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Shimazdu AA6800 Tech

The document discusses the AA-6880 Series of atomic absorption spectrophotometers. It describes the system configuration, major application fields, analysis sensitivities, and features such as enhanced flame analysis, furnace analysis, automatic optimization of gas flow rates, an optional autosampler to reduce workload, and micro sampling of small volume samples.

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Bùi An Vinh
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0% found this document useful (0 votes)
325 views20 pages

Shimazdu AA6800 Tech

The document discusses the AA-6880 Series of atomic absorption spectrophotometers. It describes the system configuration, major application fields, analysis sensitivities, and features such as enhanced flame analysis, furnace analysis, automatic optimization of gas flow rates, an optional autosampler to reduce workload, and micro sampling of small volume samples.

Uploaded by

Bùi An Vinh
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd

C122-E060

Atomic Absorption Spectrophotometers

AA- 6880 Series


System Configuration Can Evolve
with Your Needs
The AA-6880 Series can be upgraded by adding units to handle the analysis targets.

ASC MAC GFA

*1
*2

AA-6880F AA-6880F Manual Burner System (with ASC stand kit)

Major Fields of Application Analysis Sensitivities

AA-6880 Series supports a wide range of


analysis applications. Flame Furnace

Concentration limit of detection


Environment
(ppm) (ppb)
Seawater, river water, effluent,
sludge, air-borne dust
+ +H
/L %H % & 1 2 ) 1H
Metals, Semiconductors, Ceramics
Metals, minerals, glass, 1D 0J $O 6L 3 6 &O $U
ceramics, IC chips
. &D 6F 7L 9 &U 0Q )H &R 1L &X =Q *D *H $V 6H %U .U
Petroleum, Chemicals, Polymers 5E 6U < =U 1E 0R 7F 5X 5K 3G $J &G ,Q 6Q 6E 7H , ;H
Petroleum, oil, catalysts,
chemical products, biodiesel &V %D /D +I 7D : 5H 2V ,U 3W $X +J 7O 3E %L 3R $W 5Q
)U 5D $F
Medical, Biology, Pharmaceuticals &H 3U 1G 3P 6P (X *G 7E '\ +R (U 7P <E /X
Blood, animals, plants,
drugs, food products 7K 3D 8 1S 3X $P &P %N &I (V )P 0G 1R /U
* May differ according to coexisting substances in the sample.
AA - 6880 Series
Atomic Absorption Spectrophotometers

Boosting Analytical Productivity of AAS to a Higher Stage


Enhanced Flame Analysis

World-Class High-Sensitivity Furnace

Evolving System Configuration

Advanced Safety Technology

AA-6880F Dual Atomizer System

MAC ASC
Manual Atomizer Autosampler
Changing kit

GFA
Graphite Furnace Dual Atomizer System
Atomizer Manual switching between Flame and Furnace

*1 Requires ASC stand kit.


*2 Requires ASK-6880.

Flame Selection

Flame and Measurement Procedures

$LU&+ 12&+ +9* 098

AA-6880F Flame model


+ +H
/L %H % & 1 2 H
) 1H
1D 0J $O 6L 3 6 &O $UU
. &D 6F 7L 9 &U 0Q )H &R 1L &X =Q *D *H $V 6H %U .UU
5E 6U < =U 1E 0R 7F 5X 5K 3G $J &G ,Q 6Q 6E 7H , H
;H
Q
&V %D /D +I 7D : 5H 2V ,U 3W $X +J 7O 3E %L 3R $W 5Q
)U 5D $F
X
&H 3U 1G 3P 6P (X *G 7E '\ +R (U 7P <E /X
7K 3D 8 1S 3X $P &P %N &I (V )P 0G 1R /UU
AA-6880F Dual Atomizer System (with options attached)
Enhanced Flame Analysis

Monochromator

Detector

Chopper mirror Reference beam

D2 lamp

Sample beam

Beam splitter

Burner head (or graphite tube)

Hollow cathode lamp

Double-Beam Optics and Stable Hardware Achieve Superior Stability


The AA-6880 Series incorporates newly developed 3D double-beam optics.
The optical system has been designed to produce maximum performance for each measurement method through
optimal adjustment of the light beam and light beam digital filter, and by using optical components that restrict light
losses.

4
Advantages of the Double-Beam System
Long-term stability High sensitivity A
The graph shows the results of The graph shows the direct b
s

Absorbance
measurements on 2 ppm copper (Cu) measurement results for 0.1
conducted over at least one hour. ppm lead (Pb).
(The plot shows mean values for 11
repeated measurements.) Over the
course of more than 600
Measurement time
measurements, the instrument Conc(ppm)
Data Showing Long-Term Stability for 0.1 ppm to 0.4 ppm Calibration Curve for Lead (Pb)
achieved a relative standard Flame Cu Measurements
deviation within 1%.

Support for Developing Analytical Conditions


Automatic gas flow rate optimization
Automatic searching for optimal fuel gas flow rate (Japanese Patent 2099886). It is important
to determine the optimal gas flow rate for the flame when using an organic solvent or after
changing the burner height. The AA-6880F Series automatically optimizes the gas flow rate
by measuring the changes in absorbance between a blank and a standard sample. The
difference between the two is displayed on the screen. The gas flow rate achieving the
highest sensitivity is detected and this value is automatically set as the gas flow rate value.

Optional Autosampler Reduces Analysis Workload


Low carryover
Great care must be taken to avoid carryover during flame analysis. The new ASC-6880
autosampler rinses the nozzle at the rinsing port on the overflow mechanism after each Discharge
sample measurement is complete. This ensures 10-4 max. carryover during measurements
of multiple samples. The graph shows the results of consecutive analyses of 10 ppm, 20
ppm, and 50 ppm sodium (Na) standard solutions in the EMISSION mode. No carryover
could be detected when measuring the 10 ppm standard sample immediately after
measuring the 50 ppm Na standard sample. Conventional method Overflow method Data showing low carryover

Trace Sample Analysis Using Micro Sampling


Micro sampling
At least 1 mL (1000 µL) volume of a liquid sample is required for the continuous intake of
sample during normal flame analysis. With micro sampling, however, approximately 50 to 90 Sampling port Sampling port
µL of sample is injected in one shot into the flame and quantitation is based on the height
and area of the peak signal obtained. This method offers the advantages listed below.
Solenoid Solenoid
Advantages
Permits analysis of small sample volumes
valve valve
(closed) (opened)

Multi-element analysis of small sample volumes 1. Sample injected into 2. Solenoid valve opens to inject sample

No blockage of burner slot with samples having a high salt concentration micro sampling port. in one shot into the flame.

Synchronized with the autosampler for auto-dilution measurements


* Synchronization with the autosampler requires the optional micro sampling kit.

Example of micro sampling analysis


Examples of the measured waveforms (overlaid) and calibration curve for micro
sampling analysis are shown to the right.
A 2-ppm Cu standard solution was prepared by auto-dilution using the autosampler.
The autosampler can also be used to conduct dilution measurements of the sample.
(Injection volume: 90 µL)

5
World-Class High-Sensitivity Furnace

Achieves World-Class Lower Limits of Detection


Advances in optics and a new graphite furnace design achieve improved Enhanced Sensitivity due to Graphite Furnace
lower limits of detection for furnace analysis (comparison with previous Previous New
Shimadzu models). Pb 0.08ppb 0 . 0 5 ppb
This superb analysis performance is possible in all fields. Mn 0 . 0 2 p p b 0 . 0 1 ppb

6
High-Performance Autosampler
Mix and inject up to four sample types (diluted solution, standard solution,
sample, matrix modifier, etc.). (Unmixed samples can also be injected.)
Select a fluororesin tube or pipette tip as the injection nozzle.
Automatic dilution and re-analysis if the calibration curve concentration is exceeded.

Example of Automatic Dilution and Re-Analysis


Analysis of cadmium (Cd): The maximum concentration of the calibration curve has been set to 1ppb. At 1.8ppb, the sample of [003] has exceeded the
maximum concentration. As a result, it has been automatically diluted by four times and re-measured.

High-Sensitivity Application Data (Analysis of Selenium (Se))


Independent control of the gas flow through the graphite tube during
atomization achieves extremely high-sensitivity measurements.
(Japanese Patent 2067563)

Measurement Example Showing High Sensitivity


Analysis of 0 to 5 ppb selenium (Se): Sensitivity is adequate for 1 ppb measurements.
(20 µL injected volume, Pd modifier, pyro-coated graphite tube)

Digital temperature control and electronic gas flow control enhance stability
Combination of a high-sensitivity optical sensor and unique digital temperature control
technology achieves highly accurate temperature control in all temperature regions from
drying to atomization. An electronic flow controller can precisely control the inner gas
flow rate in 0.01 L/min units. These control techniques significantly enhance both the
sensitivity and the data stability.

Measurement Example Showing High Stability


Analysis of 0.5 ppb lead (Pb): Approx. 5% relative standard deviation after five
repeated measurements is adequate for quantitative analysis.

7
$$  Quickly and easily switch between flame and
Employs a quick, tool-less switching mechanism, making it as easy and effortless as shown in the photo.

From flame...

Remove the burner head.

Attach the burner head.

...to flame

Switch smoothly between Flame and Furnace

All that is involved in switching from flame to furnace is to remove the burner head and put in place the furnace
section. No tools are needed, making this a quick, easy process.
Furthermore, one autosampler can be used for both flame and furnace, which negates the need to prepare
the autosampler for each analysis method.

Selecting the Graphite Tube

High-density graphite tube Pyro-coated graphite tube Platform tube


(P/N 206-50587-11) (P/N 206-50588-11) (P/N 206-50887-02)
Can be used for all elements. Especially Effective for elements that readily form Restricts chemical interference due to
effective for low-boiling point elements carbides (Ni, Fe, Cu, Ca, Ti, Si, V, Mo, etc.). coexisting substances. Effective for the
(Cd, Pb, Na, K, Zn, Mg, etc.). analysis of environmental samples and
biosamples, such as sea water and
industrial waste.

* Depending on the state of the sample, some other combinations may be appropriate.

8
furnace

... to furnace

Attach the furnace.

Remove the furnace.

From furnace...

Slim, Easy-to-Use Design

Smallest footprint for a full system Lamp house


The system with a dual atomizer fits into a 960 mm width Just slide the cover to the side for easy replacement of the
(including power supply for the graphite furnace atomizer). hollow cathode lamps through the large opening.

AA-6300
1080mm(W) × 545(D) ×460(H)

AA-6880F Dual Atomizer System


960mm(W) × 590(D) ×702(H)

* Dimensions do not include the ASC-6880. Height (H) does not include protrusions.

9
$$  Power Supply, for Unique
High-Performance Boosted Hollow
Cathode Lamp Included as Standard

Excellent Lamp Sockets Design


The AA-6880 lamp house has an 8 lamp turret with an automatic switching function, where the No. 7 and No. 8 lamp holders can be
used for both an ordinary hollow cathode lamp and a high-performance boosted hollow cathode lamp. The AA-6880 can
simultaneously light any two hollow cathode lamps.
For the high-performance boosted hollow cathode lamp, an auxiliary cathode electrode is added based on two ordinary hollow
cathode lamps. The atoms will be produced under the sputtering action in the hollow cathode due to discharging between the
hollow cathode and the anode. The low-voltage high current between the anode and the auxiliary cathode provides excitation
energy for the atoms, and such sputtering action and excitation action will be respectively controlled by two separate discharge
processes. This greatly improves the excitation efficiency of the atomic spectrum. The high-performance hollow cathode lamp
requires a dedicated power supply.

Unique Lamp Power Design


The AA-6880 main unit has a built-in high-performance boosted hollow cathode lamp power supply.
Two high-performance hollow cathode lamps can be simultaneously illuminated without any external power supply.
An auxiliary cathode current can be automatically scanned, which only requires optimizing the test conditions.

Main Features of High-Performance Boosted Hollow Cathode Lamps


(as Compared with Ordinary Lamps):
High emission intensity and good stability
High measurement sensitivity and low detection limit
Expanded calibration curve linear range
Reduced spectrum interference from adjacent lines, so a larger spectral bandwidth can be used to further improve
the energy. In general, the electrodes of the high-performance boosted hollow cathode lamp, made by
low-melting-point and volatile elements,such as As, Bi, Pb, Sb, Se, Zn, etc., show better application results..

Air - Ac et y l ene Ai r - Ac et y l en e G ra p h i te G ra p h i te
Fla m e Anal y s i s F l am e Anal y si s F u rn a ce A n a l y si s F u rn a ce A n a l y si s

Or di nar y Hol l ow Hi gh- Per f orma n ce H o l l o w O rd i n a ry H o l l o w H i g h - P e rfo rma n ce H o llow


Ele m ent
Ca t hode L am p Cat hode L amp C a th o d e L a mp C a th o d e L a mp
Det ec t i on L i m i t Det ec t i on L i mi t D e te cti o n L i mi t D e te cti o n L i mi t
(µg/ m L ) ( µg/ m L ) (pg) (pg)
Pb 0 .0279 0. 0149 0.68 (10 µL) 0.42 (10 µL)
Zn 0 .0019 0. 0010 0.055 (20 µL) 0.025 (20 µL)

Pb and Zn: Comparison Table for Typical Detection Limits of the High-Performance Boosted Hollow Cathode Lamp and the Ordinary
Hollow Cathode Lamp

10
Advanced Safety Technology
Comprehensive Safety Functions in Every System
Safety is an extremely important consideration for flame atomic absorption
spectrophotometers using acetylene gas.
The AA-6880 Series instruments incorporate a comprehensive range of safety
mechanisms, including gas leak detectors.

Safety Functions for Flame-Specification Instruments


Multimode automatic gas leak check
The fuel gas pipes inside the instrument gas controller are automatically checked for gas
leaks when the power is turned on and when the flame is extinguished. Should a gas leak be
detected, a warning buzzer sounds and a warning is displayed on the screen.

Automatic flame ignition and extinguishing


Flame ignition and extinguishing operations are extremely simple. The Air-C2H2 flame priority
ignition mechanism prevents flashback.

Automatic Air-N2O switching system with acetylene flow-rate monitor


After the ignition of an Air-C2H2 flame, the flame automatically switches to an N2O-C2H2
flame.
If the C2H2 flow rate does not increase due to solenoid valve trouble, for example, switching
to the support gas is disabled to prevent flashback.

Pressure monitor prevents flashback Automatic gas shut-off by flame monitor


Sudden power interruption detection and re-ignition safety measures Mechanism to prevent misuse of the burner
Drain tank level monitor

Safety Functions for Furnace-Specification Instruments


Cooling water flow rate monitor Argon gas pressure monitor Furnace cooling check
Overcurrent protection unit (double-checked by circuit protector and optical sensor)
Design for preventing miss-ignition

Safety-Conscious Design
Flame-retardant materials Safe ignition switches
UL 94V-0-rated flame-retardant materials The switches perfectly fit finger contours and are positioned
are used for the instrument external near the window.
covers and atomizer unit. This superior To prevent inadvertent operation, both switches must be
design pays due consideration to safety. pressed simultaneously to start ignition.

Durable pipes and reliable couplings Clear window


All pipes are selected for durability and The large window permits observation of the flame, and the
used with highly reliable couplings. burner can be easily accessed through the large opening.
The window closes when released to eliminate the chance
of it being left open.

11
$$  Dual-Background Correction Functions
The optimal background correction methods are installed as standard:
high-speed self-reversal method (SR method) and deuterium lamp method (D2 method).

These functions can correct for spectral interference in flame measurement.


Selecting the optimal background correction method for each sample ensures
accurate and reliable analysis results.

Samples suitable for the SR method Samples suitable for the D 2 method

Samples with a complex matrix Purified water, tap water, environmental water, etc.
(Containing a large quantity of a specific element as the main component) Samples with a relatively simple matrix

SR (high-speed self-reversal) method –– accurate background correction over a wide range


Features
1. High-speed self-reversal (SR) correction is generally more accurate than deuterium lamp (D2) correction. As both atomic absorption and background
absorption can be measured using a single lamp, the correction errors due to light-axis misalignment are extremely small. This is ideal for the quantitation
of trace components in a matrix exhibiting complex background absorption, such as bio-samples and metals.
2. Permits background correction over the entire wavelength range from 185 nm to 900 nm.
3. This method can correct for spectral interference due to neighboring lines that can occur when a resonance line for another element exists near the
analytical line for the target element. (See table on next page.)
4. As no polarizer is used, measurements are possible with low light losses and a high S/N ratio.
5. The rapid lamp lighting permits accurate measurement unaffected by emission noise in the atomizer.
* Hollow cathode lamp L-2433 is required to use the SR method. It can also be used for the D2 method.

IH spectrum
Background absorption
Principle
Background A small current IL (approx. 10 mA) and a large current IH (approx. 500
Atomic absorption mA) are alternately passed through the hollow cathode lamp. The
Atomic lamp emission spectrum when the large current flows has a depression
Lamp current

IH absorption
in the center (self-reverse), due to self-absorption of the large number
of sputtered atoms in the atom cloud, as shown in the diagram to the
Wavelength Wavelength Atomic
Absorption absorption left. No significant atomic absorption is apparent and background
IL layer
IL spectrum absorption mainly occurs. Conversely, the lamp emission spectrum
Background
when the small current flows comprises a single narrow peak resulting
Time
Atomic absorption from both atomic absorption and background absorption. By
determining the difference between the two types of absorption, it is
possible to accurately correct for the background absorption and
(Lamp energy) (Sample measurement) (Energy component ratio)
measure the true atomic absorption.

Examples suitable for SR method (where differences result between SR and D2 methods)
Example: Measurement of trace levels of zinc in iron (analysis of Zn in Fe solution)
BGC-SR method BGC-D 2 method

Zn 0.25ppm
Atomic absorption signal
Atomic absorption signal Zn 0.50ppm
Background signal
Background signal
Fe 0.1%
Fe 0.5%

Fe 0.5% Zn 0.25ppm
Fe 0.5% Zn 0.5ppm

Fe 0.75% Zn 0.3ppm

The identical 0.5 ppm Zn solution is accurately corrected to Due to inadequate correction, the absorbance is higher at
the same absorbance at (2) and (6). (6) than at (2) for the identical 0.5 ppm Zn solution.

12
Examples of elements and wavelengths causing spectral
interference problems due to neighboring lines
Measured Element Analytical Line (nm) Coexisting Element Absorption Line (nm)
Al 309. 28 Mg 3 0 9 .3 0
As 193. 76 Fe 1 9 3 .7 3
Ca 422. 67 Fe 4 2 2 .6 4
Cd 228. 80 Ni 2 2 8 .8 4
Cu 324. 75 Fe 3 2 4 .7 3 The SR method is suitable for samples containing elements that cause
Ga 294. 36 Ni 2 9 4 .3 9 problems with spectral interference, as shown in the table to the left.
Mg 285. 21 Fe 2 8 5 .1 8
Ni 232. 00 Fe 2 3 2 .0 4
Pb 217. 00 Fe 2 1 6 .9 5
Sb 217. 58 Fe 2 1 7 .5 5
Se 196. 03 Fe 1 9 6 .0 5
Si 251. 61 Fe 2 5 1 .6 9
Zn 213. 856 Fe 2 1 3 .8 5 8 9

D2 (deuterium lamp) method –– highly sensitive background correction


Features
1. Detection sensitivity is superior to the SR method. Therefore, this method is suitable for the analysis of samples with a simple matrix requiring high
sensitivity, such as the measurement of trace levels of impurities in ultrapure water or environmental analyses.
2. As the lighting frequency is higher than with the SR method, it can eliminate noise due to emission components of the flame or graphite tube to permit
accurate atomic absorption measurements.
3. The original hollow cathode lamp can be used.

D2 lamp spectrum Background absorption


Principle
The deuterium lamp method involves lighting the hollow cathode lamp and the
deuterium lamp alternately at high speed. After separation by the monochromator,
Atomic absorption the light from the deuterium lamp has a bandwidth from 0.1 to 5 nm. Therefore, an
atomic absorption with a line width of only about 1/1000 nm is almost unobservable
compared to the background absorption due to wide-bandwidth molecular
absorption. However, as the light from the hollow cathode lamp has approximately
the same bandwidth as the atomic absorption band, the total of the atomic
absorption and the background absorption can be observed. With the deuterium
lamp (D2) method, light from both sources passes through the atomizer. The
difference in absorbance is determined to conduct background correction.
Hollow cathode lamp spectrum Atomic absorption + background absorption

Examples suitable for D2 method (where no difference results between SR and D2 methods)
Example: Measurement of trace levels of lead in 2% NaCl solution by molecular absorption (analysis of Pb in 2% NaCl solution)

BGC-SR method BGC-D 2 method

Background signal

Atomic absorption signal

Spike 0ppb 2ppb 4ppb Spike 0ppb 2ppb 4ppb


It can be seen that the sensitivity is higher with the BGC-D2 method.

13
Clear, Easy-to-Use Software
Features of the WizAArd Software
The WizAArd software used with the AA-6880 runs under Windows 7.

Wizard Functions Make Setting the Conditions So Simple That Even a Novice Can Do It.
Just set the measurement conditions using WizAArd to
complete the general settings.

The initial settings can also be completed simply


by following the Wizard procedures.

Start Wizard.

Select element.

Set calibration curve and sample parameters.

Set monochromator parameters.

Connect to instrument.

Measurement Screen Layout Shows Measurement Status at a Glance


Measured element Signal profile display

Real-time signal monitor Calibration curve display

MRT (Measured Results Table)


The worksheet shows sample names,
absorbance, concentrations,
and correction calibration results.

Lamp History Function Assists with Lamp Management


g
The accumulated operation time for each lamp displayed on the lamp
registration screen assists with lamp service life management. Multiple
lamps for the same element are differentiated using lamp IDs.

14
Software Provides Comprehensive Information Displays and Flexible Settings

Identical software operation for flame and furnace measurements


Even if the calibration curve is created after sample measurements,
concentration calculations can be conducted on past data. This
allows trial measurements to be directly used as actual
measurements.

Extrapolation of calibration curve range. If the sample concentration


exceeds the calibration curve range, additional measurements can be
performed on standard solutions to re-calculate the concentration.

Use existing calibration curves for measurements. Useful for sample


concentration order checks and for checking the instrument
sensitivity.

One-touch re-measurement operation. No need to repeat the


measurement from the beginning.

Create and save multiple calibration curves on a single worksheet.


Select the appropriate calibration curve for the sample concentration
and composition.

Combining a high-performance autosampler simplifies


p advanced settings
g
Real-time drying and ashing progress display for furnace
measurement
A higher temperature cleaning operation than the cleaning stage
can be added for each measurement. This reduces the graphite tube
memory effect. Tube deterioration is reduced by minimizing the
cleaning operations.

Add optional autosampler rinsing operations to ensure adequate


rinsing of the autosampler after completing the measurement of
high-concentration samples.

Set up sample dilution and spike-and-recovery tests on the same


screen.

Overlay function allows size and shape comparison of peak profiles.

Large-volume injection permits high-sensitivity measurements.

Precision control of drying and ashing temperatures reduces analysis


time.

15
$$  Supports System Management and Accuracy
FDA 21 CFR Part 11 Compliance

A combination of enhanced WizAArd software with Shimadzu's network-compatible CLASS-Agent data


management software supports FDA 21 CFR Part 11 compliance.
WizAArd used alone provides comprehensive system policy settings, as well as user management, log browser,
audit trail, and electronic signature system management functions.
Hardware validation software installed as standard.

Comprehensive Data Management Functions

System Policy CLASS-Agent (Option)


The system policy settings allow advanced Connection to CLASS-Agent permits
password and lockout settings. The levels efficient, long-term database
can be set in stages from "unrestricted" management of large amounts of analysis
to "Part 11 compatible". dat
data.

Userr Management
Use Mana
Managem
gement
ent
User management restricts the users of Log Br
Brows
Browser
owser
er
the system. It registers each user to The log browser easily displays a variety of logs to check the
determine how each one uses the system modification history and other log information.
software.

16
Management

Accuracy Management (QA/QC) Functions Permit User Level Management, Audit Trail, and Electronic Signatures
QA/QC compatibility
The QA/QC functions permit accuracy
management.

Hardware validation software installed as standard


The hardware validation software makes it simple to evaluate the instrument
performance. When combined with the autosampler, it automatically determines
the wavelength accuracy, noise level, baseline drift, absorbance and repeatability,
and prints out the results for comparison with the pass criteria.

* Data from all Shimadzu analytical instruments can be centrally managed by CLASS-Agent.

17
$$  Installation Conditions
Dimensions
Wall

Table

200
150
465

588
870

200 max.
280

ø150 to ø200

Exhaust fan

Damper

Approx. 500 × 500

417
1100 to 1200

Unit: mm
AA-6880 S=1: 2 0
Above dimensions do not include PC or printer.
702

GFA-6880

ASC-6880
390

340

702

960

Both for flame analysis and furnace analysis

18
Make sure all required equipment is available before starting instrument installation. See the installation guidelines for details.

Example of recommended piping for the atomic absorption system Operating Temperature range 10 to 35 °C
environment Humidity range 20 to 80% (less than 70% when temperature is higher than 30 °C)
Stainless steel piping 1500 mm min. (W) × 700 mm min. (D)
(inner diameter greater than 7 mm) Testing bench
Withstand load: 200 kg *1, 2
Stop cock Stop cock Setting pressure 0.11 MPa Material Stainless *3
Gas tube
Dimensions 7 mm min. I.D. × 80 mm min. (L)
Cylinder: 0.11 MPa
Acetylene
Pressure regulator
Lab: 0.09 MPa
Compressor: 0.4 MPa
Acetylene gas
Gas supply Air
Pressure range 0.3 MPa pressure Lab: 0.35 MPa
Setting pressure 0.09 MPa Setting pressure 0.4 MPa (set secondary Cylinder: 0.4 MPa
pressure) Dinitrogen oxide
Lab: 0.35 MPa
Cylinder: 0.4 MPa
Argon
Lab: 0.35 MPa
Material Stainless
Setting pressure 0.4 MPa
Dinitrogen For flame: Approx. 500 mm W × 500 mm D
oxide gas Dimensions
Pressure range 1 MPa Exhaust duct For furnace: ø150 mm to ø200 mm
Setting pressure 0.35 MPa
For flame: 600 to 1200 m3/hr
Intake capacity
For furnace: 10 to 180 m3/hr
Argon gas
Pressure range 1 MPa Cooling water (GFA-6880) Cooling water circulation unit or tap-water equipment *4
Setting pressure 0.35 MPa
*1 Atomic absorption spectrophotometer stand recommended
Setting pressure 0.4 MPa
Mist separator *2 Maintain a free maintenance space of 150 to 200 mm to the sides and rear of the instrument.
*3 Do not use pipes containing copper, silver, gold, or mercury (or alloys containing these metals)
Pressure range 1 MPa as pipes for acetylene.
Setting pressure 0.35 MPa *4 If tap-water equipment is used, ensure that it meets the specifications below.
Lab Outdoor
Compatible faucet Faucet 13 or 12 to 15 mm O.D. rimmed faucet
80 mm max. Air compressor
Water temperature 10 to 30 °C
Water flow rate 0.6 to 1.5 L/min
Supply pressure 0.08 to 0.15 MPa *5
Supply port 7 mm min.

*5 If the supply pressure exceeds 0.17 MPa, use the optional Regulator ASSY.

19
AA-6880 Series

For Research Use Only. Not for use in diagnostic procedure.


This publication may contain references to products that are not available in your country. Please contact us to check the availability of these
products in your country.
Company names, product/service names and logos used in this publication are trademarks and trade names of Shimadzu Corporation or its
affiliates, whether or not they are used with trademark symbol “TM” or “®”. Third-party trademarks and trade names may be used in this
publication to refer to either the entities or their products/services. Shimadzu disclaims any proprietary interest in trademarks and trade names
other than its own.

The contents of this publication are provided to you “as is” without warranty of any kind, and are subject to change without notice. Shimadzu
[Link]/an/ does not assume any responsibility or liability for any damage, whether direct or indirect, relating to the use of this publication.

© Shimadzu Corporation, 2016


First Edition: June 2016, Printed in Japan 3655-05613-20ANS

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