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Macroanalytical Procedures Manual (MPM)

Editors' Preface
The Macroanalytical Procedures Manual (MPM) is currently being revised to update its content
and add new material. In the interim, we have converted the original 1984 edition of the manual
for display on the FDA website. This website version was produced as a cooperative effort
between the editors and the Center for Food Safety and Applied Nutrition (CFSAN). Our
purpose is to provide access to the out-of-print 1984 manual until the revised edition is
available.

As editors, we have tried to faithfully restore the website manuscript its original 1984 content
and format. None of the methods have been changed. Where appropriate, we have inserted
clearly marked editorial comments that alert users to potential changes or other useful
information. In addition, we have updated (as far as possible) references to methods published
by AOAC International in their compendium "Official Methods of Analysis" and to FDA
Compliance Policy Guidelines.

We deeply appreciate and herein acknowledge the guidance of John C. Gecan (CFSAN)
throughout the project.

Table of Contents
Chapter Title

I. Introduction (/food/laboratory-methods/mpm-i-introduction) (Updated September 2023)

II. Apparatus for Macroanalytical Methods (/food/laboratory-methods/mpm-ii-apparatus-

macroanalytical-methods) (Updated September 2023)

III. Reagents for Macroanalytical Methods (/food/laboratory-methods-food/mpm-iii-reagents-

macroanalytical-methods) (Update May 2021)

IV. Special Techniques (/food/laboratory-methods/mpm-iv-special-techniques)

V. Macroanalytical Methods

V. 1. Beverage and Beverage Materials (/food/laboratory-methods/mpm-v-1-beverages-and-

beverage-materials)

V. A. Method for Coffee Beans (/food/laboratory-methods/mpm-v-1-beverages-and-

beverage-materials#v)

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Chapter Title

V. 2. Bakery Products, Cereals, and Alimentary Pastes (/food/laboratory-methods/mpm-v-2-

bakery-products-cereals-and-alimentary-pastes)

V. A. Method for Bakery Products, Cooked Cereals, and Alimentary Pastes

(/food/laboratory-methods/mpm-v-2-bakery-products-cereals-and-alimentary-
pastes#v)

V. B. Method for Modified Whole Grains (/food/laboratory-methods/mpm-v-2-bakery-

products-cereals-and-alimentary-pastes#v)

V. 3. Whole Grains and Pseudo-Grains (/food/laboratory-methods/mpm-v-3-grains-and-grain-

products) (Update May 2021)

V. A. Method for Wheat, Corn, Popcorn Kernels, and Rice

V. B. Method for Other Grains

V. C. Method for Pseudo-Grains

V. 4. Chocolate, Sugars, and Related Products (/food/laboratory-methods/mpm-v-4-chocolate-

sugars-and-related-products)

V. A. Method for Cocoa Beans (/food/laboratory-methods/mpm-v-4-chocolate-sugars-and-

related-products#v)

V. B. Method for Candy (/food/laboratory-methods/mpm-v-4-chocolate-sugars-and-

related-products#v)

V. 5. Miscellaneous and Multiple Food Products (/food/laboratory-methods/mpm-v-5-

miscellaneous-and-multiple-food-products)

V. A. Method for Plant Gums (/food/laboratory-methods/mpm-v-5-miscellaneous-and-

multiple-food-products#v)

V. 6. Dairy, Cheese, and Related Products (/food/laboratory-methods/mpm-v-6-dairy-cheese-

and-related-products) (Update July 2023)

V. A. Method for Casein and Sodium Caseinate (/food/laboratory-methods/mpm-v-6-

dairy-cheese-and-related-products#v)

V. 7. Seafood (/food/laboratory-methods/mpm-v-7-seafood)

V. A. Method for Microscopic Detection of Fish Tissue in Crab Meat or Crab Cakes
(/food/laboratory-methods/mpm-v-7-seafood#v)

V. B. Method for Determination of Parasites in Fin Fish (/food/laboratory-methods/mpm-v-

7-seafood#v)

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Chapter Title

V. 8. Spices, Condiments, Flavors, and Crude Drugs (/food/laboratory-methods/mpm-v-8-

spices-condiments-flavors-and-crude-drugs)

V. A. General Method for Spices, Herbs, and Botanicals (/food/laboratory-methods/mpm-

v-8-spices-condiments-flavors-and-crude-drugs#v)

V. B. Supplemental Method for Black and White Pepper (/food/laboratory-methods/mpm-

v-8-spices-condiments-flavors-and-crude-drugs#v)

V. C. SUPPLEMENTAL Method for Nutmegs (/food/laboratory-methods/mpm-v-8-spices-

condiments-flavors-and-crude-drugs#v)

V. 9. Fruits and Fruit Products (/food/laboratory-methods/mpm-v-9-fruits-and-fruit-products-v-

42-v-48)

V. A. Method for Apple Products (/food/laboratory-methods/mpm-v-9-fruits-and-fruit-

products-v-42-v-48#v)

V. B. Method for Decomposition in Blackberries, Raspberries and Other Drupelet Berries

(/food/laboratory-methods/mpm-v-9-fruits-and-fruit-products-v-42-v-48#v)

V. C. Method for Decomposition in Blueberries (/food/laboratory-methods/mpm-v-9-fruits-

and-fruit-products-v-42-v-48#v)

V. D. Method for Cherries (/food/laboratory-methods/mpm-v-9-fruits-and-fruit-products-v-

42-v-48#v)

V. E. Method for Canned and Frozen Fruits (/food/laboratory-methods/mpm-v-9-fruits-

and-fruit-products-v-51-v-78)

V. F. Method for Dried Fruits (/food/laboratory-methods/mpm-v-9-fruits-and-fruit-products-

v-51-v-78#v)

V. G. Method for Grape Products (/food/laboratory-methods/mpm-v-9-fruits-and-fruit-

products-v-51-v-78#v)

V. H. Method for Jams, Preserves, and Jellies (/food/laboratory-methods/mpm-v-9-fruits-

and-fruit-products-v-51-v-78#v)

V. I. Method for Lingonberries (/food/laboratory-methods/mpm-v-9-fruits-and-fruit-

products-v-51-v-78#v)

V. J. Method for Mincemeat (/food/laboratory-methods/mpm-v-9-fruits-and-fruit-products-

v-51-v-78#v)

V. K. Method for Olives (/food/laboratory-methods/mpm-v-9-fruits-and-fruit-products-v-51-

v-78#v)

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Chapter Title

V. L. Method for Pineapple Products (/food/laboratory-methods/mpm-v-9-fruits-and-fruit-

products-v-51-v-78#v)

V. M. Method for Raisins (/food/laboratory-methods/mpm-v-9-fruits-and-fruit-products-v-

51-v-78#v)

V. N. Method for Processed Strawberries (/food/laboratory-methods/mpm-v-9-fruits-and-

fruit-products-v-51-v-78#v)

V. 10. Nuts and Nut Products (/food/laboratory-methods/mpm-v-10-nuts-and-nut-products-

methods)

V. A. Method for In-shell and Shelled Tree Nuts (/food/laboratory-methods/mpm-v-10-

nuts-and-nut-products-methods#v)

V. B. Method for Peanuts and Peanut Siftings (/food/laboratory-methods/mpm-v-10-nuts-

and-nut-products-methods#v)

V. C. Method for Microscopic Detection of Foreign Plant Tissues in Peanut Butter

(/food/laboratory-methods/mpm-v-10-nuts-and-nut-products-methods#v)

V. 11. Vegetables and Vegetable Products (/food/laboratory-methods/mpm-v-11-vegetables-

and-vegetable-products)

V. A. Method for Asparagus (/food/laboratory-methods/mpm-v-11-vegetables-and-

vegetable-products#v)

V. B. Method for Brussels Sprouts (/food/laboratory-methods/mpm-v-11-vegetables-and-

vegetable-products#v)

V. C. Method for Microscopic Detection of Substitute Vegetable Tissues in Ground

Horseradish (/food/laboratory-methods/mpm-v-11-vegetables-and-vegetable-
products#v)

V. D. Method for Lettuce (/food/laboratory-methods/mpm-v-11-vegetables-and-vegetable-

products#v)

V. E. Method for Mushroom Products (/food/laboratory-methods/mpm-v-11-vegetables-

and-vegetable-products#v)

V. F. Method for the Reservation and Identification of Mushrooms (/food/laboratory-

methods/mpm-v-11-vegetables-and-vegetable-products#v)

V. G. Method for Peas and Beans (Canned, Frozen, and Dried) (/food/laboratory-
methods/mpm-v-11-vegetables-and-vegetable-products#v)

V. H. Method for Pickled Vegetables and Relish (/food/laboratory-methods/mpm-v-11-

vegetables-and-vegetable-products#v)

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Chapter Title

V. I. Method for Pimientos (/food/laboratory-methods/mpm-v-11-vegetables-and-

vegetable-products#v)

V. J. Method for Potato Chips (/food/laboratory-methods/mpm-v-11-vegetables-and-

vegetable-products#v)

V. K. Method for Corn Husks (/food/laboratory-methods/mpm-v-11-vegetables-and-

vegetable-products#v)

V. L. Method for Garlic Bulbs (/food/laboratory-methods/mpm-v-11-vegetables-and-

vegetable-products#v)

V. 12. Cosmetic Products (/food/laboratory-methods/mpm-v-12-cosmetic-products) (Updated

March 2023)

V. A. Method for Cosmetic Brushes (/food/laboratory-methods/mpm-v-12-cosmetic-

products#v)

VI. Applications of Macroanalytical Methods to Field Testing and Factory Samples

(/food/laboratory-methods/mpm-vi-applications-macroanalytical-methods-field-testing-and-
factory-sampling)

Glossary (/food/laboratory-methods/mpm-glossary)

Index of Tables and Figures (/food/laboratory-methods/mpm-index-tables-and-figures)

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