DOC023.52.

90643

BioTector B7000i Online TOC Analyzer

Maintenance and Troubleshooting

01/2024, Edition 3
 Table of Contents

Section 1 Maintenance ....................................................................................................................... 3

1.1 Safety information........................................................................................................................ 3
1.1.1 Safety symbols and markings............................................................................................ 3
1.1.2 Use of hazard information................................................................................................... 4
1.1.3 Electrical safety precautions................................................................................................4
1.1.4 Ozone precautions.............................................................................................................. 4
1.2 Maintenance schedule................................................................................................................. 5
1.3 Weekly maintenance.................................................................................................................... 5
1.4 Fill or replace the reagents........................................................................................................... 6
1.5 Replace a fuse............................................................................................................................. 6
1.6 Shutdown procedure.................................................................................................................... 8
1.6.1 Flush the reagent lines........................................................................................................ 9
Section 2 Troubleshooting ..............................................................................................................11
2.1 System Faults............................................................................................................................ 11
2.2 System warnings........................................................................................................................ 13
2.3 Notifications................................................................................................................................ 19
2.4 Show the status history before a fault........................................................................................ 19
Section 3 Diagnostics ...................................................................................................................... 21
3.1 Do a pressure test...................................................................................................................... 21
3.2 Do a flow test............................................................................................................................. 21
3.3 Do an ozone test........................................................................................................................ 22
3.4 Do a sample pump test.............................................................................................................. 22
3.5 Do a pH test............................................................................................................................... 23
3.6 Do a sample valve test............................................................................................................... 24
3.7 Do simulations .......................................................................................................................... 25
3.8 Do a relay or 4–20 mA output test............................................................................................. 27
3.9 Show the input and output status............................................................................................... 27
3.10 Show the oxygen controller status........................................................................................... 28
3.11 Show the Modbus status.......................................................................................................... 29
3.12 Modbus troubleshooting........................................................................................................... 29
Section 4 Analysis enclosure ......................................................................................................... 31
Section 5 Control enclosure components ...................................................................................35
Section 6 Replacement parts and accessories .......................................................................... 37

1
Table of Contents

2
Section 1 Maintenance

DANGER
Multiple hazards. Only qualified personnel must conduct the tasks described in this
section of the document.

1.1 Safety information

Please read this entire manual before maintenance tasks or troubleshooting is done on
this equipment. Pay attention to all danger and caution statements. Failure to do so could
result in serious injury to the operator or damage to the equipment.
Make sure that the protection provided by this equipment is not impaired. Do not use or
install this equipment in any manner other than that specified in this manual.
1.1.1 Safety symbols and markings
Read all labels and tags attached to the instrument. Personal injury or damage to the
instrument could occur if not observed. A symbol on the instrument is referenced in the
manual with a precautionary statement.
The safety symbols and marking that follow are used on the equipment and in the product
documentation. The definitions are in the table that follows.
Caution/Warning. This symbol identifies that an appropriate safety instruction should be followed or a potential
hazard exists.

Hazardous voltage. This symbol indicates that hazardous voltages are present where a risk of electrical shock
exists.

Hot surface. This symbol indicates that the marked item can be hot and should not be touched without care.

Corrosive substance. This symbol identifies the presence of a strong corrosive or other hazardous substance and a
risk of chemical harm. Only individuals qualified and trained to work with chemicals should handle chemicals or
perform maintenance on chemical delivery systems associated with the equipment.
Toxic. This symbol indicates a toxic/poisonous substance hazard.

This symbol indicates the presence of devices sensitive to Electro-static Discharge (ESD) and indicates that care
must be taken to prevent damage with the equipment.

This symbol indicates a flying debris hazard.

Protective earth. This symbol indicates a terminal which is intended for connection to an external conductor for
protection against electric shock in case of a fault (or the terminal of a protective earth (ground) electrode).

Noiseless (clean) earth. This symbol indicates a functional earthing (grounding) terminal (e.g., a specially designed
earthing (grounding) system) to avoid a malfunction of the equipment.

This symbol indicates an inhalation hazard.

This symbol indicates there is a lifting hazard because the object is heavy.

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Maintenance

This symbol indicates a fire hazard.

Electrical equipment marked with this symbol may not be disposed of in European domestic or public disposal
systems. Return old or end-of-life equipment to the manufacturer for disposal at no charge to the user.

1.1.2 Use of hazard information

The alert boxes that follow are used in this document to indicate important instructions for
the safe operation of the equipment.

DANGER
Indicates a potentially or imminently hazardous situation which, if not avoided, will result in death
or serious injury.

WARNING
Indicates an instruction for a potentially hazardous situation that may result in death or a serious
injury.

CAUTION
Indicates that a precaution must be followed for a potentially hazardous situation that may result in
minor or moderate injury.

NOTICE
Indicates a situation which, if not avoided, may cause damage to the instrument. Information that
requires special emphasis.

1.1.3 Electrical safety precautions

The power supplies in the electrical enclosure contain capacitors that are charged to
hazardous voltages. After the main power is disconnected, let the capacitors discharge
(1 minute minimum) before the electrical enclosure is opened.
1.1.4 Ozone precautions

CAUTION
Ozone inhalation hazard. This instrument produces ozone that is contained within the
equipment, specifically within the internal plumbing. The ozone could be released under
fault conditions.

It is recommended to plumb the exhaust gas port to a fume hood or to the building
exterior in accordance with local, regional and national requirements.
Exposure to even low concentrations of ozone can damage delicate nasal, bronchial and
pulmonary membrane. In sufficient concentration, ozone can cause headaches,
coughing, eye, nose and throat irritation. Immediately, move the victim to uncontaminated
air and seek first aid.
The type and harshness of symptoms are based on the concentration and exposure time
(n). Ozone poisoning includes one or more of the symptoms that follow.
• Irritation or burning of the eyes, nose or throat
• Lassitude
• Frontal headache
• Sensation of sub-sternal pressure
• Constriction or oppression

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 Maintenance

• Acid taste in mouth

• Asthma
In case of more severe ozone poisoning, the symptoms can include dyspnea, cough,
choking sensation, tachycardia, vertigo, lowering of blood pressure, cramping, chest pain,
and generalized body pain. Ozone can cause a pulmonary oedema one or more hours
after exposure.

1.2 Maintenance schedule

NOTICE
To prevent instrument damage, weekly maintenance must be done by a Hach trained operator or
Hach trained maintenance personnel.
To prevent instrument damage, 6-month maintenance and troubleshooting must be done by Hach
trained maintenance personnel.

Table 1 shows the recommended schedule of maintenance tasks. Facility requirements

and operating conditions may increase the frequency of some tasks.
Table 1 Maintenance schedule
Task 1 week 6 months 12 months As necessary
Weekly maintenance X
on page 5
6-month maintenance1 X
Fill or replace the X
reagents on page 6
Replace a fuse X
on page 6
Shutdown procedure X
on page 8

1.3 Weekly maintenance

Use the checklist that follows to complete weekly maintenance. Do the tasks in the order
given.
Task Initial
Select OPERATION > START,STOP > FINISH & STOP or EMERGENCY STOP.
Wait for the display to show "SYSTEM STOPPED".
Make sure that the instrument air pressure supplied to the analyzer is correct.

• Instrument air plumbed to analyzer—1.5 bar

• BioTector compressor plumbed to analyzer—1.2 bar

Select MAINTENANCE > DIAGNOSTICS > SIMULATE. Select MFC. Set the flow to 20 L/h. Push to start
the mass flow controller (MFC). The measured flow shows on the display.

Make sure that the oxygen pressure regulator shows 400 mbar at 20 L/h. Refer to Analysis enclosure
on page 31 for the location.
Make sure that the reagent levels are sufficient. Fill or replace reagent containers as necessary. Refer to Fill
or replace the reagents on page 6.

1 Refer to the documentation supplied with the maintenance kit for instructions.

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Maintenance

Task Initial
Make sure that there are no leaks at the reagent pumps. Refer to Analysis enclosure on page 31 for the
location.
Make sure that there are no leaks at the sample pump.
Make sure that the oxidized sample catch-pot has no leaks.
Make sure that there are no leaks at the valves in the analyzer. Refer to Analysis enclosure on page 31 for
the location.
Make sure that there are no blockages in the sample lines to the analyzer or the sample lines in the analyzer.
Make sure that there are no blockages in the drain lines from the analyzer or the drain lines in the analyzer.
Make sure that there is sufficient sample flow to the oxidized sample catch-pot or the sample tubing for a fresh
sample for each analysis cycle.
Make sure that there is no blockage in the exhaust tubing.
Make sure that there are no blockages in the filter in the fan housing and the vent housing on the side of the
analyzer.
If a sampler is used, make sure that the operation of the sampler is correct. Make sure that there is sufficient
flow to the sample pipe.

1.4 Fill or replace the reagents

CAUTION
Chemical exposure hazard. Obey laboratory safety procedures and wear all of the
personal protective equipment appropriate to the chemicals that are handled. Refer to
the current safety data sheets (MSDS/SDS) for safety protocols.

CAUTION
Chemical exposure hazard. Dispose of chemicals and wastes in accordance with local,
regional and national regulations.

Fill or replace the acid and base reagent containers as necessary when the analyzer is
stopped.

1. Select OPERATION > START,STOP > FINISH & STOP or EMERGENCY STOP.
2. Fill or replace the reagents.
3. Select MAINTENANCE > COMMISSIONING > REAGENTS MONITOR.
4. Set the reagents volumes.
5. Select OPERATION > REAGENTS SETUP> INSTALL NEW REAGENTS to prime
the reagent tubing and do a zero calibration.

1.5 Replace a fuse

DANGER
Electrocution hazard. Isolate all power to the instrument and disconnect all power from
the instrument and relay connections before this maintenance task is started

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 Maintenance

DANGER
Electrocution hazard. Use the same type and current rating to replace fuses.

Replace a blown fuse for correct operation. Refer to Figure 1 for the fuse locations. Refer
to Table 2 for the fuse specifications.
In addition, a diagram of the fuse locations is available on the top door.

Figure 1 Fuse location diagram

Table 2 Fuse specifications

Item Name Number Size Material Number Current Type
1 Cooler DIN rail Terminal 47 Miniature Ceramic F1 2.5 A (DC) T 2.5A H250V
5 x 20 mm
2 Relay PCB 81204001-03 Miniature Glass F1 2.5 A (DC) T 2.5 A L125V DC
5 x 20 mm
F2 0.5 A (DC) T 500mA L 125V DC
F3 0.5 A (DC) T 500mA L 125V DC
F4 1.0 A (DC) T 1A L125 V DC
F5 1.0 A (DC) T 1A L125 V DC
F6 1.0 A (DC) T 1A L125 V DC
F7 1.0 A (DC) T 1A L125 V DC
F8 1.0 A (DC) T 1A L125 V DC

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Maintenance

Table 2 Fuse specifications (continued)

Item Name Number Size Material Number Current Type
3 115 VAC Power PCB (Mains PCB) 81204030-03 Miniature Ceramic F1 T 2.5 A T 2.50A H250V
5 x 20 mm
F2 0.5 A T 500 mA H250V
F3 1.0 A T 1A H250V
F4 2.5 A T 2.50A H250V
F5 3.15 A T 3.15A H250V
F6 0.5 A T 500mA H250V
4 230 VAC Power PCB (Mains PCB) 81204030-03 Miniature Ceramic F1 T 2.5 A T 2.50A H250V
5 x 20 mm
F2 0.5 A T 500mA H250V
F3 1.0 A T 1A H250V
F4 1.6 A T 1.60A H250V
F5 2.0 A T 2A H250V
F6 0.5 A T 500mA H250V
5 Main board (Motherboard) 81204022-09 Miniature Glass F1 0.5 A (DC) T 500mA L125V DC
5 x 20 mm
6 Signal PCB 81204010-02 Miniature Glass F1 1.0 A (DC) T 1A L125V DC
5 x 20 mm
F3 0.5 (DC) T 500mA L125V DC
7 Stream Expansion PCB 81204040-02 Miniature Glass F1 1.0 A (DC) T 1A L125V DC
5 x 20 mm

Key:
A—Amperes
F—Fuse
H—High interrupt
ID—Identification
L— Low interrupt
mA—Milliamperes
PCB—Printed circuit board
T—Time lag (time delay)
V—Volts

1.6 Shutdown procedure

If power will be removed from the analyzer for more than 2 days, use the checklist that
follows to prepare the analyzer for shutdown or storage. Do the tasks in the order given.
Task Initial
Select OPERATION > START,STOP > FINISH & STOP or EMERGENCY STOP.
Wait for the display to show "SYSTEM STOPPED".
Remove the reagent from the reagent lines for safety. Refer to Flush the reagent lines on page 9.
Disconnect the SAMPLE fittings from the sample sources. Connect the SAMPLE fittings to an open drain or
empty plastic container.

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 Maintenance

Task Initial
Do the steps that follow:

1. Select MAINTENANCE > DIAGNOSTICS > SIMULATE > CLEANING VALVE. Select ON to open the
cleaning valve.
2. Make sure that all of the stream, manual and calibration valves are closed.
3. Select SAMPLE PUMP, then select REV to set the pump to operate in reverse. Operate the sample pump
in reverse until the sample lines and the oxidized sample catch-pot are empty.

Remove power to the analyzer.

1.6.1 Flush the reagent lines

CAUTION
Chemical exposure hazard. Obey laboratory safety procedures and wear all of the
personal protective equipment appropriate to the chemicals that are handled. Refer to
the current safety data sheets (MSDS/SDS) for safety protocols.

CAUTION
Chemical exposure hazard. Dispose of chemicals and wastes in accordance with local,
regional and national regulations.

Remove the reagent from the reagent lines for safety.

1. Put on the personal protective equipment identified in the safety data sheets
(MSDS/SDS).
2. Remove the tubes from the ACID and BASE ports on the side of the analyzer.
3. Plumb the ACID and BASE ports to a deionized water container. If deionized water is
not available, use tap water.
4. Select CALIBRATION > ZERO CALIBRATION > RUN REAGENTS PURGE to start a
purge cycle.
5. Do step 4 a second time.
The analyzer replaces the reagents in the reagents lines with water.
6. When the reagent purge cycle is complete, remove the tubing from the deionized
water container and put them in open air.
7. Do step 4 two times.
The analyzer replaces the water in the reagents lines with air.

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Maintenance

10
Section 2 Troubleshooting

2.1 System Faults

Select OPERATION > FAULT ARCHIVE to see the system faults that have occurred.
Faults and warnings with an asterisk (*) are active.
When "SYSTEM FAULT" shows in the top-left corner of the Reaction Data screen or the
Reagent Status screen, a system fault has occurred. Measurements have stopped. The
4–20 mA outputs are set to the fault level (default: 1 mA). The system fault relay is set to
onif configured..
To start the analyzer again, complete the troubleshooting steps for the system fault. Refer
to Table 3. To acknowledge the fault, select the fault and push .
Note: There are system faults (e.g., 05_Pressure Test Fail) that cannot be acknowledged by the
user. These faults are reset and acknowledged automatically by the system when the system is
started, the system is rebooted or when the fault condition is removed.
Table 3 System Faults
Message Description Cause and solution
01_LOW O2 FLOW - The oxygen flow through the exhaust • Oxygen supply problem. The oxygen pressure
EX (EX) valve (MV1) was less than 50% of should be 400 mbar (±10 mbar) at 20 L/h MFC flow.
the oxygen flow MFC (mass flow Select MAINTENANCE > DIAGNOSTICS > O2-
controller) setpoint for more than the CTRL STATUS.
LOW O2 FLOW TIME setting.
• Blockage in the ozone destructor
Refer to MAINTENANCE > SYSTEM • Blockage in the tube after the MFC
CONFIGURATION > FAULT SETUP >
• Failure of or blockage in the exhaust valve
LOW O2 FLOW TIME.
• Failure of the MFC. Do a flow test. Refer to Do a flow
test on page 21.

02_LOW O2 FLOW - The oxygen flow through the sample • Oxygen supply problem. The oxygen pressure
SO out (SO) valve (MV5) was less than should be 400 mbar (±10 mbar) at 20 L/h MFC flow.
50% of the MFC setpoint for more than Select MAINTENANCE > DIAGNOSTICS > O2-
the LOW O2 FLOW TIME setting. CTRL STATUS.
Refer to MAINTENANCE > SYSTEM • Failure of or blockage in the sample out valve
CONFIGURATION > FAULT SETUP > • Failure of or blockage in the exhaust valve (MV1)
LOW O2 FLOW TIME.
• Failure of the MFC. Do a flow test. Refer to Do a flow
test on page 21.

03_HIGH O2 FLOW The oxygen flow through the exhaust • Failure of the MFC
valve (MV1) was more than 50% of the
• Oxygen supply problem. The oxygen pressure
MFC setpoint for more than the HIGH
should be 400 mbar (±10 mbar) at 20 L/h MFC flow.
O2 FLOW TIME setting.
Select MAINTENANCE > DIAGNOSTICS > O2-
Refer to MAINTENANCE > SYSTEM CTRL STATUS.
CONFIGURATION > FAULT SETUP >
HIGH O2 FLOW TIME.
04_NO REACTION No TOC (or TC) CO2 peak or the CO2 • The acid reagent and/or base reagent are the
(can be set as a fault or peak is less than the CO2 LEVEL incorrect concentration.
warning) setting for three consecutive reactions.
• The acid reagent container and/or base reagent
Refer to MAINTENANCE > SYSTEM container are empty.
CONFIGURATION > REACTION • The acid and/or base reagent lines have a blockage
CHECK > CO2 LEVEL. or air bubbles.
• The operation of the acid pump and/or base pump is
incorrect.
• The operation of the mixer reactor is incorrect. Do a
pH test. Refer to Do a pH test on page 23.

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Troubleshooting

Table 3 System Faults (continued)

Message Description Cause and solution
05_PRESSURE TEST The MFC flow did not decrease to less • The analyzer has a gas and/or liquid leak.
FAIL than the PRESSURE TEST FAULT
• A valve has a leak.
setting during the pressure test.
• Examine the sample out valve, sample (ARS) valve
Refer to MAINTENANCE > SYSTEM and analyzer fittings for leaks.
CONFIGURATION > SEQUENCE
• Examine the mixer reactor for leaks. Do a pressure
PROGRAM > PRESSURE/FLOW
test. Refer to Do a pressure test on page 21.
TEST > PRESSURE TEST FAULT.
06_PRESSURE CHCK The MFC flow did not decrease to less
FAIL than the PRESSURE CHCK FAULT
setting during the pressure check for
three consecutive reactions (default).
Refer to MAINTENANCE > SYSTEM
CONFIGURATION > SEQUENCE
PROGRAM > PRESSURE/FLOW
TEST > PRESSURE CHCK FAULT.
08_RELAY PCB FAULT • 81204001 relay board has a blown Examine the 24V DC input power. Examine the fuses on
fuse. the relay board. Refer to Control enclosure components
on page 35 for the location. Examine the fuse F3 on the
• 81204010 signal board has a
signal board.
blown fuse, F3.
• The operation of the 24V PSU is LED 6 on the signal board is set to off when the fault is
incorrect. corrected.

09_OZONE PCB The operation of the ozone board is Replace the ozone board. Contact technical support.
FAULT incorrect.
11_CO2 ANALYZER The operation of the CO2 analyzer is Examine the 24V DC input power to the CO2 analyzer
FAULT incorrect. from the motherboard wires 101 and 102). Refer to
Control enclosure components on page 35 for the
location.
Examine the signal from the CO2 analyzer. Open the CO2
analyzer and clean the lenses.
Remove and then apply power to the analyzer.
For more tests, refer to the information sheet T019.
BioTector CO2 Analyzer Troubleshooting.
12_HIGH CO2 IN O2 There is a high level of CO2 in the input Select MAINTENANCE > DIAGNOSTICS > SIMULATE.
oxygen gas. If the CO2 value on the display is more than 250 to
300 ppm, examine the oxygen purity.
Identify if there is CO2 contamination in the oxygen
supply. Refer to Examine the oxygen supply in the
Operation and Installation Manual.
If the oxygen purity is sufficient, open the CO2 analyzer
and clean the lenses. If the problem continues, replace
the CO2 analyzer filters.
If the oxygen purity is not satisfactory, replace the oxygen
concentrator.
13_SMPL VALVE SEN The sample valve sensors are in a Identify if faults 14_SAMPLE VALVE SEN1, 15_SAMPLE
SEQ wrong sequence. The sample valve VALVE SEN2 or 16_SAMPLE VALVE SEN3 have
sensors should be in the sequence occurred.
Sensor 1, 2 and 3. Examine fuse F6 on the Relay PCB. Select
MAINTENANCE > DIAGNOSTICS > SAMPLE VALVE.
Examine the operation of the sample valve. Examine the
sample valve sensor wiring.

12
 Troubleshooting

Table 3 System Faults (continued)

Message Description Cause and solution
14_SAMPLE VALVE Sample Valve Sensor 1, 2 or 3 did not Examine fuse F6 on the Relay PCB. The operation of the
SEN1 show the position of the valve. sample valve sensors is incorrect or there is an
15_SAMPLE VALVE orientation problem. Examine the wiring on the valve
SEN2 board and on the Signal PCB. Refer to Control enclosure
components on page 35 for the location.
16_SAMPLE VALVE
SEN3 Examine the sensor signals. Look at LEDs 12, 13 and
14 on the Signal PCB and DI01, DI02 and DI03 in the
DIGITAL INPUT menu. Select MAINTENANCE >
DIAGNOSTICS > INPUT/OUTPUT STATUS > DIGITAL
INPUT. Refer to Control enclosure components
on page 35 for the board location.
Replace the valve assembly.
17_SMPL VALVE NOT The correct sensor position (Sensor 1) Replace Relay 4 on the Relay PCB. Refer to Control
SYNC was not identified in the sample valve enclosure components on page 35 for the location.
when the sample pump is in operation. Examine the sensor signal. Look at LED 12 on the signal
board and DI01 in DIGITAL INPUT menu. Select
MAINTENANCE > DIAGNOSTICS > INPUT/OUTPUT
STATUS > DIGITAL INPUT. Refer to Control enclosure
components on page 35 for the board location.
Select MAINTENANCE > DIAGNOSTICS > SAMPLE
VALVE. Examine the sample valve SEN1 position and
SEN1 signal.
For more tests, refer to the information sheets T018.
BioTector Sample Valve Not Synchronized Fault
Troubleshooting and TT002. BioTector Sample Valve Not
Sync Fault Quick Troubleshooting.
18_LIQUID LEAK DET A liquid leak detector in the analyzer is Look for a liquid leak in the analyzer enclosure.
active. There is a liquid leak. Disconnect the leak detector connector on the bottom of
the reactor to identify if the reactor has a leak. Examine
the liquid leak detector.
20_NO REAGENTS The calculated reagent levels identify Replace the reagents. Refer to Fill or replace the
(can be set as a fault, that the reagent containers are empty. reagents on page 6.
warning or notification)
129_REACT PURGE There is a blockage in the reactor, There is an air or oxygen supply problem. Look at the
FAIL sample out valve or the associated O2-CTRL STATUS menu to examine the oxygen
tubing and fittings. The MFC operation pressure. The pressure is usually 400 mbar (±10 mbar) at
is not correct or the MFC tubing has a 20 L/h MFC flow.
blockage. Do a flow test. Refer to Do a flow test on page 21.

2.2 System warnings

Select OPERATION > FAULT ARCHIVE to see the warnings that have occurred. Faults
and warnings with an asterisk (*) are active.
When "SYSTEM WARNING" shows in the top-left corner of the Reaction Data screen or
the Reagent Status screen, a warning occurred. Measurements continue. The 4-20 mA
outputs do not change. The system fault relay is not set to on.
Complete the troubleshooting steps for the warning. Refer to Table 4. To acknowledge
the warning, select the warning and push .
If there are multiple warnings in the instrument, examine the fuses on the relay board and
signal board.

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Troubleshooting

Table 4 System warnings

Message Description Cause and solution
21_CO2 ANL LENS The optical device of the CO2 analyzer is Clean the CO2 analyzer. Clean the lenses in the CO2
DIRTY dirty. analyzer.
22_FLOW WARNING – The oxygen flow through the exhaust • Oxygen supply problem. The oxygen pressure
EX (EX) valve (MV1) decreased to less than should be 400 mbar (±10 mbar) at 20 L/h MFC
the FLOW WARNING setting during the flow. Select MAINTENANCE > DIAGNOSTICS >
pressure test. O2-CTRL STATUS.
Refer to MAINTENANCE > SYSTEM • Blockage in the ozone destructor
CONFIGURATION > SEQUENCE • Blockage in the tube after the mass flow
PROGRAM > PRESSURE/FLOW TEST controller (MFC)
> FLOW WARNING.
• Failure of or blockage in the exhaust valve
• Failure of the MFC. Do a flow test. Refer to Do a
flow test on page 21.

23_FLOW WARNING – The oxygen flow through the sample out • Oxygen supply problem. The oxygen pressure
SO valve (MV5) decreased to less than the should be 400 mbar (±10 mbar) at 20 L/h MFC
FLOW WARNING setting during the flow. Select MAINTENANCE > DIAGNOSTICS >
pressure test. O2-CTRL STATUS.
Refer to MAINTENANCE > SYSTEM • Failure of or blockage in the sample out valve
CONFIGURATION > SEQUENCE • Blockage in the tube after MFC
PROGRAM > PRESSURE/FLOW TEST
• Failure of the MFC. Do a flow test. Refer to Do a
> FLOW WARNING.
flow test on page 21.

26_PRESSURE TEST The MFC flow did not decrease to less • The analyzer has a gas and/or liquid leak.
WARN than the PRESSURE TEST WARN
• A valve has a leak.
setting during the pressure test.
• Examine the sample out valve, sample (ARS)
Refer to MAINTENANCE > SYSTEM valve and analyzer fittings for leaks.
CONFIGURATION > SEQUENCE
• Examine the mixer reactor for leaks. Do a
PROGRAM > PRESSURE/FLOW TEST
pressure test. Refer to Do a pressure test
> PRESSURE TEST WARN.
on page 21.

28_NO PRESSURE The pressure test was not done during The analyzer was started with a quick startup. The
TEST the system startup sequence. RIGHT arrow key was pushed when START was
Note: The warning stays active until a selected.
pressure test is passed.

29_PRESSURE TEST The daily pressure test and flow test Set the pressure test and flow test functions to on in
OFF functions are set to off. the MAINTENANCE > SYSTEM CONFIGURATION >
SEQUENCE PROGRAM > PRESSURE/FLOW TEST
menu.
30_TOC SPAN CAL FAIL The result of the TIC or TOC span Make sure that the concentration of the prepared
31_TIC SPAN CAL FAIL calibration is not within the TIC BAND or standard solution is correct. Make sure that the
TOC BAND setting. settings in the CALIBRATION > SPAN
Refer to MAINTENANCE > SYSTEM CALIBRATION menu are correct. Examine the
CONFIGURATION > SEQUENCE operation of the analyzer.
PROGRAM > SPAN PROGRAM > TIC
BAND or TOC BAND.
33_TOC SPAN CHCK The result of the TIC or TOC span check
FAIL is not within the TIC BAND or TOC BAND
34_ TIC SPAN CHCK setting.
FAIL Refer to MAINTENANCE > SYSTEM
CONFIGURATION > SEQUENCE
PROGRAM > SPAN PROGRAM > TIC
BAND or TOC BAND.

14
 Troubleshooting

Table 4 System warnings (continued)

Message Description Cause and solution
42_ZERO CAL FAIL The zero calibration result is not within Examine the stability of the zero reactions and the
the ZERO BAND setting. Refer to quality of the reagents.
MAINTENANCE > SYSTEM Do a zero calibration. Refer to the Installation and
CONFIGURATION > SEQUENCE Operation Manual.
PROGRAM > ZERO PROGRAM > ZERO
BAND.
43_ ZERO CHCK FAIL The zero check result is not within the
ZERO BAND setting. Refer to
MAINTENANCE > SYSTEM
CONFIGURATION > SEQUENCE
PROGRAM > ZERO PROGRAM > ZERO
BAND.
50_TIC OVERFLOW The TIC reading at the end of the TIC Unusually high TIC reading. Look at the operation
analysis is more than the TIC CHECK ranges in OPERATION > SYSTEM RANGE DATA
setting. In addition the TIC reading is menu. Change the operation range (e.g., from 1 to 2)
more than the TIC CHECK setting after in the MAINTENANCE > COMMISSIONING >
the TIC sparge time was increased STREAM PROGRAM menu to decrease the sample
300 seconds. volume added to the reactor.
Refer to MAINTENANCE > SYSTEM Increase the TIC SPARGE TIME setting. Refer to
CONFIGURATION > REACTION CHECK MAINTENANCE > SYSTEM CONFIGURATION >
> TIC CHECK. OXIDATION PROGRAM 1 > TIC SPARGE TIME.
51_TOC OVERFLOW The TOC reading at the end of the TIC
Unusually high TOC reading. Look at the operation
analysis is more than the TOC CHECK
ranges in OPERATION > SYSTEM RANGE DATA
setting, even after the TOC sparge time
menu. Change the operation range (e.g., from 1 to 2)
was increased 300 seconds. in the MAINTENANCE > COMMISSIONING >
Refer to MAINTENANCE > SYSTEM STREAM PROGRAM menu to decrease the sample
CONFIGURATION > REACTION CHECK volume added to the reactor.
> TOC CHECK. Increase the TOC SPARGE TIME setting. Refer to
MAINTENANCE > SYSTEM CONFIGURATION >
OXIDATION PROGRAM 1 > TOC SPARGE TIME.
52_HIGH CO2 IN BASE The CO2 level in the base reagent is Make sure that the CO2 filter on the base reagent
more than the BASE CO2 ALARM container is in good condition. Make sure that the
setting. base reagent container has no air leak. Identify the
Refer to MAINTENANCE > SYSTEM quality of the base reagent. Replace the base
CONFIGURATION > FAULT SETUP > reagent.
BASE CO2 ALARM.
Note: The CO2 level in the base reagent is
identified during a zero calibration or zero
check.

53_TEMPERATURE The analyzer temperature is more than Identify the internal analyzer temperature. Examine
ALARM the TEMPERATURE ALARM setting. the filters in the fan and the vent. Examine the
Refer to MAINTENANCE > SYSTEM operation of the fan.
Note: At temperatures below 25 °C (77 °F), the analyzer
CONFIGURATION > FAULT SETUP >
sets the fan to off.
TEMPERATURE ALARM.
Note: The analyzer fan operates in backup
mode until the warning is acknowledged.

54_COOLER LOW TEMP The cooler temperature is less than 2 °C Look at the flashing LED 3 on the signal board to
for more than 600 seconds. examine the operation of the cooler. The operation of
the temperature sensor is incorrect. Replace the
cooler.

15
Troubleshooting

Table 4 System warnings (continued)

Message Description Cause and solution
55_COOLER HIGH The cooler temperature is 5 °C (9 °F) Look at the flashing LED 3 on the signal board to
TEMP more than the cooler setpoint examine the operation of the cooler. The operation of
temperature and more than 8 °C (14 °F) the temperature sensor or cooler peltier element is
below the ambient temperature for more incorrect. Identify if the current received by the peltier
than 600 seconds. element is approximately 1.4 A. If not, replace the
cooler.
For more tests, refer to the information sheet T022.
BioTector Cooler Troubleshooting.
62_SMPL PUMP STOP The sample pump stopped with its Examine the rotation of the sample pump.
ON rotation sensor set to on or the operation Replace Relay 2 on the relay board.
of the rotation sensor is incorrect
Examine the pump sensor signal. Look at LED 15 on
(continuously on).
the signal board and DI04 in the DIGITAL INPUT
ON = LED 15 is on (signal board) menu. Refer to MAINTENANCE > DIAGNOSTICS >
63_SMPL PUMP STOP The sample pump stopped with its INPUT/OUTPUT STATUS > DIGITAL INPUT.
OFF rotation sensor set to off or the operation Replace the sample pump. Refer to Replacement
of the rotation sensor is incorrect (no parts and accessories on page 37
rotation sensed). For more tests, refer to the information sheet TT001.
OFF = LED 15 is off (signal board) BioTector Sample Pump Stop On and Off
Warning_Quick Troubleshooting.
64_ACID PUMP STOP The acid pump stopped with its rotation Examine the rotation of the acid pump.
ON sensor on or the operation of the rotation Examine the pump sensor signal. Look at LED 16 on
sensor is incorrect (continuously on). the signal board and DI05 in the DIGITAL INPUT
ON = LED 16 is on (signal board) menu. Refer to MAINTENANCE > DIAGNOSTICS >
INPUT/OUTPUT STATUS > DIGITAL INPUT.
65_ACID PUMP STOP The acid pump stopped with its rotation Replace the pump.
OFF sensor off or the operation of the rotation
sensor is incorrect (no rotation sensed).
OFF = LED 16 is off (signal board)
66_BASE PUMP STOP The base pump stopped with its rotation Examine the rotation of the base pump.
ON sensor on or the operation of the rotation Examine the pump sensor signal. Look at LED 17 on
sensor is incorrect (continuously on). the signal board and DI06 in the DIGITAL INPUT
ON = LED 17 is on (signal board) menu. Refer to MAINTENANCE > DIAGNOSTICS >
INPUT/OUTPUT STATUS > DIGITAL INPUT.
67_BASE PUMP STOP The base pump stopped with its rotation Replace the pump.
OFF sensor off or the operation of the rotation
sensor is incorrect (no rotation sensed).
OFF = LED 17 is off (signal board)
81_ATM PRESSURE The reading of the atmospheric pressure Examine ADC[8] in the ANALOG INPUT menu. Refer
HIGH sensor is more than 115 kPa. The to MAINTENANCE > DIAGNOSTICS >
atmospheric pressure sensor reading is INPUT/OUTPUT STATUS > ANALOG INPUT. The
set to 101.3 kPa (fault operation mode). reading should be approximately 4 V.
82_ATM PRESSURE The reading of the atmospheric pressure The operation of the pressure sensor is incorrect.
LOW sensor is less than 60 kPa. The Replace the motherboard. Refer to Replacement
atmospheric pressure sensor reading is parts and accessories on page 37
set to 101.3 kPa (fault operation mode).
83_SERVICE TIME Service is necessary (200 day interval) Complete the necessary service tasks. Then, reset
the service counter to acknowledge the warning.
Select MAINTENANCE > DIAGNOSTICS >
SERVICE > RESET SERVICE COUNTER.
84_SAMPLER ERROR There is no/low sample or low air Examine the LCD screen of the sampler for more
pressure/vacuum in the sampler. information. Refer to the sampler user manual.

16
 Troubleshooting

Table 4 System warnings (continued)

Message Description Cause and solution
88_O2 CONTROLLER There is a communication problem Make sure that LED 2 (L2) on the O2 Controller Board
WARN between the motherboard and the O2 is on.
Controller Board. Examine the 24 VDC power on the O2 Controller
board at terminal J6.
Examine the ribbon cable connections on the board.
Removed and then apply power to the analyzer.
Replace the O2 Controller Board if necessary. Refer
to Replacement parts and accessories on page 37.
89_TC SPAN CAL FAIL The TC span calibration result is not Examine the concentration of the standard solution.
within the TC BAND setting. Examine the SPAN CALIBRATION settings.
90_TC SPAN CHCK FAIL The TC span check result is not within the
TC BAND setting.
91_TC OVERFLOW The TC readings are high even after the Examine the operation ranges in the SYSTEM
TC time was extended to the maximum RANGE DATA menu.
time of 300 seconds. Increase the operation range to decrease the sample
volume.
Increase the TC SPARGE TIME in SYSTEM
PROGRAM > SYSTEM PROGRAM 1.
92_HI AIR PRESSURE 2 The air pressure supply was more than The external air regulator is not operating correctly.
2.0 bar for more than 5 seconds. When Decrease the external air supply pressure to 1.5 bar
the oxygen concentrator is on, the air when the oxygen concentrator is not in operation.
pressure supply is normally between
When the problem is fixed, acknowledge the warning
0.9 bar to 1.5 bar. If the air pressure does
to reset the O2 Controller Board.
not decrease to normal values, the air
supply is isolated from the analyzer and
oxygen is not made.
93_HI AIR PRESSURE 1 The air pressure supply was more than The external air regulator is not operating correctly.
1.8 bar for more than 60 seconds. When Stop the analyzer. Decrease the external air supply
the oxygen concentrator is on, the air pressure to 1.5 bar when the oxygen concentrator is
pressure supply is normally between not in operation.
0.9 bar to 1.5 bar.
When the problem is fixed, acknowledge the warning
to reset the O2 Controller Board.
94_LO AIR PRESSURE The air pressure supply was less than The external air regulator is not operating correctly.
2 0.6 bar for more than 5 seconds. When Increase the external air supply pressure to 1.5 bar
the oxygen concentrator is on, the air when the oxygen concentrator is not in operation.
pressure supply is normally between
When the problem is fixed, acknowledge the warning
0.9 bar to 1.5 bar. If the air pressure does
to reset the O2 Controller Board.
not increase to normal values, the air
supply is isolated from the analyzer and
oxygen is not made.
95_LO AIR PRESSURE The air pressure supply was less than The external air regulator is not operating correctly.
1 0.8 bar for more than 60 seconds. When Stop the analyzer. Increase the external air supply
the oxygen concentrator is on, the air pressure to 1.5 bar when the oxygen concentrator is
pressure supply is normally between not in operation.
0.9 bar to 1.5 bar.
When the problem is fixed, acknowledge the warning
to reset the O2 Controller Board.

17
Troubleshooting

Table 4 System warnings (continued)

Message Description Cause and solution
96_HI O2 PRESSURE 2 The oxygen pressure supply was more Select MAINTENANCE > DIAGNOSTICS > O2-CTRL
than 500 mbar for more than 5 seconds. STATUS. Use the oxygen pressure regulator to
If the oxygen pressure does not decrease decrease the oxygen pressure to 400 mbar
to normal values, the air supply is isolated (±10 mbar) at 20 L/h MFC flow. When the problem is
from the analyzer and oxygen is not fixed, acknowledge the warning to reset the O2
made. Controller Board.
97_HI O2 PRESSURE 1 The oxygen pressure supply was more Select MAINTENANCE > DIAGNOSTICS > O2-CTRL
than 450 mbar for more than 60 seconds. STATUS. Use the oxygen pressure regulator to
If the oxygen pressure does not decrease decrease the oxygen pressure to 400 mbar
to normal values, the air supply is isolated (±10 mbar) at 20 L/h MFC flow.
from the analyzer and oxygen is not
made.
98_LO O2 PRESSURE 2 The oxygen pressure supply was less Select MAINTENANCE > DIAGNOSTICS > O2-CTRL
than 150 mbar for more than 5 seconds. STATUS. Use the oxygen pressure regulator to
If the oxygen pressure does not increase increase the oxygen pressure to 400 mbar
to normal values, the air supply is isolated (±10 mbar) at 20 L/h MFC flow. When the problem is
from the analyzer and oxygen is not fixed, acknowledge the warning to reset the O2
made. Controller Board.
99_LO O2 PRESSURE 1 The oxygen pressure supply was less Select MAINTENANCE > DIAGNOSTICS > O2-CTRL
than 200 mbar for more than 60 seconds. STATUS. Use the oxygen pressure regulator to
If the oxygen pressure does not decrease increase the oxygen pressure to 400 mbar
to normal values, the air supply is isolated (±10 mbar) at 20 L/h MFC flow.
from the analyzer and oxygen is not
made.
100_ROTARY V The rotary valve stopped with the rotation Select MAINTENANCE > DIAGNOSTICS >
STOP:ON sensor on (sensor signal 1). The sensor it SIMULATE > MFC. Set the MFC to 20 L/h. Examine
not operating correctly because it always the rotation of the rotary valve. Select
shows on (sensor signal 1). MAINTENANCE > DIAGNOSTICS > O2-CTRL
STATUS. Look at the rotary valve signals (1 = on, 0 =
101_ROTARY V The rotary valve stopped with the rotation off) as the valve rotates.
STOP:OFF sensor off (sensor signal 0). The sensor it
not operating correctly because it always Replace the rotary valve for the oxygen concentrator.
shows off (sensor signal 0). Refer to Replacement parts and accessories
on page 37.
When the warning is gone, the green LED (Stepper)
on the Oxygen PCB is on.
114_I/O WARNING Changes in the Input/Output bus extender When the analyzer senses a difference between the
MCP23S17 chips were identified during requested and the read configuration registers
the periodic checks done automatically. values, all of the devices on the SPI (serial peripheral
The Input/Output bus extender interface) bus are reset and re-initialized
MCP23S17 chips have read/write control automatically. Select OPERATION > FAULT
registers. ARCHIVE. Acknowledge the warning and tell
Note: The Input/Output bus extender technical support.
MCP23S17 chips have read/write control
registers.

128_REACT PURGE The gas flow is not normal. There is an • Blockage in the mixer reactor, the sample out
WARN instrument air or oxygen supply problem. valve or the sample out tubing and fittings
• Blockage in the tube after MFC
• Failure of the MFC

Select MAINTENANCE > DIAGNOSTICS > O2-CTRL

STATUS. The oxygen pressure is normally 400 mbar
(±10 mbar) at 20 L/h MFC flow.
Do a flow test. Refer to Do a flow test on page 21.

18
 Troubleshooting

Table 4 System warnings (continued)

Message Description Cause and solution
133_BACKUP BAT LOW The voltage of the cell/coin backup Replace the cell/coin backup battery on the
battery on the motherboard is less than motherboard. Refer to Replacement parts and
2.6 V. accessories on page 37.
135_MODBUS WARN Internal Modbus tasks are in an unknown When this warning occurs, the Modbus circuit starts
condition. again automatically. Acknowledge the warning and
tell the distributor or the manufacturer. If the warning
continues, replace the motherboard. Refer to
Replacement parts and accessories on page 37.

2.3 Notifications
Select OPERATION > FAULT ARCHIVE to see the notifications. When "SYSTEM NOTE"
shows in the top-left corner of the Reaction Data screen or the Reagent Status screen, a
notification has occurred. Refer to Table 5.
Table 5 Notifications
Message Description Solution
85_LOW REAGENTS The calculated reagent levels identify Replace the reagents. Refer to Fill or replace the reagents
(can be set as a warning that the reagent containers are at a on page 6.
or note) low level. To increase the number of days before a LOW
REAGENTS notification occurs, select MAINTENANCE >
COMMISSIONING > REAGENTS MONITOR > LOW
REAGENTS AT.
86_POWER UP Power was supplied to the analyzer This notification is automatically acknowledged. No action
or a power reboot was done after the is necessary.
processor watchdog timeout.
87_SERVICE TIME The service counter has been set to This notification is automatically acknowledged. No action
RESET 200 days (default). is necessary.
RESET SERVICE COUNTER was
selected.
116_LOW/NO SAMPLE 1 The sample sensor does not sense Examine the sample liquid level and the sampling system
117_LOW/NO SAMPLE 2 sample or the sample quantity is less for each sample source.
118_LOW/NO SAMPLE 3 than the limit for the sample source Select MAINTENANCE > DIAGNOSTICS > SIMULATE >
(default: 75%). SAMPLE PUMP. Select PUMP FORWARD TEST.
Examine the sample delivery and the sample bypass
tubing.
Identify if there are air bubbles in the sample tubing.
122_SAMPLE FAULT 1 An external device sent a sample Examine the external sample liquid level and sampling
123_SAMPLE FAULT 2 fault input signal to the analyzer. system for the sample channel.
124_SAMPLE FAULT 3 Examine the external sample monitoring device and the
external input signal wiring.

2.4 Show the status history before a fault

Show a short status history of some analyzer components before a fault occurs. The
default 0.0 value identifies that there are no faults for the component.

19
Troubleshooting

1. Select MAINTENANCE > SYSTEM CONFIGURATION > FAULT STATUS.

2. Select an option.
Option Description
O2 FLOW Shows 120 entries for the MFC (mass flow controller) setpoint value
(first column) and MFC flow value (second column). The entries are at
1 second intervals. If a fault occurs, the entries are kept in the
O2 FLOW fault archive until a new fault occurs.
RELAY PCB FAULT Shows 120 readings of the input to terminal S41 FLT on the signal
board. If a fault occurs, the number logged is “1”. The readings are
kept in the RELAY PCB FAULT archive until a new fault occurs. Use
the readings to identify if the fault was an sudden fault or an
intermittent fault.
OZONE PCB Shows 120 readings of the input to terminal S42 FLT O3 on the signal
FAULT board. If a fault occurs, the number logged is “1”. The readings are
kept in the OZONE PCB FAULT archive until a new fault occurs. Use
the readings to identify if the fault was an sudden fault or an
intermittent fault.
CO2 ANALYZER Shows 120 readings of the input to terminal S11, which is the 4–20 mA
FAULT signal from the CO2 analyzer on the signal board. The readings are at
2 second intervals (4 minutes total). If a fault occurs, the readings are
kept in the CO2 ANALYZER FAULT archive until a new fault occurs.
BIOTECTOR Shows 120 readings of the analyzer temperature. The readings are at
TEMPERATURE 2 seconds intervals (4 minutes total). If a fault occurs, the readings are
kept in the BIOTECTOR TEMPERATURE fault archive until a new fault
occurs.
COOLER Shows 120 readings of the cooler temperature. The readings are at
TEMPERATURE 10 seconds intervals (20 minutes total). If a fault occurs, the reading
are kept in the COOLER TEMPERATURE fault archive until a new
fault occurs.

20
Section 3 Diagnostics

3.1 Do a pressure test

Do a pressure test to identify if there is a gas leak in the analyzer.

1. Select MAINTENANCE > DIAGNOSTICS > PROCESS TEST > PRESSURE TEST.
2. Select PRESSURE TEST, then push .
A pressure test starts (60 seconds). The information that follows shows.
Item Description
TIME Shows the remaining time for the test.
MFC Shows the mass flow controller (MFC) setting for the test (default: 40 L/hr).
SETPOINT
MFC FLOW Shows the flow from the MFC. If there is no gas leak, the flow will slowly
decrease to near 0 L/hr after 25 seconds.
STATUS Shows the results of the test.
TESTING—Test in progress
PASS—The flow from the MFC at the end of the test is less than 4 L/hr
(default).
WARNING—The flow from the MFC at the end of the test is more than
4 L/hr but less than 6 L/hr (default).
FAIL—The flow from the MFC at the end of the test is more than 6 L/hr
(default).
Note: To change the default limits for the test, select MAINTENANCE >
SYSTEM CONFIGURATION > SEQUENCE PROGRAM >
PRESSURE/FLOW TEST.

3. If the pressure test fails, select PRESSURIZE REACTOR, then push to find the
location of a leak. A longer test starts (999 seconds).

3.2 Do a flow test

Do a flow test to identify if there is blockage in the gas exhaust or the sample out lines.

1. Select MAINTENANCE > DIAGNOSTICS > PROCESS TEST > FLOW TEST.
2. Select EXHAUST TEST, then push .
A flow test starts (30 seconds). The information that follows shows.
Item Description
TIME Shows the remaining time for the test.
MFC Shows the mass flow controller (MFC) setting for the test (default: 80 L/hr).
SETPOINT
MFC FLOW Shows the flow from the MFC. If there is no blockage, the flow is
approximately 80 L/hr.
STATUS Shows the results of the test.
TESTING—Test in progress
PASS—The flow from the MFC at the end of the test is more than 72 L/hr
(default).
WARNING—The flow from the MFC at the end of the test is less than
72 L/hr but more than 40 L/hr (default).
FAIL—The flow from the MFC at the end of the test is less than 40 L/hr
(default).
Note: To change the default limits for the test, select MAINTENANCE >
SYSTEM CONFIGURATION > SEQUENCE PROGRAM >
PRESSURE/FLOW TEST.

21
Diagnostics

3. If the exhaust test fails, select EXHAUST FLOW, then push to find the location of
the blockage (e.g., at the exhaust valve). A longer test starts (999 seconds).
4. Select SAMPLE OUT TEST, then push .
A sample out test is started. The test identifies if there is a blockage sample out lines.
5. If the sample out test fails, select SAMPLE OUT FLOW, then push to find the
location of the blockage (e.g., at the sample out valve). A longer test starts
(999 seconds).

3.3 Do an ozone test

Do an ozone test to identify if the operation of the ozone generator is correct.

1. Install the ozone tester in the analyzer. Refer to information sheet T029. Procedure to
check the ozone level in a BioTector B3500 and B7000 using a universal ozone
tester..
2. Select MAINTENANCE > DIAGNOSTICS > PROCESS TEST > OZONE TEST.
3. Select START TEST.
The analyzer does a pressure test. Then the ozone generator is set to on. An ozone
warning message shows on the display.
4. When the O-ring in the tester breaks, select STOP TEST.
The analyzer removes all of the ozone from the ozone tester (30 seconds). The test
results show on the display.
Item Description
TIME Shows the time for the O-ring to break.
STATUS Shows the results of the test.
TESTING—Test in progress
PASS—The time to break the O-ring was less than 18 seconds (default).
LOW OZONE—The time to break the O-ring was more than 18 seconds but less
than 60 seconds (default).
FAIL—The time to break the O-ring was more than 60 seconds.
Note: To change the default limits for the test, select MAINTENANCE > SYSTEM
CONFIGURATION > FAULT SETUP > OZONE TEST TIME.

3.4 Do a sample pump test

Do a sample pump test to identify the correct forward and reverse times for the sample
pump for each sample stream.

1. Select MAINTENANCE > DIAGNOSTICS > PROCESS TEST > SAMPLE PUMP
TEST.
2. Select an option.
Option Description
VALVE Sets the SAMPLE or MANUAL fitting used for the test. For example, to
select the SAMPLE 1 fitting, select STREAM VALVE 1.

22
 Diagnostics

Option Description
PUMP Starts the sample pump in the forward direction.
FORWARD Note: First select PUMP REVERSE TEST to empty the sample lines, then
TEST select PUMP FORWARD TEST.
1. Push to stop the timer when the sample is through the sample
(ARS) valve and the sample drips into the drain pipe on the side of the
analyzer.
2. Record the time on the display. The time is the correct forward time for
the selected stream.

PUMP Starts the sample pump in the reverse direction.

REVERSE
TEST 1. Push to stop the timer when the sample lines and the oxidized
sample catch-pot/cleaning vessel are empty.
2. Record the time on the display. The time is the correct reverse time for
the sample pump.

SAMPLE Goes to the MAINTENANCE > COMMISSIONING > SAMPLE PUMP menu
PUMP to set the forward and reverse times for each sample stream.

3.5 Do a pH test

CAUTION
Chemical exposure hazard. Obey laboratory safety procedures and wear all of the
personal protective equipment appropriate to the chemicals that are handled. Refer to
the current safety data sheets (MSDS/SDS) for safety protocols.

CAUTION
Chemical exposure hazard. Dispose of chemicals and wastes in accordance with local,
regional and national regulations.

Do a pH test to identify if the pH of the solution in the reactor is correct at the different
steps of a reaction.
Items to collect:
• pH paper
• Glass beaker
• Personal protective equipment (refer to MSDS/SDS)

1. Put on the personal protective equipment identified in the safety data sheet
(MSDS/SDS).
2. Select MAINTENANCE > DIAGNOSTICS > PROCESS TEST > pH TEST.
3. Select RANGE,VALVE.
4. Set the operation range (e.g., 1) and the stream (e.g., STREAM 1) to use for the test.
Refer to the OPERATION > SYSTEM RANGE DATA screen to see the operation
ranges. Select the operation range that agrees with normal measurements for the
sample stream.
5. Select MODE.
6. Select the test mode (e.g., TIC+TOC or TC).
7. Select START TEST.
8. Push again to confirm that the previous reaction completed normally.

23
Diagnostics

The analyzer does the items that follow in sequence:

• A normal startup completes in approximately 210 seconds (ozone purge, reactor
purge, pressure test and flow test).
• Adds the sample and TIC acid to the reactor. Then the program pauses so the
TIC pH can be measured by the user.
• Adds the base reagent to the solution in the reactor. Then the program pauses so
the base pH can be measured by the user.
• Adds the TOC acid to the solution in the reactor. Then the program pauses so the
pH can be measured by the user.
• The reactor and CO2 analyzer purge phase is completed.
9. When "TEST TIC pH" shows on the display, select an option.
Option Description
TAKE SAMPLE Sets the sample out valve to on for 0.1 seconds.
Select TAKE SAMPLE four times to remove old sample from the sample
out line, then collect a sample in the glass beaker. Use a pH paper to
identify the pH of the sample. The expected pH shows on the display.
Note: The loss of volume in the reactor when a sample is collected can
have a negative effect on the pH of the samples collected at the next step.
For the best accuracy, collect only one sample during a pH test, then
complete the test. Start the pH test again and collect a sample at a
different step (e.g., TEST BASE pH).

CONTINUE TO The analyzer goes to the next step of the program.

NEXT PHASE
STOP TEST The analyzer goes to the last step of the program, reactor purge.
10. When "TEST BASE pH" shows on the display, select an option. The options are the
same as for the previous step.
11. When "TEST TOC pH" shows on the display, select an option. The options are the
same as for the previous step.
12. When "CONFIRM ALL TUBES RE-CONNECTED" shows, push to confirm.
The reactor and CO2 analyzer purge phase is done.

3.6 Do a sample valve test

Identify if the sample ball valve is aligned with the sample valve ports. Adjust the
alignment as necessary.

1. Select MAINTENANCE > DIAGNOSTICS > PROCESS TEST > SAMPLE VALVE
TEST.
2. Select TEST FIRST FAILURE to start the test.
The analyzer rotates the sample valve from sensor position 1, 2, then 3.
"COMPLETE" shows when the test is completed.
• LOOP COUNT —Shows the number of loops the sample ball valve is rotated for
each adjustment point for each sensor position during the test (default: 2).
• CURRENTLY TESTING —Shows the adjustment points (the time delay
implemented by the software) for each sensor during the test. The adjustment
points are from 0 to 15 with 1 point increments.
• FIRST FAILURE POINT —Shows the adjustment point at which the analyzer
does not detect the position of the valve.
3. Select ADJUST SAMPLE VALVE to set the sample valve stop position to align the
sample ball valve with the sample valve ports. Follow the instructions on the display.

24
 Diagnostics

The analyzer shows the position of the valve (e.g., SENS 1) when the adjustment
values are entered.
If a 17_SMPL VALVE NOT SYNC fault occurs, refer to the information sheets T018.
BioTector Sample Valve Not Synchronized Fault Troubleshooting after Valve
Replacement and TT002. BioTector Sample Valve Not Sync Fault Quick
Troubleshooting.
Note: When the sample valve is replaced, refer to the information sheet M046. Sample Valve
Adjustment and Sample Tube Positioning Guidelines.

3.7 Do simulations
Do simulations to identify if a component (e.g., pumps, valves and mass flow controller)
operation is correct.
Note: Each time a component is activated, the analyzer will stop the operation of other devices as
necessary to prevent damage to the analyzer.
When the back key is pushed to exit the menu, the analyzer does a pump
synchronization process.

1. Select MAINTENANCE > DIAGNOSTICS > SIMULATE.

The status of the analyzer components show.
2. Select an option.
When a component is on, an asterisk (*) shows before the component name on the
display.
Note: Changes made to settings in this menu are not saved.

Option Description
MFC Sets the mass flow controller (MFC) flow (e.g., 40 L/h). Set the flow.
Push to start the mass flow controller (MFC). The measured flow
shows at the top of the display.
Note: If the flow shown is 0.0 L/h, the MFC is off.

OZONE Sets the ozone generator to on or off.

GENERATOR Note: For safety, before the ozone generator is set to on, a pressure
test is done. If a gas leak is found, the ozone generator is not set to
on.

ACID PUMP Sets the acid pump to on or off. Sets the number of pulses (½
revolution).
When the pump is in operation, the actual pulse time (external
brackets) and the set pulse time (internal brackets) show.
ACID VALVE Sets the acid valve to on or off.
BASE PUMP Sets the base pump to on or off. Sets the number of pulses (½
revolution).
When the pump is in operation, the actual pulse time (external
brackets) and the set pulse time (internal brackets) show.
PH ADJUST VALVE Sets the pH adjust valve to on or off.
SAMPLE VALVE Sets the sample (ARS) valve to the selected position. Options:
SEN1 (sample pump to bypass), SEN2 (sample pump to reactor) or
SEN3 (acid or base to reactor).

25
Diagnostics

Option Description
SAMPLE PUMP Sets the sample pump to the selected operation mode. Options: FWD
(forward), REV (reverse), P-FWD (pulse control forward) or P-REV
(pulse control reverse).
If P-FWD or P-REV is selected, set the number of pulses (½
revolution of the pump roller).
When the pump is in operation, the actual pulse time (external
brackets) and the set pulse time (internal brackets) show.
INJECTION VALVE Sets the injection valve to on or off.
REACTOR MOTOR Sets the mixer reactor motor to on or off.
SAMPLE OUT Sets the sample out valve to on or off.
VALVE
EXHAUST VALVE Sets the exhaust valve to on or off.
CLEANING VALVE Sets the cleaning valve to on or off.
CALIBRATION Sets the zero or span calibration valve to on or off. Options: ZERO,
VALVE (optional) SPAN or OFF.
STREAM VALVE Sets a sample stream valve to on or off. Select the number of the
stream valve. Only one stream valve can be set to on at one time.
Note: The stream valves can be controlled from the programmable
relays or from the stream expansion (auxiliary) board.

MANUAL VALVE Sets a manual valve to on or off. Select the manual valve. Only one
manual valve can be set to on at one time.
COOLER Sets the cooler to on, off or automatic to identify if the cooler relay
operation is correct.
LEAK DETECTOR The LEAK DETECTOR option cannot be selected. The condition of
the Liquid Leak Detector alarm input shows on the display.
FAN Sets the fan to on, off or automatic to identify if the fan relay operation
is correct. The analyzer temperature shows on the display.
When FAN is set to AUTO, the analyzer sets the fan to off when the
analyzer temperature is less than 25 °C. The fan operates
continuously when the analyzer temperature is more than 25 °C.
TEMP SWITCH Sets the temperature switch to on, off or automatic to identify if the
temperature switch operation is correct.
When TEMP SWITCH is set to AUTO, the analyzer sets the
temperature switch to on when the analyzer temperature is 25 °C
(default) or higher. The temperature switch stays on until the analyzer
temperature is less than 25 °C.
SAMPLER FILL Sets the signal to fill the sampler to on or off. The signal stays on until
set to off.
SAMPLER EMPTY Sets the signal to make the sampler empty to on or off. The signal
stays on for 5 seconds.
SAMPLER ERROR Sets the signal for a sampler error to on or off. The sampler error
signal is normally sent from the sampler when there is an error in the
sampler.
SAMPLE SENSOR The SAMPLE SENSOR option cannot be selected. The condition of
the sample sensor shows on the display.
REACTOR PURGE Starts the reactor purge operation.

26
 Diagnostics

Option Description
RUN REAGENTS Starts the reagent prime operation, which fills the reagent tubing with
PURGE reagent.
INPUT/OUTPUT Goes to the MAINTENANCE > DIAGNOSTICS > INPUT/OUTPUT
STATUS STATUS menu. The INPUT/OUTPUT STATUS menu shows the
conditions of the digital inputs, digital outputs, analog inputs and
analog outputs.

3.8 Do a relay or 4–20 mA output test

Do a signal simulation to identify if the relay and 4–20 mA output operation is correct.

1. Select MAINTENANCE > DIAGNOSTICS > SIGNAL SIMULATE.

2. Select an option.
Option Description
ALARM 1 to 6 Sets the ALARM relay to on if configured.
CHANNEL 1 to 6 Sets a 4–20 mA output (e.g., CHANNEL 1) to a selected
4–20 mA signal.
CO2 ALARM 1 to 6 Sets the CO2 ALARM relay to on if configured.
STM ALARM 1 to 6 Sets a STM ALARM relay to on if configured.
SAMPLE FAULT 1 to 6 Sets the SAMPLE FAULT relay to on for a specified stream if
configured.
SYNC RELAY Sets the SYNC relay to on if configured.
SAMPLE STATUS 1 to 6 Sets the SAMPLE STATUS relay to on for a specified stream if
configured.
CAL SIGNAL Sets the CAL SIGNAL relay to on if configured.
MAINT SIGNAL Sets the MAINT SIGNAL relay to on if configured.
REMOTE STANDBY Sets the REMOTE STANDBY relay to on if configured.
STOP Sets the STOP relay to on if configured.
FAULT Sets the FAULT relay to on if configured.
FAULT OR WARN Sets the FAULT OR WARN relay to on if configured.
WARNING Sets the WARNING relay to on if configured.
NOTE Sets the NOTE relay to on if configured.
MAN MODE TRIG Sets the MAN MODE TRIG relay to on if configured.
4-20mA CHNG Sets the 4-20mA CHNG relay to on if configured.
4-20mA CHNG 1 to 6 Sets a 4-20mA CHNG1 to 6 relay to on for a specified stream if
configured.
4-20mA READ Sets the 4-20mA READ relay to on if configured.
INPUT/OUTPUT STATUS Goes to the MAINTENANCE > DIAGNOSTICS >
INPUT/OUTPUT STATUS menu. The INPUT/OUTPUT STATUS
menu shows the conditions of the digital inputs, digital outputs,
analog inputs and analog outputs.

3.9 Show the input and output status

Show the signals at the digital inputs, digital outputs, analog inputs and analog outputs to
examine their operation.

27
Diagnostics

1. Select MAINTENANCE > DIAGNOSTICS > INPUT/OUTPUT STATUS.

2. Select an option.
Option Description
DIGITAL Shows the digital signal at the digital inputs (1 = active, 0 = not active). "DI"
INPUT followed by two digits identifies the digital inputs. For example, DI09 is Digital
Input 9.
The digital input number is followed by the digital signal at the input and then
the function. "[PROGRAMMABLE]" identifies the configurable digital inputs.
Note: DI09 is the enter key. Push and hold down the enter key to change the
digital signal at DI09 to 1.

DIGITAL Shows the digital signal at the digital outputs (1 = active, 0 = not active). "DO"
OUTPUT followed by two digits identifies the digital outputs. For example, DO21 is Digital
Output 21.
The digital output number is followed by the digital signal at the output and then
the function. "[PROGRAMMABLE]" identifies the configurable digital outputs.
Note: When the analyzer is set to on, all of the digital outputs are set to 0.
Note: DO21 has a digital signal of 1 when the cooler is on and 0 when the
cooler is off. The cooler operates for approximately 3 seconds and then is off
for 7 seconds.

ANALOG Shows the ADC converter digital value, input voltage and function of each
INPUT analog input. The analyzer uses a 12-bit ADC, so the range of the digital value
is 0 to 4095. The input voltage range is 0 to 5.00 V.
ANALOG Shows the DAC converter digital value, output voltage and function of each
OUTPUT analog output. The analyzer uses a 12-bit DAC, so the range of the digital value
is 0 to 4095. The output voltage range is 0 to 10.00 V.

3.10 Show the oxygen controller status

Show the system air supply, oxygen supply, gas flow, pressure and temperature
parameters.

1. Select MAINTENANCE > DIAGNOSTICS.

2. Select O2-CTRL STATUS.
The oxygen concentrator is set to on. The information that follows shows on the
display:
• IDENTIFICATION —The identification number for the oxygen controller board.
• VERSION —The software version of the oxygen controller board.
• MODE —Sets the mode of the oxygen controller board. The modes follow:
MFC: The oxygen controller board operates the mass flow controller.
O2: The oxygen controller board operates the oxygen concentrator.
MFC AND O2: The oxygen controller board operates the MFC and oxygen
concentrator.
• TEMPERATURE SENSOR —The first value is the temperature of the analyzer at
the oxygen controller board. The second value is the voltage reading from the
temperature sensor.
• AIR PRESS SENSOR —The first value is the air inlet pressure for the oxygen
concentrator. The second value is the voltage reading from the air pressure
sensor.
• O2 PRESS SENSOR — The first value is the oxygen inlet pressure for the MFC
(normally 400 mbar (±10 mbar) at 20 L/h MFC setpoint. The second value is the
voltage reading from the oxygen pressure sensor.

28
 Diagnostics

• VALVE1, 2, 3—The oxygen controller valve outputs for Valves 1, 2 and 3 (1 = on,
0 = off). Valve 1 is the air isolation valve. Valve 2 and 3 are reserved.
• ROTARY VALVE —The operation of the rotary valve (FORWARD, REVERSE or
STOP).
Note: Approximately September 2022, the rotary valve was removed from the analyzer.
• ROTARY VALVE SENSOR —The sensor position of the rotary valve (1 = rotary
valve is on the sensor, 0 = the valve is not on the sensor).
Note: Approximately September 2022, the rotary valve sensor was removed from the
analyzer.
• MFC SETPOINT —Sets the setpoint for the mass flow controller. Push enter
(checkmark icon), select the setpoint, then push enter again. The MFC flow
shows at the top of the display. The MFC is off when the flow is 0.0 L/h.
• MFC FLOW —The first value is the MFC flow. The second value is the voltage
reading from the MFC. When the analyzer is stopped or in remote standby, the
MFC setpoint is 1 L/h.

3.11 Show the Modbus status

1. Select MAINTENANCE > DIAGNOSTICS > MODBUS STATUS.
2. Select an option.
Option Description
MODE Shows the Modbus operating mode, which is BIOTECTOR.
DEVICE BUS ADDRESS Shows the Modbus address of the instrument.
BUS MESSAGE COUNT Shows the number of Modbus messages that were correctly
received and were sent to the Modbus address of the
instrument.
Note: When the count is 65,535, the subsequent message
received sets the count to 1.

BUS COM ERROR Shows the number of corrupted or not fully received Modbus
COUNT messages that the Modbus received.
Note: When the count is 65,535, the subsequent message
received sets the count to 1.

MANUFACTURE ID Shows the manufacturer ID for the instrument (e.g., 1 for Hach).
DEVICE ID Shows the class or family of the instrument, if entered (default:
1234).
SERIAL NUMBER Shows the serial number of the instrument.
LOCATION TAG Shows the location of the instrument.
FIRMWARE REV Shows the firmware revision installed on the instrument.
REGISTERS MAP REV Shows the Modbus register map version used by the
instrument. Refer to the Modbus register maps in the Advanced
Configuration Manual.

After the menu options, the first 17 bytes of the last received (RX) and transmitted (TX)
Modbus message show.

3.12 Modbus troubleshooting

1. Make sure that the device bus address is correct. Refer to the Configure the Modbus
settings in the Installation and Operations Manual.
2. Make sure that the register address (5-digit code) is correct.

29
Diagnostics

3. Select MAINTENANCE > DIAGNOSTICS > MODBUS STATUS > BUS COM ERROR
COUNT. Look at the bus transmission error count.
The bus error count should increase each time the analyzer reads an invalid or not
fully received Modbus message.
Note: Valid messages that are not addressed to the instrument do not increase the counter.
4. For the Modbus RTU option, make sure that the wire connected to terminal D+ is
positively biased compared to the wire connected to terminal D– when the bus is in
an idle condition.
5. Make sure that there is a jumper installed on J15 of the motherboard at the end of the
bus to terminate the bus. The motherboard is in the electronic enclosure on the door
behind the stainless steel cover.
6. For the Modbus TCP option, open the web interface. Refer to Configure the Modbus
TCP/IP module in the Installation and Operation Manual. If the web interface does not
open, do the steps that follow:
a. Make sure that the network settings are correct.
b. Make sure that the Ethernet cable connectors are fully installed in the Ethernet
ports.
c. Make sure that the LED for the Modbus TCP/IP (RJ45) connector is green.

30
Section 4 Analysis enclosure
Approximately September 2022, the oxygen concentrator parts changed.
Figure 2 shows the pumps and components in the analysis enclosure after the change.
Figure 3 shows the valves in the analysis enclosure after the change.
Figure 4 shows the pumps and components in the analysis enclosure before the change.
Figure 5 shows the valves in the analysis enclosure before the change.
Figure 2 Analysis enclosure—Pumps and components

1 Mixer reactor 8 CO2 analyzer

2 Cable ties (2x) 9 Oxidized sample catch-pot (OSCP)
3 Molecular sieve bed 10 Base pump, P4
4 Oxygen pressure regulator 11 Acid pump, P3
5 Cooler 12 Sample pump, P1
6 Ozone generator 13 Liquid leak detector
7 Ozone destructor

31
Analysis enclosure

Figure 3 Analysis enclosure—Valves

1 Exhaust filter 7 Air isolation valve, OV1

2 Acid valve, MV6 8 Exhaust valve, MV1
3 Sample (ARS) valve, MV4 9 Injection valve, MV7
4 Non-return valve (check valve) 10 Cleaning valve
5 Valves for oxygen concentrator 11 Manual/Calibration valve (span calibration valve), MV9
6 Pressure relief valve, OV1 12 Sample out valve, MV5

32
 Analysis enclosure

Figure 4 Analysis enclosure—Pumps and components (before September 2022)

1 Mixer reactor 7 CO2 analyzer

2 Molecular sieve bed 8 Oxidized sample catch-pot (OSCP)
3 Oxygen pressure regulator 9 Base pump, P4
4 Cooler 10 Acid pump, P3
5 Ozone generator 11 Sample pump, P1
6 Ozone destructor 12 Liquid leak detector

33
Analysis enclosure

Figure 5 Analysis enclosure—Valves (before September 2022)

1 Acid valve, MV6 7 Air isolation valve, OV1

2 Sample (ARS) valve, MV4 8 Exhaust valve, MV1
3 Non-return valve (check valve) 9 Injection valve, MV7
4 Rotary valve, OV2 10 Cleaning valve
5 Exhaust filter 11 Manual/Calibration valve (span calibration valve), MV9
6 Pressure relief valve, OV1 12 Sample out valve, MV5

34
Section 5 Control enclosure components
Figure 6 Control enclosure components

1 Power supply, for main board/motherboard 9 Relay PCB

2 Power supply, for pumps and valves 10 Auxiliary/stream expansion PCB (optional)
3 Mains power PCB (printed circuit board) 11 Mass flow controller
4 Main power switch 12 Oxygen Controller Board
5 Motherboard 13 Safety board for ozone generator
6 LCD screen brightness access hole 14 4-20 mA isolators
7 SD/MMC card slot 15 Fan
8 Signal PCB

35
Control enclosure components

Figure 7 Motherboard components

1 Motherboard 2 Battery (Varta, CR2430, Lithium, 3V, 285mAh)

36
Section 6 Replacement parts and accessories

WARNING
Personal injury hazard. Use of non-approved parts may cause personal injury, damage
to the instrument or equipment malfunction. The replacement parts in this section are
approved by the manufacturer.

Note: Product and Article numbers may vary for some selling regions. Contact the appropriate
distributor or refer to the company website for contact information.
Consumables

Description Quantity Item no.

20 L
Acid reagent, 1.8 N Sulfuric Acid containing 80mg/L Manganese Sulfate Monohydrate 25255061
(5.2 gallons)
20 L
Base reagent, 1.2 N Sodium Hydroxide 2985562
(5.2 gallons)
Deionized water 4 L (1 gallon) 27256
TOC standard, 50.0 mg/L 4L 5847200
TOC standard, 100 mg/L 1L LCW843
TOC standard, 200 mg/L 1L LCW845
TOC standard, 250 mg/L 1L LCW848
TOC standard, 500 mg/L 1L LCW846
TOC standard, 500 mg/L 4L 5847300
TOC standard, 1000 mg/L 4L 5846900
TOC standard, 5000 mg/L 4L 5847400

Oxygen concentrator replacement parts

Refer to Figure 2 on page 31 and Figure 3 on page 32 to identify the oxygen concentrator
parts.
Quantity to
Description Item no.
stock
Oxygen concentrator, pressure relief valve 0 10-NOR-025
Oxygen concentrator, pressure regulator 0 10-DVB-012
Oxygen concentrator, full assembly, includes:
1 10-NID-001
Sieve beds, valves and fittings

Oxygen concentrator replacement parts (before September 2022)

Refer to Figure 4 on page 33 and Figure 5 on page 34 to identify the oxygen concentrator
parts.
Quantity to
Description Item no.
stock
Exhaust filter/muffler 1 10-DVB-005
Oxygen concentrator, molecular sieve beds (2) 1 12-DVB-013
Oxygen concentrator, pressure relief valve 0 10-DVB-024
Oxygen concentrator, pressure regulator 0 10-DVB-012
Oxygen concentrator, rotary valve 1 20-B5C-011

37
Replacement parts and accessories

Replacement parts
Quantity to
Description2 Item no.
stock
6-month maintenance kit, B7000i TOC analyzer 1 19-KIT-131
Air isolation valve, N/C 0 19-B5C-012
Acid pump or base pump, SR25 0 19-ASF-004
ARM main board, Rev 9, includes:
0 19-PCB-053
processor and LCD
CO2 analyzer, Hastelloy, 0–15000 ppm 0 20-CO2-011
Cooler , B4M with glass bead filter 0 19-BAS-018
Instrument air filter pack, B5C 0 10-SMC-001
Filter pack elements for air supply, B5C 13 12-SMC-001
Isolation amplifier 1 10-KNK-001
Mass flow controller (MFC) 0 12-PCP-001
Mixer reactor motor, B4M, 24 VDC, complete with leak detection 1 19-BAS-015
Mixer reactor, B4M, PTFE, complete with 24 VDC motor 0 19-BAS-016
Mixer reactor, B4M, PTFE 0 19-BAS-017
Ozone destructor heater 0 10-HAW-001
Ozone generator module B7000i 0 20-OZN-003
Ozone tube subassembly (with PCBA) 0 20-OZN-002
Ozone tube subassembly (without PCBA) 0 20-OZN-006
Ozone PCBA 0 ZBA81204326
Oxidized sample catch-pot (OSCP), cleaning vessel, glassware, 50 mm 1 10-KBS-018
Oxygen control board, complete 0 20-PCB-136
Power board, 115 VAC analyzer, B7000 1 19-PCB-160
Power board, 230 VAC analyzer, B7000 1 19-PCB-250
PTFE diaphragm for mixer reactor 1 10-KNF-038
PTFE ferrule and PEEK locking ring set, 1 x 3/16-in. 5 10-EMT-136
PTFE ferrule and PEEK locking ring set, 1 x 1/4-in. 5 10-EMT-114
Sample pump, WMM60, B4M 13 19-MAX-104
Safety board holder assembly 0 20-OZN-001
Tubing, PFA, 3/16-in. OD x 1/8-inch ID, 1 m length 5 m length 10-SCA-002
Tubing, PFA, 1/4-in. OD x 4 mm ID, 1 m length 5 m length 10-SCA-003
Tubing, PFA, 1/4-in. OD x 1/8-in. ID (6.35-mm OD x 3.18-mm ID), 1 m length 5 m length 10-SCA-006
Tubing, PFA, 3/16-in. OD x 1/16-inch ID, 1 m length 1 m length 10-SCA-007
Tubing, EMPP 562, 6.4 mm OD x 3.2 mm ID, 1 m length 2 m length 10-REH-002

2 Consumables/wearing parts: EMPP tubing, Y tube fittings, filters for the fan and vent, FPM/FKM tubing in the
ozone generator, catalyst in the ozone destructor, CO2 filter for the base reagent container, 24 V relay on the
ozone board, 24 V plug-in relays in the relay board (81204001), sample out valve, exhaust valve, acid valve,
diaphragm in the mixer reactor and the wetted parts of the sample valve (ARS valve).
3 Normally replaced at 24 month intervals.

38
 Replacement parts and accessories

Replacement parts (continued)

Quantity to
Description2 Item no.
stock
Tubing, EMPP, 5.6 mm OD x 2.4 mm ID, 1 m length 1 m length 10-REH-003
Tubing, EMPP, 6.9 mm OD x 4.1 mm ID, 1 m length 1 m length 10-REH-008
Valve, N/C with plug, Type 6606 Burkert 1 19-EMC-001
Valve, N/O with plug, Type 6606 Burkert 1 19-EMC-002
Valve, C/O with plug, Type 6606 Burkert 1 19-EMC-003
Valve, non-return (check valve), 1 psi 1 10-SMR-001
Valve, pinch, B4M, C/O, complete 0 12-BIO-001
Valve, sample, PEEK ARS, 3.0 mm with integrated fittings 13 10-EMT-089
Valve, sample, PEEK ARS, 2.5 mm with integrated fittings 13 10-EMT-090

2 Consumables/wearing parts: EMPP tubing, Y tube fittings, filters for the fan and vent, FPM/FKM tubing in the
ozone generator, catalyst in the ozone destructor, CO2 filter for the base reagent container, 24 V relay on the
ozone board, 24 V plug-in relays in the relay board (81204001), sample out valve, exhaust valve, acid valve,
diaphragm in the mixer reactor and the wetted parts of the sample valve (ARS valve).

39
Replacement parts and accessories

40
HACH COMPANY World Headquarters HACH LANGE GMBH HACH LANGE Sàrl
P.O. Box 389, Loveland, CO 80539-0389 U.S.A. Willstätterstraße 11 6, route de Compois
Tel. (970) 669-3050 D-40549 Düsseldorf, Germany 1222 Vésenaz
(800) 227-4224 (U.S.A. only) Tel. +49 (0) 2 11 52 88-320 SWITZERLAND
Fax (970) 669-2932 Fax +49 (0) 2 11 52 88-210 Tel. +41 22 594 6400
[email protected] [email protected] Fax +41 22 594 6499
www.hach.com www.de.hach.com

© Hach Company/Hach Lange GmbH, 2020, 2022, 2024. All rights reserved. Printed in Ireland.
*DOC023.52.90643*