iLF Forschungs- und Entwicklungsgesellschaft Lacke und Farben mbH
Fichtestraße 29 | D-39112 Magdeburg
TEST REPORT
Test report No.: 160695.1
Client: Sika Deutschland GmbH
Mr Claus Ackfeld
Rieter Tal
D – 71665 Vaihingen
Contract No./Date: 03/08/2016
Quotation No.: -
Subcontractors: none
Archiving of samples: 3 months
Subjects of testing: Coated steel plates
Aim of testing: Testing in accordance to ISO 12944-6; C3-high [1998]
Origin of sample: Samples sent by customer
Entry Date of samples: 04/08/2016
Start of testing: 19/08/2016
End of testing: 21/09/2016
Laboratory: Application Technology
Test methods: Pull-off test for adhesion according to DIN EN ISO 4624
Cross-cut testing according to DIN EN ISO 2409
Salt spray test according to DIN EN ISO 9227
Resistance to moisture: Part 1 Continuous condensation
according to DIN EN ISO 6270-1
Number of pages: 5
Fichtestraße 29 Stadtspk. Magdeburg Geschäftsführer: USt-IdNr.:
D-39112 Magdeburg BLZ: 810 532 72 Dr. Ulrich Westerwelle DE163828357
Tel: +49 (0)391 6090-0 Kto.: 34 372 260 AG Stendal HRB 107162
Fax: +49 (0)391 6090-217 Nord/LB Magdeburg Sitz der Gesellschaft:
[email protected] BLZ: 250 500 00 Magdeburg
www.lackinstitut.de Kto.: 122 034 036
Test Report No. 160695.1
1. Test specimen
The client delivered 10 coated steel plates with the following structure:
Substrate: Steel
Surface preparation: Sa 2 ½ according to DIN EN ISO 12944-4
Roughness: 50 – 85 µm
Conditioning: storage of the samples according to DIN EN ISO 12944-6
3 weeks in standard atmosphere (23 ± 2) °C and (50 ± 5) % RH
System:
DB: 160 µm SikaCor EG-120 (Charge: A = 3001978999, B = 3001995759)
Table 1: Panel Number and film thickness by client
Panel No. Mean value Maximum Minimum
Client [µm] [µm] [µm]
S1-1 184 191 168
S1-2 185 190 172
S1-3 176 188 153
S1-4 183 191 170
S1-5 163 180 148
S1-6 176 184 157
S1-7 182 192 169
S1-8 173 181 170
S1-9 190 198 180
S1-10 189 197 167
2. Test procedure
2.1. Initial adhesion
Test procedure: Cross-cut test according to DIN EN ISO 2409
Pull-off test for adhesion according to DIN EN ISO 4624
Adhesive: 2K UHU endfest 300
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Test Report No. 160695.1
Table 2: Results – initial adhesion
Cross-cut Pull-off test
Panel – No. target value: target value: no A/B, unless ≥ 5 MPa
2
Gt ≤ 1 N/mm Fracture appearance
6,0 100% B
S1-1 Gt 0
8,0 100% B
6,0 100% B
S1-2 Gt 0
6,0 100% B
7,0 60% B 40% Y
S1-3 Gt 0
6,0 70% B 30% Y
2.2. Resistance to humidity
Test procedure: Resistance to humidity: Part 1 Continuous condensation according to DIN
EN ISO 6270-1
Test time: 240 h
Evaluation: Blistering according to DIN EN ISO 4628-2
Rusting according to DIN EN ISO 4628-3
Degree of cracking according to DIN EN ISO 4628-4
Degree of flaking according to DIN EN ISO 4628-5
Cross-cut according to DIN EN ISO 2409
Pull-off test for adhesion according to DIN EN ISO 4624
Glue: 2K UHU endfest 300
Table 3: Results after 240 h humidity test
Blistering Rusting Cracking Flaking
Panel – No.
target value: 0 (S0) target value: Ri 0 target value: 0 (S0) target value: 0 (S0)
S1-8 0 (S0) Ri 0 0 (S0) 0 (S0)
S1-9 0 (S0) Ri 0 0 (S0) 0 (S0)
S1-10 0 (S0) Ri 0 0 (S0) 0 (S0)
Table 4: Adhesion results after humidity test
Cross-cut Pull-off test
Panel – No. target value: target value: no A/B, unless ≥ 5 MPa
2
Gt ≤ 1 N/mm Fracture appearance
7,0 90% B 10% Y
S1-8 Gt 0
7,0 100% B
6,0 100% B
S1-9 Gt 0
6,0 100% B
5,0 100% B
S1-10 Gt 0
5,5 100% B
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Test Report No. 160695.1
2.3. Salt spray test
Test procedure: Salt spray test according to DIN EN ISO 9227 (NSS)
Test time: 480 h
Evaluation: Blistering according to DIN EN ISO 4628-2
Rusting according to DIN EN ISO 4628-3
Degree of cracking according to DIN EN ISO 4628-4
Degree of flaking according to DIN EN ISO 4628-5
Delamination/Corrosion around scribe according to DIN EN ISO 4628-8
Scratch width: 1,0 mm
Cross-cut according to DIN EN ISO 2409
Pull-off test for adhesion according to DIN EN ISO 4624
Glue: 2K UHU endfest 300
Table 5: Results after 480 h salt spray test
Corrosion
Panel - Blistering Cracking Flaking Rusting
target value: 0 target value: target value: target value:
c [mm]
No. (S0) 0 (S0) 0 (S0) Ri 0
target value:
c ≤ 1 mm
S1-4 0 (S0) Ri 0 0 (S0) 0 (S0) c = 0,8 mm
S1-5 0 (S0) Ri 0 0 (S0) 0 (S0) c = 0,7 mm
S1-6 0 (S0) Ri 0 0 (S0) 0 (S0) c = 0,7 mm
Table 6: Adhesion results after 480 h salt spray test
Pull-off test
Cross-cut
Panel target value: no A/B, unless ≥ 5 MPa
target value:
– No. 2 Fracture
Gt ≤ 1 N/mm
appearance
6,0 100% B
S1-4 Gt 0
> 20 -
5,5 100% B
S1-5 Gt 1
> 20 -
6,0 100% B
S1-6 Gt 0
7,0 100% B
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Test Report No. 160695.1
3. Summary
The coating system tested in accordance with ISO 12944-6, corrosivity category C3 – high,
fulfils the requirements.
Magdeburg, den 06.10.2016
iLF Forschungs- und Entwicklungsgesellschaft Lacke und Farben mbH
Dipl.-Chem. Cornelia Dreyer Dipl.-Ing. Katharina Nelius
Lab supervisor Application Technology Laboratory person in charge
Notation:
This test report is a shortened test report that does not cover all test conditions required by the
applicable standards.
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