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Oyani Mixed Secondary School: Chemistry Paper3 (Practical)

This document appears to be instructions for a chemistry practical exam involving 3 questions. [1] The first question involves determining the concentration of an unknown dibasic acid solution and calculating the molar heat of neutralization through a titration experiment. Students are provided solutions of the acid, potassium carbonate, and sodium hydroxide to carry out titrations and measurements. [2] The second question involves testing an unknown solid labeled M using common reagent tests and making observations and inferences about its identity. Tests include reactions with sodium hydroxide, sulfuric acid, ammonia, lead nitrate, and barium nitrate. [3] The third question involves dividing an unknown liquid labeled

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100% found this document useful (1 vote)
794 views7 pages

Oyani Mixed Secondary School: Chemistry Paper3 (Practical)

This document appears to be instructions for a chemistry practical exam involving 3 questions. [1] The first question involves determining the concentration of an unknown dibasic acid solution and calculating the molar heat of neutralization through a titration experiment. Students are provided solutions of the acid, potassium carbonate, and sodium hydroxide to carry out titrations and measurements. [2] The second question involves testing an unknown solid labeled M using common reagent tests and making observations and inferences about its identity. Tests include reactions with sodium hydroxide, sulfuric acid, ammonia, lead nitrate, and barium nitrate. [3] The third question involves dividing an unknown liquid labeled

Uploaded by

Almadi
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
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Download as DOCX, PDF, TXT or read online on Scribd
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NAME ………………………………………………………………… ADM. NO. ……………………………….

CLASS……………………………………………… CANDIDATES SIGN……........………………......………...

DATE………………………………

233/3
FORM FOUR
CHEMISTRY PAPER 3
PRACTICAL
MARCH 2020
TIME: 21/4 HOURS

OYANI MIXED SECONDARY SCHOOL


CHEMISTRY PAPER3 (PRACTICAL)

Instructions to candidates

1. Write your name and index number in the spaces provided above
2. Sign and write the date of examination in the spaces provided above\
3. Answer ALL the questions in the spaces provided.
4. You are NOT allowed to start working with the apparatus for the first 15 minutes of the21/4 hours
allowed for this paper. This time is to enable you read the question paper and make sure you have all the
chemical and apparatus that you need.
5. Mathematical tables and silent electronic calculators may be used.
6. All workingMust be clearly shown where necessary.

For examiner’s use Only

Questions Maximum Score Candidate’s Score


1 22
2 10
3 08
Total score 40

1. You are provided with;

Turn over
 A dibasic acid, labeled solution P
 Solution R containing 5.56g per litre of potassium carbonate
 Aqueous sodium hydroxide, labeled solution T
You are required to determine the :
- Concentration of solution P in moles per litre
- Molar heat of neutralization of solution p with sodium hydroxide labeled solution T

A Procedure 1

Using a pipette and a pipette filler, place 25cm3 of solution P into a 250ml volumetric flask. Add water to
make 250cm3 of solution. Label this solution Q. Place solution Q in a burette. Clean the pipette and use it to
place 25.0cm3 of solution R into a conical flask. Add 2 drops of methyl orange indicator provided and titrate
with solution Q. Record your results in table 1. Repeat the titration two more time and complete the table.

Table 1

I II III
Final burette reading
Initial burette reading
Volume of solution Q used (cm3)
(4 mks)

Calculate the:
(i) Average volume of solution Q used (1 mk)

(ii) Concentration of potassium carbonate in solution R (K = 39.0, O = 16.0, C = 12.0) (1 mk)

(ii) Concentration of dibasic acid in solution Q (2 mks)

(iii) Concentration of dibasic acid in solution P (1 mk)

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Procedure 2
Clean the burette and fill it with solution T. Clean the pipette and use it to place 25.0cm3 of solution P into a
100cm3 plastic beaker. Measure the initial temperature of this solution and record it in table 2.
From the burette, place 5cm3 of solution T into the beaker containin 25.0cm3 of solution P, stir the mixture
carefully with a thermometer and record the highest temperature of the mixture in table 2. Place another
5cm3 of solution T into the mixture in the beaker, stir carefully and record the highest temperature of this
mixture in table2. Continue this procedure of placing 5cm3 portions of solution T and complete table 2.
Table 2
Total volume of solution T added (cm3) 0 5 10 15 20 25 30
3
Volume of solution P (cm ) 25 25 25 25 25 25 25
Temperature (0C)
(4 mks)
(i) On the grid provided, draw a graph of temperature (vertical axes) against volume of solution T used.
(3
mks)

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(ii) From the graph, determine
I The highest temperature change, ∆T (1 mk)

II The volume of solution T required to react with 25cm3 of solution P (1 mk)

(iii) Calculate the ,


I The number of moles of solution P used (1 mk)

II Molar heat of neutralization of P with sodium hydroxide solution labeled T (assume the specific heat
capacity of the solution is 4.2Jg-1K-1 and density of solution is 1.0gcm-3 (3 mks)

2. You are provided with solid labeled M. Use it for the test below.
(a) Put all of solid M in a clean boiling tube. Add about 10cm3 of distilled water and shake thoroughly.
Use about 2cm3 of the resulting mixture for the test (b) to f below

Observation inferences

(1 mk) (1 mk)

(b) Add a few drops of aqueous sodium hydroxide and then excess

Observation inferences

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(1 mk) (1 mk)
3
(c) Add about 2cm of dilute sulphuric (vi) acid
Observation inferences

(1 mk) (1 mk)

(d) Add a few drops of aqueous ammonia solution and then excess
Observation inferences

(1 mk) (1/2 mk)

(e) Add about 2cm3 of acidified lead (ii) nitrate


Observation inferences

(1/2 mk) (1 mk)

(f) Add about 2cm3 of barium nitrate solution


Observation inferences

(1/2mk) (1/2mk)

3. You are provided with liquid N. Divide it into 4 portions and use it for the tests below.
(a) Place about 3 drops of N on a clean watch glass and ignite
Observation inferences

(1 mk) (1 mk)

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(b) Add about 3 drops of acidified potassium manganate (vii) to the second portion
Observation inferences

(1 mk) (1 mk)

(c) Add the sodium carbonate provided to the third portion.


Observation inferences

(1/2mk) (1/2mk)

(d) Use sample 4 to test whether the substance is polar or not. Give the procedure for the test
Procedure Observation inferences

(1 mk) (1 mk) (1 mk)

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