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Tabel

This document describes a series of experiments observing the reactions of various transition metal salts (CrCl3, Mn(SO4), Fe(NH3)2SO4, etc.) with sodium hydroxide, ammonium hydroxide, and ammonium thiocyanate solutions. It records the initial colors of the salts and any color changes or precipitates observed after adding the reactive solutions. The experiments aim to identify the ions formed in each reaction through observation of properties and comparison to reference data on ion complexes.

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ayu irsalina
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40 views4 pages

Tabel

This document describes a series of experiments observing the reactions of various transition metal salts (CrCl3, Mn(SO4), Fe(NH3)2SO4, etc.) with sodium hydroxide, ammonium hydroxide, and ammonium thiocyanate solutions. It records the initial colors of the salts and any color changes or precipitates observed after adding the reactive solutions. The experiments aim to identify the ions formed in each reaction through observation of properties and comparison to reference data on ion complexes.

Uploaded by

ayu irsalina
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© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
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First Experiment

a. Reaction with NaOH 1M


Observation
Salt After added NaOH After added NaOH Ion Complex
Initial Compound equation
(3 drops) excess (3 drops) equation
CrCl3 Blue Dark green precipitate [Cr(H2O)3(OH)3]-(aq) Dark green [Cr(H2O)2(OH)4](s)
Mn(SO4) Colorless Brown (-) [Mn(H2O)4(OH)2](s) Dark brown [Mn(H2O)3(OH)3](s)
Fe(NH3)2SO4 Yellow (-) Dark Green (+) [Fe(H2O)4(OH)2]-(aq) Dark green (+) [Fe(H2O)3(OH)3](s)
Brown (+++),
FeCl3 Yellow Brown (+) [Fe(H2O)3(OH)3]-(aq) [Fe(H2O)3(OH)3] (s)
precipitate
Green (++),
CoCl2 Pink Tosca, precipitate [Co(H2O)4(OH)2](s) [Co(H2O)3(OH)3] (s)
Precipitate
NiCl2 Green (-) Green (-), precipitate [Ni(H2O)4(OH)2](s) Green (-), Precipitate [Ni(OH)3(H2O)3](s)
Dark Blue (+),
CuSO4 Blue (+) Blue (+) , Precipitate [Cu(H2O)4(OH)2](s) [Cu(H2O)3(OH)3] (s)
Precipitate
ZnCl2 Colorless Turbid, Precipitate [Zn(H2O)4(OH)2](s) Turbid, Precipitate [Zn(H2O)3(OH)3](s)
b. Reaction with NH3 2M
Observation
Salt After added NH3 (3 After added NH3 Ion Complex
Initial Compound equation
drops) excess (3 drops) equation
CrCl3 Blue Dark green Cr(OH)3(s) Green precipitate [Cr(NH3)6]3+(aq)
Dark brown, brown
Mn(SO4) Colorless Turbid yellow Mn(OH)2(s) [Mn(NH3)6]2+(aq)
precipitate
Green, Dark green
Fe(NH3)2SO4 Yellow (-) Dark Green (++) [Fe(H2O)(NH3)5]2+(aq [Fe(NH3)6]2+(aq)
precipitate
Brown , Brown
FeCl3 Yellow Turbid Brown [Fe(H2O)(NH3)5]3+(aq) [Fe(NH3)6]3+(aq)
precipitate
Blue, Tosca
CoCl2 Pink Blue precipitate [Co(NH3)6]2+(aq) Co(OH)3(s)
precipitate
NiCl2 Green (-) Blue (-) [Ni(H2O)(NH3)5]2+(aq) Turbid blue (--) [Ni(NH3)6]2+(aq)
Dark blue, Blue
CuSO4 Blue (+) [Cu(H2O)(NH3)3]2+(aq) Tosca (++) [Cu(NH3)4]2+(aq)
precipitate
Colorless, White
ZnCl2 Colorless Colorless turbid Zn(OH)2(s) [Zn(NHs)(OH)2](s)
precipitate
c. Reaction transition metal ion with NH4CNS 0,1M

Observation
Salt
Initial after NH4CNS (10 drops) Ion complex equation
CrCl3 Blue Blue (--) [Cr(H2O)5(SCN)]2+

Mn(SO4) Colorless Colorless [Mn(H2O)5(SCN)]+

Fe(NH3)2SO4 Yellow (-) Reddish Brown (+) [Fe(H2O)5(SCN)]+

FeCl3 Yellow Reddish Brown [Fe(H2O)5(SCN)]+


CoCl2 Pink Pink [Co(H2O)5(SCN)]+
NiCl2 Green (-) Green (--) [Ni(H2O)5(SCN)]+
CuSO4 Blue (+) Green (-) [Cu(H2O)5(SCN)]+

d. Blanco

observation
Salt
Initial After added 1mL aquadest
CrCl3 Blue Light Blue
Mn(SO4) Colorless Colorless
Fe(NH3)2SO4 Yellow (-) Light Yellow (-)
FeCl3 Yellow Light Yellow
CoCl2 Pink Light Pink
observation
Salt
Initial After added 1mL aquadest
NiCl2 Green (-) Light Green (-)
CuSO4 Blue (+) Light Blue (+)

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