Scribd
Upload
54 views1 page

29A Flow Chart

A procedure was carried out where 38 mg of 1,4-dichlorobenzene was added to a conical vial with nitric acid and let stand for 15 minutes. Water was then added dropwise while stirring and the mixture was cooled in an ice bath. The product was filtered, washed, dried and a melting point was taken to identify the crystal product.

Uploaded by

Tyler Markus
Copyright
© Attribution Non-Commercial (BY-NC)
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as DOCX, PDF, TXT or read online on Scribd
54 views1 page

29A Flow Chart

A procedure was carried out where 38 mg of 1,4-dichlorobenzene was added to a conical vial with nitric acid and let stand for 15 minutes. Water was then added dropwise while stirring and the mixture was cooled in an ice bath. The product was filtered, washed, dried and a melting point was taken to identify the crystal product.

Uploaded by

Tyler Markus
Copyright
© Attribution Non-Commercial (BY-NC)
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as DOCX, PDF, TXT or read online on Scribd
You are on page 1/ 1

In a 3ml conical vial equipped with a air condenser ad 38 mg of 1,4dichlorobenzene, then 10L of anhydrous nitric acid using a auto

pipette.

Let stand at room temperature for 15 minutes.

Add 1.0 mL of water from a pipette drop wise while stirring with a glass rod.

Place in an ice bath in order to cool.

Weigh the product.

Allow to dry.

Wash the filter product with 4 1.0mL portions of water.

Collect the crystal product using a Hirsch funnel.

Complete a mixed melting point of product.

I certify that this is my own work and I understand that if I am found to be in violation of the honor code, I will be subject to the highest penalty. Jonathan Melgar X__________________________________

You might also like