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Data Pengamatan Distilasi Batch

This document provides steps to calculate carbon dioxide absorption rate in a sodium hydroxide solution. It involves: 1) Determining the CO2 absorption rate in the sodium hydroxide solution by analyzing sample composition and concentrations. 2) Observing the mass equilibrium in the absorption column by collecting data on gas and liquid flow rates, concentrations, pressures, and temperatures. 3) Using the data to calculate the amount of CO2 removed, sodium hydroxide consumption, sodium carbonate produced, and overall mass transfer coefficient.

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39 views3 pages

Data Pengamatan Distilasi Batch

This document provides steps to calculate carbon dioxide absorption rate in a sodium hydroxide solution. It involves: 1) Determining the CO2 absorption rate in the sodium hydroxide solution by analyzing sample composition and concentrations. 2) Observing the mass equilibrium in the absorption column by collecting data on gas and liquid flow rates, concentrations, pressures, and temperatures. 3) Using the data to calculate the amount of CO2 removed, sodium hydroxide consumption, sodium carbonate produced, and overall mass transfer coefficient.

Uploaded by

ribka
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
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LANGKAH PERHITUNGAN

A. Menentukan laju penyerapan CO2 dalam larutan Sodium Hydroxide dari analisis
sampel
Menentukan komposisi sampel
 Konsentrasi NaOH (CC) dalam sampel asli:

 Konsentrasi Na2CO3 (CN) dalam sampel asli:

B. Pengamatan kesetimbangan massa yang terjadi pada kolom absorbsi


Tabel 2.6 Data perhitungan kesetimbangan massa
Quantity Symbol Comments
Air flow rate (l/min) F2 Convert to l/s by dividing by 60

CO2 flow rate (l/min) F3 Convert to l/s by dividing by 60

Sodium Hydroxide (NaOH) Li = Lo Convert to l/s by dividing by 60


flow rate (l/min)
CO2 outlet concentration Yo Read values from the console
display
CO2 inlet concentration Yi Read values from the console
display
Liquid Samples outlet
Titration with HCl (ml) T1(o) Refer to exercise A Module 10
(0.2M HCl used in titration of
100 ml sample)
Titration with HCl (ml) T2(o) Refer to exercise A Module 10
(0.2M HCl used in titration of
100 ml sample)
Titration with HCl (ml) T 3(o) Refer to exercise A Module
(0.2M HCl used in titration of
100 ml sample)
Liquid samples inlet
Titration with HCl (ml) T1(i) Refer to exercise A Module 10
(0.2M HCl used in titration of
50ml sample)
Titration with HCl (ml) T2(i) Refer to exercise A Module 10
(0.2M HCl used in titration of
50ml sample)
Titration with HCl (ml) T3(i) Refer to exercise A Module 10
(0.2M HCl used in titration of
100ml sample)
Column pressure drop (mbar) ∆P1 Read values from the console
display
Column pressure drop (mbar) ∆P2 Read values from the console
display
Pressure of column (mbar) P ∆P2 + ∆P1
Temperature of feed gas (oC)  Convert to K by adding 273

 Aliran Gas

Jumlah CO2 yang hilang


 Aliran fluida cair
NaOH: Konsentrasi CO2 terkait dengan konsumsi hidroksida dalam cairan:

Na2CO3
Seperti dari percobaan A Module 10, konsentrasi Na2CO3:

Karbonat dihasilkan oleh penyerapan CO2 (𝑔.𝑚𝑜𝑙 / 𝑠𝑒𝑐)


C. Menentukan koefisien Mass Transfer Keseluruhan menggunakan film gas (Kog).
1. Gunakan nilai N (laju penyerapan CO2) yang dihitung dalam percobaan A modul
9.
2. a adalah area bahan isian / volume unit menara, untuk cincin Raschig 10 mm
adalah 440 m2 / m3.
3. A.H. adalah volume kolom (area = π / 4 x (d)2, H = tinggi kolom)
4. Log mean driving force

5. Mass transfer coefficient:

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