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Penentuan Kadar Sari (Modul 5)

The document discusses the determination of extract content from a sample. It describes calculating the percentage of water-soluble and ethanol-soluble extracts from the sample by measuring the solids obtained after evaporating solvents. The procedures for determining the water-soluble and ethanol-soluble extract contents are described step-by-step. Calculations of extract percentages are shown based on weights measured before and after drying.

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Setyo Wibowo
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2K views5 pages

Penentuan Kadar Sari (Modul 5)

The document discusses the determination of extract content from a sample. It describes calculating the percentage of water-soluble and ethanol-soluble extracts from the sample by measuring the solids obtained after evaporating solvents. The procedures for determining the water-soluble and ethanol-soluble extract contents are described step-by-step. Calculations of extract percentages are shown based on weights measured before and after drying.

Uploaded by

Setyo Wibowo
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
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Download as DOCX, PDF, TXT or read online on Scribd
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Modul 5

Penentuan Kadar Sari

Lampiran

A. Perhitungan
Bobot sari yang di dapat
Larut air : a. 79,28 gram -79,22 gram = 0,06 gram
b. 92,12 gram - 92,05 gram = 0,07 gram
Larut etanol : a. 93,33 gram - 93,24 gram = 0,09 gram
b. 90,44 gram - 90,57 gram = 0,07 gram

% Kadar sari
Larut air : a. 0,06 gram x 100 x 100% = 12 %
2 gram 25

b. 0,07 gram x 100 x 10% = 14 %


2 gram 25

Larut Etanol : a. 0,09 gram x 100 x 100% = 18 %


2 gram 25

b. 0,07 gram x 100 x 100% = 14 %


2 gram 25

Rata rata bobot sari


Larut air : 0,06 + 0,07 = 0,065 gram
2

0,09 + 0,07 = 0,08 gram


2
Perhitungan bobot sari
Persyaratan bobot tetap 0,05 mg/gram
Cawan 1 : 0,05 mg/gram x 79,28 gram = 39,64 mg = 0,0396 gram
t1 : 79,27 gram
t2 : 79,28 gram
t : 0,01 gram (0,01 < 0,03 gram) ... bobot tetap pada t2

Cawan 2 : 0,05 mg/gram x 92,12 gram = 46,06 mg = 0,046 gram


t1 : 92,11 gram
t2 : 92,10 gram
t : 0,01 gram (0,01 < 0,04 gram) ... bobot tetap pada t2
Cawan 3 : 0,05 mg/gram x 93,33 gram = 46,66 mg = 0,046 gram
t1 : 93,22 gram
t2 : 93,31 gram
t : 0,01 gram (0,01 < 0,04 gram) ... bobot tetap pada t2

Cawan 4 : 0,05 mg/gram x 90,44 gram = 45,22 mg = 0,045 gram


t1 : 90,43 gram
t2 : 90,42 gram
t : 0,01 gram (0,01 < 0,45 gram) ... bobot tetap pada t2
B. Dokumentasi
C. Diagram Alir

1. Penetapan kadar sari larut etanol

2,0 4,0 gram Simplisia

- Dimaserasi dengan etanol selama 18 jam


sambil sesekali dikocok selama 6 jam
pertama
- Di saring

Filtrat Residu
- Diambil 25,0 ml
- Diuapkan dalam cawan dangkal di tangas air
Residu Pengeringan
- Dipanaskan pada suhu 1050 C ad bobot tetap
- Dihitung % kadar
% Kadar sari larut etanol

2. Penetapan kadar sari larut air (metode panas)


2,0 4,0 gram simplisia pada erlenmeyer
- (+) 100 ml air
- Ditimbang wadah dan isinya
- Diaduk, biarkan 1 jam
- Dinginkan dan timbang kembali
- Ditambah air hingga bobot awal
- Aduk
- Saring

Filtrat Residu
- Diuapkan 25,0 ml - Dipanaskan pada
dalam cawan dangkal suhu 1050 hingga
di atas tangas air hingga bobot tetap
kering
- Dihitung kadar
Hasil
dalam persen
terhadap berat
simplisia
Hasil

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