest PC configuration for latest Windows XP base operation and compact with a
fast laser printer
LCD display, 220 V AC, Stray Light better than 0.02% T at 220 nm (NaI) and 340nm (NaNO2)
Better baseline flatness less than + 0.0006 Abs. over the entire range of 190 to 1100nm.
Scan speed: Variable options of 3000nm/min to 2nm/min so as to capture maximum data
points, hence to increase the resolution.
Noise level less than 0.00005 Abs. at 700nm.
Baseline stability less than 0.0003 Abs/Hour at 700nm
Multi-wavelength Photometric Measurement mode as standard
Abs / %T measurement possible at 6 wavelengths simultaneously in Photometric mode
Photometric, Multi-Wavelength Photometric, Spectrum, Quantitation, Kinetics and Multi-
Component measurement modes should be provided.
Expanded Photometric range up to -4 to +4 Abs / 0 to 400%, enables high concentration
measurement.
Photometric repeatability less than +/- 0.001 Abs at 1Abs.
Detector : Dual silicone photodiode
Monochromator having High end optics feature with Czerny-Turner mounting for high energy
though put and high sensitivity
Spectrophotometer should have facility for 5 USB ports for data communication with PC and
Printer compatibility.
Two sets of Quartz cell (optional)
USB Pen drive compatibility for data storage and transfer
Built-in- hardware validation for the parameters such as: Wavelength Accuracy, Wavelength
Repeatability, Spectral Bandwidth, Baseline Flatness, Baseline Stability, Noise Level, Photometric
Accuracy, Photometric repeatability & Stray Light
Semi-automatic testing: Interactive display for simplified testing of test items
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Automatic Testing :Automatic measurement and pass/fail evaluation and printing of results
Water Double Distillation Apparatus
Quartz double distillation apparatus with automatic cut off system
Main boiler
A built-in heater enclosed in quartz glass tube
Housing auto water level adjuster
Bottom outlet for cleaning waste discharge which is fitted with Teflon screw cap valve
A coil condenser fitted on top for condensing vapors
Whole unit is mounted on epoxy coated metal box stand and covered with acrylic sheet cover for
protection
Features:
Temperature resistant
Saving of electrical energy in every start
Convenient bottom drain for easy drainage as accumulated solids impair the efficiency,
cleaning is also possible
Distilled water in cold condition
Automatic start, cut-off & re-start in synchrony with water pressure/opening by
electronic circuit
(I)-TOTAL ORGANIC CARBON ANALYSER (TOC)
Compact PC controlled TOC analyzer for the determination of TOC, TIC, TC, NPOC and POC in
water samples.
The system should comply with DIN, ASTM and USEPA standards.
The system should have high temperature combustion unit of up to 950 Deg C to ensure complete
digestion of even stable compounds.
Sample feed should be through valve and septum free direct injection.
The injection volume should be variable from 50ul to 500ul.
The system should have high sensitive focused beam NDIR detector.
The measurement range should be from 50ppb to 30000 ppm without sample dilution.
The system should have facility to do multipoint calibration with single standard using different
injection volumes.
The system should have provision to select automatically the optimum calibration curve for
sample measurement.
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The instrument should have self check system to control all parameters for device safety as well to
ensure quality of results. The quoted software should be FDA 21 CFR PART 11 compliance. The
system should be upgradeable for solid sample analysis with either integrated double furnace or
with High temperature combustion module (1300 deg C temperature ).
The system should also have provision to upgrade for Total Nitrogen measurement using either
electrochemical detector or chemiluminiscence detector.
(J)-FOUR CHANNEL WET CHEMISTRY ANALYSER
(Four parameters to be analyzed simultaneously)
The analyser should be modular with the following modules; Auto sampler, module, module
holder, module with flow cell and filter, detector, interface and software.
The system should be up gradable into more simultaneous analysis possibility, and capable of
adding more parameters in future.
The sample is to have continuous flow with air bubble Segmentation and the detection is
colorimetric, Provision for other detectors like IR and UV and flame photometer should be
available.
Auto sampler:
Random access sampler; should have more than 100 sample cups; should have
built in rinsing pump, for day-to-day easy maintenance.
Sample cup capacity is to be up to 10ml
Optional built-in dilutor.
Separate cups for working standards.
Chemistry Unit :
Should have capacity to hold upto 5 chemistry modules
Should have two multi speed proportioning pumps, The two pumps should provide
32 tubings for reagent transportation to the analytical module.
Should have air pump. Air pump should have built-in compressor.
The multi speed pump should have speed adjustments for normal (analysis), fast
(washing) and slow (stand by position, to save reagents).
Chemistry modules:
Each parameter should have separate module and each module to have its own filter and
flow cell. All components of analysis like dialyser, reactor etc (wherever applicable)
should be provided within each module.
Parameter for analysis: Chloride, Total Hardness, Calcium, Phosphate and
Bicarbonate. Nitrate + Nitrite, Fluoride, Total Nitrogen,
The analysis module should have its own flow cell and filter.
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Flow cell to be supplied with black coating to avoid interference of external light in
the analysis.
Flow cell is to be part of the chemistry module and should not be inside the photometer.
Detector: Two Dual channel Digital detector with high degree of accuracy and wide dynamic
range; capable of measuring four parameters simultaneously.
The photometer detector head is to have an insert board and cable
Digital detector with high degree of accuracy and wide dynamic range.
Capable of measuring four parameters simultaneously.
Wavelength selection by insert of interference filters.
Wavelength range 340-1050 nm.
Accommodation for 2 flow cells of 5 upto 50 mm path length each
Software controlled automatic baseline and peak height settings.
Software controlled lamp switching on / off
32 bits high resolution absorption recording
Detecting range up to 6.5 AU
Signal / noise ratio <0.0003 AU
Software : The software is to be windows based and user friendly. Provision should be there for
raw data storage. Automatic back ground correction should be possible;
PC & Printer : Suitable branded latest PC & colored laser printer should be offered.
(K)-ATOMIC ABSORPTION SPECTROPHOTOMETER (AAS)
Computer operated double beam Atomic Absorption Spectrophotometer with high sensitivity,
capability to analyze Flame Atomization with Air-Acetylene and Nitrous Oxide Acetylene Flame
with Hydride Vapour Generator and future upgradeable to Graphite Furnace.
Wavelength range from 185 nm to 900 nm., Slit width 0.2 to 2.0 mm in steps.
High efficiency atomization achieved through new design Polypropylene nebulizer with Platinum-
Iridium orifice and Ceramic impact bead for high sensitivity. High-end automation with fully
motorized burner head up-down motion with automatic optimum height setting.
Deuterium and background correction modes (preferably Self-Reversal) should be available as
standard.
Standard measurement modes include Flame continuous.
Auto selection of Hollow Cathode lamps with motorized 8 lamp turret.
Fully computerized gas flow control system with automatic setting of optimum fuel and oxidant
flow rates.
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Hallow Cathode lamp for each single elements to ensure maximum sensitivity, Cathode Lamps-
Fe, Mn, Pb, Zn, Cu, Co, Cd, Cr, As, Ni, Hg, Se, Bi and Au.
Regulators- Nitrogen, Nitrous oxide and Air Acetylene.
Compressor- Oil Free.
VGA- Continuous flow base automatic vapour generation for hydride forming elements with
peristaltic pump
Incorporates all safety measures as standard including the unique leak check on power 'ON',
flame monitor, gas pressure monitor, inter-lock for wrong burner head use, Air - Acetylene / N2 O
- Acetylene automatic change- over with flow rate monitor using optical sensor and drain tank
level monitor to prevent flash-back.
Advanced 32-bit Windows 2000 based software for complete instruments control, data
acquisition and data processing.
(L)-ION CHROMATOGRAPH (IC)
Electronics Type Microprocessor controlled digital signal processing, autoranging
Cell Drive 8 kHz square wave
Linearity 1%
Resolution 0.00238 nS/cm
Digital Signal Range: 0-15,000 µS/cm,
Output Range
Analog Signal Range: 0-15,000 µS/cm
<0.2 nS at 23 µS/cm background
Noise, Wet
<0.1 nS at 1 µS/cm background
Filter Rise times 0 to 10 s, programmable
Sampling Rate 1 to 100 Hz, user settable or automatic
5 °C above DC upper zone temperature to 60 °C maximum. User settable, w
Cell Temperature
settable range.
Cell Temperature Stability <0.001 °C
Cell Temperature Compensation Default 1.7% per °C ; programmable from 0–3% per °C
Flow Cell Maximum Pressure 10 MPa (1500 psi)
Flow Cell Volume 0.7 µL (Analytical); 0.02 µL (capillary)
Cell Electrodes Passivated 316 stainless steel. Compatible with MSA
Cell Body Chemically inert polymeric material
Heat Exchanger Inert, tortuous-path for low axial dispersion
Software Chromatography Management Software, requires Microsoft Windows® 20
Automated Procedure Wizards Yes, standard feature
System Smart Startup and Shutdown Yes, standard feature
System Wellness and Predictive
Yes, standard feature
Performance
Application Templates Yes, standard feature
Multivendor Automation Support of 3rd Yes, fully controls over 300 different instruments from more than 30 manu
Party and MS.
Customizable System Control Panels Yes, standard feature
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Signal Channels Conductivity, Total Conductivity
Data Trending Yes, all detector numerical parameters
System Status Virtual Channels Yes, standard feature
Power Failure Protection Yes, standard feature
System Trigger Commands and Conditionals Yes, standard feature
Daily & Sample Audit Trail Yes, standard feature
System Calibration Storage Yes, factory, present, and previous. Completely user selectable
M-INDUCTIVELY COUPLED PLASMA MASS SPECTROMETER (ICP-MS)
Mass spectrometry unit :
(1) Spectrometry unit Quadru-pole mass spectrometer
Hyperbolic rod made of molybdenum (main rod)
Cylindrical rod made of molybdenum (pre-rod)
Power supply frequency:2.5MHz
Mass number range 2 to 250
Resolution Max. 2 M is possible.
Mass number stability ±0.1 a.m.u
(2) Detector Channel Thoron detector
Must be installed perpendicular to the quadrupole rod
(3) Counting method Analog/Pulse selection
Pulse measurement 24 bit counter
Max. Frequency 108cps
Analog measurement: Gain 2 step selection
Integration time can be set for each element
Plasma ion source
(1) Torch unit Spray chamber
Plasma mini-torch
Coaxial type nebulizer
Peristaltic pump
Equipped with adjustment function of X, Y, Z, three axes torch position
CPU control for direction of torch axis
(2) RF power matching unit : Equipped with automatic matching circuit
(3) Gas controller 3-flowline method for plasma
Coolant gas 7.9 L/min
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Plasma gas 1.5 L/min
Carrier gas 0.2 to 1.4 L/min
CPU controls carrier gas
RF power supply :
(1) Oscillator Quartz oscillator
(2) Frequency 27.120 MHz ±0.05%
(3) RF output 0.2, 0.8, 1.0, 1.2 kW
(4) Output stability Within ±0.3%
(5) RF circuit element Power MOS FET
(6) Control system Controlled by using CPU
(7) Lighting unit Full automatic ignition start
(8) PA unit cooling Water-cooling
(9) Equipped with safety function
Vacuum container and exhaust unit
(1) Vacuum container 3-stage differential exhaust system
(2) Exhaust system 1st stage Rotary pump
2nd stage Air-cooling type turbo molecular pump
3rd stage Air-cooling type turbo molecular pump
Gas Chromatograph with Mass Spectrometer (GC-MS)
High performance Designed towards improved productivity, enhanced efficiency, and ease of
operation
Column oven temp up to 450 0C
20-step Column oven temperature programming
Maximum column oven heating rate of 250 0C/min
High pressure sample injection possible with standard Split / Splitless injection port
Capability of installing 3 injection ports and 4 detectors
Instrument should be quoted with Dual packed column and one Capillary injector
Detector sampling frequency of 250 Hz (4 msec sampling time) helps accurate acquisition of
sharp and narrow peaks and also enables fast GC analysis
Ultra High Speed GC capability – reduces analysis time with better resolution suitable even for
narrow bore column of I.D. 0.1mm
Third Generation Advanced Flow Controller (AFC)
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Carrier Head Pressure Control up to 970 kPa
Carrier Flow Control up to 1200 ml/min
Split Ratio Setting up to 9999.9 : 1
7 Step Pressure / Flow programming
All auxiliary gases like Air, H2, Make-up gas for FID, septum purge and digitally controlled
through third generation Advanced Pressure Controller (APC) and Gas Cylinders.
Patented Constant Linear Velocity mode ensures maximum separation efficiency for any carrier
gas. Hence even N2 gas can be used very efficiently for capillary column analysis
Large LCD window (240 x 320 dots) Graphic User Interface makes operation very easy and
enables display of all GC set parameters, monitored values and also displays the acquired
chromatogram
Built in GC System Check and Self Diagnostics function
Mass Spectometer: Quadruple (gold coated)/Ion trap Mass Spectrometer.
Cooling Unit: Thermostatically recirulating.
Dynode Detector: High energy dynode detector (preferably +/- 15 KV) for +/- Ion mass
analysis
Unit Mass Resolution Ionisation: Unit mass resolution over entire range of 10-900 AMU.
External ionization source having option for positive and negative ions with automatic switching
from El to Cl.
Turbo Pump: Highly efficient pump (approx 200L/s- maintenance free, all accessories for
safety controls and indicators.
Library for Pesticides: Latest library with spectra and 200 pesticides
Equipment Tuning: Both Auto and Manual.
Gas Control: Separate control for Helium gas flow.
Software Features:
New 32/64-Bit, Windows NT Compatible GC Solutions software, Digital data acquisition
from GC
Full Qualitative and Quantitative processing capabilities, Multi Tasking, Multi Function
capability for easy operation, User Management Functions , Full GLP / GMP support
Multi level security with passwords, Audit Trail, System Check, Validation Assistant,
System Suitability functions built-in QA / QC Functions with Pass / Fail judgements, All-
in-one file configuration for easy method transfer, Customized Report generation,
Networking capability
FID :
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Temperature Range : up to 400 0C
Minimum detected quantity : 3 pg/S (dodecane)
Dynamic Range : 10 7
ECD :
Temperature Range : up to 400 0C
Minimum detected quantity : 0.1 pg/S (- BHC)
Dynamic Range : 10 4
FPD :
Temperature Range : up to 350 0C
Minimum detected quantity :
P : 0.5 pgP/S (Tributyl Phosphate)
S :8 pgS/S (dodecane thiol)
Dynamic Range : P :10 4 , S : 10 3
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