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Basic Analytical Techniques MCQ-1

This document contains a series of multiple-choice questions (MCQs) related to basic analytical techniques in chemistry, focusing on methods of separation and purification. Topics covered include filtration, distillation, crystallization, chromatography, and solvent extraction. Each question is followed by the correct answer and an explanation.

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0% found this document useful (0 votes)
1K views13 pages

Basic Analytical Techniques MCQ-1

This document contains a series of multiple-choice questions (MCQs) related to basic analytical techniques in chemistry, focusing on methods of separation and purification. Topics covered include filtration, distillation, crystallization, chromatography, and solvent extraction. Each question is followed by the correct answer and an explanation.

Uploaded by

pranav.ks1975
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd

XI - Science Marks : 50

LAKSHYA
SUBJECT : CHEMISTRY
MCQs Time (mm:ss) : 50:00
Basic Analytical Techniques

1. The most common method of separation of liquid from insoluble solid is

a) Distillation

b) Filtration

c) Chromatography

d) Solvent extraction

Ans 2
:

Exp Filtration
:

2. In filtration, insoluble part remaining on filter paper is called

a) filtrate

b) residue

c) sample

d) solution

Ans 2
:

Exp residue
:

3. Liquid collected in beaker after filtration is called as

a) filtrate

b) residue

c) sample

d) solution

Ans 1
:

Exp filtrate
:

4. If a crude solid is made of mainly one substance and has some impurities then it is purified by
__________.

a) Crystallization
b) Distillation

c) Extraction

d) Sublimation
Ans 1
:

Exp Crystallization
:

5. Benzoic acid can be purified by crystallization using solvent as

a) Ethyl alcohol

b) Water

c) Methyl alcohol

d) Acetone

Ans 2
:

Exp Water
:

6. Impure common salt can be purified by

a) crystallization

b) extraction

c) sublimation

d) distillation

Ans 1
:

Exp crystallization
:

7. The solvent used for crystallization must be

a) inert and volatile

b) sparingly soluble at room temperature

c) highly soluble at high temperature

d) all of the above

Ans 4
:

Exp all of the above


:

8. Which of the following solvent is most commonly used for the crystallization of CuSO4.

a) methanol
b) ether

c) water

d) acetone

Ans 3
:

Exp water
:

9. Which of the following methods can be used to separate two compounds with different
solubilities in the same solvent?

a) Fractional crystallization

b) Crystallization

c) Distillation

d) Solvent extraction
Ans 1
:

Exp Fractional crystallization


:

10. A mixture of acetone and benzene can be sperated by the following method ________.

a) Simple distillation

b) Fractional distillation

c) Distillation under reduced pressure

d) Sublimation
Ans 2
:

Exp Fractional distillation


:

11. In distillation of liquid, water condenser is used

a) to boil the liquid

b) to collect the liquid

c) to condense hot vapours of the liquid

d) to absorb the liquid

Ans 2
:

Exp to collect the liquid


:

12. Different liquids boil and evaporate at different temperature is the principle of
a) Distillation

b) Crystallization

c) Solvent extraction

d) Fractional crystallization

Ans 1
:

Exp Distillation
:

13. Mercury is distilled

a) at high pressure

b) at low pressure

c) at moderate pressure

d) in vacuum

Ans 4
:

Exp in vacuum
:

14. The method is used for the purification of liquid which boil without decomposition

a) simple distillation

b) fractional crystallization

c) distillation under reduced pressure

d) sublimation

Ans 1
:

Exp simple distillation


:

15. Which of the following techniques is used for separation of glycerol from soap in soap industry?

a) Distillation under reduced pressure

b) Fractional distillation

c) Filtration

d) Crystallization
Ans 1
:

Exp Distillation under reduced pressure


:

16. This method is used for the purification of liquids which have a very high boiling point
a) Simple distillation

b) Fractional distillation

c) Distillation under reduced pressure

d) Sublimation

Ans 3
:

Exp Distillation under reduced pressure


:

17. Glycerol is purified by

a) steam distillation

b) vacuum distillation

c) fractional distillation

d) simple distillation

Ans 2
:

Exp vacuum distillation


:

18. Separation of binary mixture of acetone and methyl alcohol is done by _______.

a) Simple distillation

b) Fractional distillation

c) Fractional crystallization

d) Re-crystallization
Ans 2
:

Exp Fractional distillation


:

19. Which of the following method is uesd to separate different fractions of crude oil?

a) Solvent extraction

b) Simple distillation

c) Fractional distillation

d) TLC
Ans 3
:

Exp Fractional distillation


:
20. Fractional distillation is a type of distillation which involves the separation of

a) miscible liquids

b) immiscible liquids

c) mixtures

d) solids and liquids

Ans 1
:

Exp miscible liquids


:

21. Fractional distillation depends upon

a) Boiling point

b) Freezing point

c) Melting point

d) All of the above

Ans 1
:

Exp Boiling point


:

22. A common example of fractional distillation in industries is separation of various components of

a) Coal

b) Crude oil

c) Petrol

d) Diesel

Ans 2
:

Exp Crude oil


:

23. Which of the following techniques can be used to separate a mixture of liquid which do not differ much in
their boiling point ?

a) Fractional distillation

b) Simple distillation

c) Vacuum distillation

d) Evaporation

Ans 1
:

Exp Fractional distillation


:
24. The process of separation of components by using difference in boiling point is called as

a) Distillation

b) Crystallization

c) Solvent extraction

d) Fractional crystallization

Ans 1
:

Exp Distillation
:

25. Which of the following is used in fractional distillation?

a) Adsorbent column

b) Fractionating column

c) Separating column

d) Buchner funnel

Ans 2
:

Exp Fractionating column


:

26. Which technique cannot be used to purify a solid ?

a) Sublimation

b) Filtration

c) Crystallization

d) Fractional distillation

Ans 4
:

Exp Fractional distillation


:

27. Which technique is widely used in industry to separate components of mixture and also to purify
them?

a) Steam distillation

b) Chromatography

c) Solvent extraction

d) Filtration
Ans 2
:
Exp Chromatography
:

28. Colourless components on chromatogram CANNOT be observed by which of the following?

a) Using UV light

b) Using iodine chamber

c) Using the spraying reagent

d) Using infrared light


Ans 4
:

Exp Using infrared light


:

29. The stationary phase and mobile phase in partition chromatography are _______ respectively.

a) Solid and liquid

b) Solid and gas

c) Liquid and solid

d) Liquid and liquid


Ans 4
:

Exp Liquid and liquid


:

30. The principle of differential adsorption is applicable for which of the following chromatographic
technique ?

a) Column chromatography

b) Thin layer chromatography

c) Paper chromatography

d) Both (a) and (b)


Ans 4
:

Exp Both (a) and (b)


:

31. Paper chromatography is based on the principle of _________.

a) Adsorption

b) Partition

c) Solubility

d) Volatility
Ans 2
:

Exp Partition
:

32. In paper chromatography, the mobile phases rises up the chromatography paper due to
___________.

a) Evaporation of volatile solvent

b) Capillary action

c) Gravitational force

d) Differential adsorption
Ans 2
:

Exp Capillary action


:

33. Principle of paper chromatography is

a) Differential partioning

b) Differential adsorption

c) Difference in solubility of solute in two solids

d) Difference in the degree to which solutes are adsorbed.

Ans 1
:

Exp Differential partioning


:

34. In paper chromatography paper sheets are used as :

a) Adsorbate

b) Adsorbent

c) Solvent

d) Sampel

Ans 2
:

Exp Adsorbent
:

35. In paper chromatography paper sheets acts as

a) Stationary phase

b) Mobile phase

c) Neither
d) Both

Ans 1
:

Exp Stationary phase


:

36. Which of the following is separated through column chromatography ?

a) Chlorophyll and carotenoids

b) Inorg. cations or complex

c) Sugar derivative

d) Amino acid

Ans 1
:

Exp Chlorophyll and carotenoids


:

37. Column chromatography is based on principle on

a) Absorption

b) Differential adsorption

c) Ion exchange

d) Exclusion principle

Ans 2
:

Exp Differential adsorption


:

38. Which factor is responsible for separation in column chromatography ?

a) Polarity difference between solvent

b) Polarity difference between solute

c) Polarity indifference between solvent

d) Polarity indifference between solvent

Ans 2
:

Exp Polarity difference between solute


:

39. Paper chromatography is an example of

a) Partition

b) TLC

c) Column
d) Adsorption

Ans 1
:

Exp Partition
:

40. On a TLC plate is found, that a compound moves 12cm and solvent moves 15cm. What is retention factor for
the compound.

a) 0.5

b) 0.8

c) 1.08

d) 0.75

Ans 2
:

Exp 0.8
:

41. The stationary phase and mobile phase in TLC are ________ respectively.

a) Solid and liquid

b) Solid and gas

c) Liquid and solid

d) Liquid and liquid


Ans 1
:

Exp Solid and liquid


:

42. Which of the following means Retention factor (RF) ?

a) Ratio of distance travelled by solute to the distance travelled by solvent

b) Ratio of distance travelled by solvent to the distance travelled by solute

c) Ratio of the concentration of the solute in one phase to its concentration in the other phase.

d) Ratio of concentration of solute in organic phase to its concentration in the aqueous phase.

Ans 1
:

Exp Ratio of distance travelled by solute to the distance travelled by solvent


:

43. Adsorption chromatography is a chromatographic technique based on the principle of _________.

a) Differential adsorption

b) Differential solubility
c) Differential extraction

d) All of these
Ans 1
:

Exp Differential adsorption


:

44. Which reagent is used as a spraying agent to detect amino acids on TLC plates ?

a) Bromocresol green

b) Ninhydrin

c) Fuchsin

d) Rhodamine B

Ans 2
:

Exp Ninhydrin
:

45. Which of the following method involves separation of substances in a mixture on thick layer of adsorbent ?

a) Solvent extraction

b) Fractional distillation

c) Crystallization

d) Chromatography

Ans 4
:

Exp Chromatography
:

46. Which of the following method will give clean separation of sample of chloroform (organic liquid)
and water in short time span?

a) TLC

b) Distillation under reduced pressure

c) Solvent extraction

d) Simple distillation
Ans 3
:

Exp Solvent extraction


:

47. Which method can be used to separate a compound based on difference in solubility in two liquids ?

a) Distillation
b) Solvent extraction

c) Fractional distillation

d) Crystallization

Ans 2
:

Exp Solvent extraction


:

48. The principle of separation of substances in chromatography is similar to this method

a) Solvent extraction

b) Fractional crystallization

c) Simple distillation

d) Sublimation

Ans 1
:

Exp Solvent extraction


:

49. Separating funnel is used mainly to segregate

a) Two immiscible liquids

b) Two miscible solids

c) Homogenous mixture

d) Heterogenous mixture

Ans 1
:

Exp Two immiscible liquids


:

50. The method used to separate a given organic compound present inaqueous solution by shaking with a
suitable solvent in which the compound is more soluble than water is called

a) Simple distillation

b) Solvent extraction

c) Crystallization

d) Fractional distillation

Ans 2
:

Exp Solvent extraction


:

* ALL THE BEST *

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