Jordan University of Science and Technology
Department of Civil Engineering
Materials of Construction Laboratory
(CE 326)
Experiment 1:
Time of Setting of Hydraulic cement
By:
Eng. Zain Ghazi AL-Kofahi
Cement Tests
Number of tests are performed in the cement plant
laboratory to ensure that the cement is of the
desired quality and that it conforms to the
requirements of the relevant national standards.
Objectives
1.
2.
To determine the amount of water required to
prepare cement paste for testing.
To determine the time of setting of hydraulic
cement by means of the Vicat needle.
Apparatus
1.
2.
3.
4.
5.
6.
Mixer.
Vicat apparatus.
Conical ring.
Glass plate.
Balance.
Timer.
Materials
Hydraulic cement 650g.
Water (23oC)
Normal consistency test (ASTM 187 - 86
Re approved 1991)
In the acceptance tests for cement, the water content is
regulated by bringing the paste to a standard condition of
wetness. This is called Normal Consistency
- Cement of normal consistency is required to measure
setting time.
Definition of terms
- Normal consistency: A standard measure of plasticity of a
cement paste. A paste has normal consistency when a
Vicat plunger (10 mm in diameter) penetrates 10 1 mm
in 30 sec under its own weight. The required water/cement
ratio is determined by trial and error.
The quantity of mixing water to form a standard paste
for setting and soundness test .
It depends upon the compound composition and
fineness of cement.
About 24%~30% ( by weight) for Portland cement.
Normal consistency test
Mixing of Cement Paste :
- place all the mixing water in the bowl.
-Add the cement to the water and allow
30s for the absorption of the water.
- Mix at slow speed (140 5 r/min.) for
30s.
- Stop the mixer and wait for 15s, during
this time scrap down into batch any
paste that may have collected on sides
of the bowl.
-Mix at medium speed (285 10 r/min.)
for 1minute.
Normal consistency test
Molding Test Specimen:
- Mold cement paste into shape of
a ball. With gloved hands, toss
ball six times through a free
path of about six inches from
one hand to another.
- Press ball into larger end of
Vicat ring and completely fill
ring with paste.
- Remove excessive paste without
compressing samples and
locate ring under plunger of
Vicat apparatus.
Consistency Determination:
- Place plunger in contact with top of
paste and lock. Set indicator on the
scale to zero.
- Release plunger and record settlement
of plunger in mm after 30 seconds.
- Repeat process with trial paste with
varying percentages of water until
normal consistency is observed.
Report
Record the weight of water added to 650g of cement,
when the plunger penetrates 10mm (9mm to 11mm) in 30
seconds.
W =--------------- g of water.
w/c = --------------%
Discussion Question:
With finer cement particle size, would more or less water be
required to achieve the normal consistency? Briefly
explain.
Set Time Test (ASTM C 191 - 92)
Setting time is the term used to describe the stiffening of the
cement paste, and it refers to a change from a fluid state to a rigid
state.
Definition of terms:
- Time of initial set: The time at which the concrete can no longer be
properly mixed, finished or compacted. (Represented by a Vicat
needle ( 1mm in diameter) penetration of 25 mm or less). ASTM
C150 prescribes a minimum initial setting time of 60 minute for
Portland cement. (45 minutes (BS12:1978))
- Time of final set: The time required for the cement to harden to a
point where it can sustain some load. (Represented by no
penetration of Vicat needle, the needle makes an impression and
the cutting edge fails). ASTM C150 prescribes a maximum final
setting time of 10-12 hours for Portland cement.
Set Time Test
Factors affecting setting time:
Temperature and humidity.
Amount of water (w/c)
Chemical composition of
cement.
Fineness of cement ( finer
cement faster setting).
Set Time Test
Procedures
- Mix 650 g of cement with the percentage of water
required for normal consistency as described
previous.
- After molding cement paste into the test ring,
place specimen in moist room for 30 minutes.
- Place specimen ring under Vicat apparatus and
lock needle on surface of paste. Set indicator
scale to zero.
- Release weighted needles and record the
penetration in mm after 30 seconds.
- Repeat process every fifteen minutes until initial
set is achieved.
- Repeat processes every hour until final set is
achieved.
Report
Calculation
Calculate the time to the nearest minute required for the paste of
normal consistency to achieve initial and final sets.
The setting time for the given cement sample are found to be :
Initial setting (Represented by a Vicat needle penetration of 25
mm) =.minutes
Final setting time =.minutes
Discussion Questions:
(1) Does the initial setting time satisfy the requirements of
the British Standards?
(2) Discuss briefly the significance of determining the initial
and final setting times.
(3)If the initial setting time is not qualified, can we use the
cement in engineering?
Conclusions:
The amount of water required to prepare cement
paste for testing is
The setting times for the given cement sample are
found..(within/ not within)
the standards.
