Jerome 631-X: User Manual Hydrogen Sulfide Analyzer Operation Manual
Jerome 631-X: User Manual Hydrogen Sulfide Analyzer Operation Manual
JEROME® 631-X
HYDROGEN SULFIDE ANALYZER
OPERATION MANUAL
September 2017
www.azic.com
Email:
General – [email protected]
International – [email protected]
Customer Service – [email protected]
Operation Manual
This manual contains valuable information and material developed by Arizona Instrument LLC for
use with the Jerome® 631-X Hydrogen Sulfide Analyzer. No part of this manual can be
reproduced or transmitted in any form or by any means, electronic, mechanical or otherwise. This
includes photocopying and recording or in connection with any information storage or retrieval
system without the express written permission of Arizona Instrument LLC.
This manual contains details that will optimize the results and the life of your instrument. Read
and refer to the manual for complete details on operation, maintenance and troubleshooting,
special voltage inputs and data output.
The Jerome® 631-X is easy to operate and ready for use upon receipt from the factory.
• Remove the instrument from the packing material.
• Check the voltage setting (110 or 220 VAC) on the back of the
instrument. Ensure that it is set to the correct voltage. If the
pointer is not aligned to the local voltage, turn the selector to
point to the correct voltage.
CAUTION
Do not adjust the ZERO after the instrument has measured hydrogen sulfide
or before the next regeneration. (Occasionally the display may drop to .L.L.L
(indicating low) between the initial zeroing and the first sample. It is OK to
readjust the ZERO if the instrument has not measured hydrogen sulfide.)
• The instrument is designed for ambient air monitoring. DO NOT allow the probe or the
instrument’s intake to be exposed to any liquid.
• The instrument is not explosion proof.
• Press the SAMPLE button to start a 10 second sampling cycle.
• Perform sensor regeneration after each day’s testing.
• Perform another sensor regeneration and re-zero the instrument before each day’s use.
• Perform sensor regeneration after 30 days of storage or inactivity.
Note: There are two different versions of the 631-X, and they can be distinguished by a small
‘SMV’ label located above the serial label on the back of the instrument. In this manual, when it
is necessary to distinguish between the two versions, they are referred to as ‘SMV’ instruments or
‘Non-SMV’ instruments. Check for the ‘SMV’ label on your instrument to determine which steps
apply to your instrument. ‘SMV’ instruments can be purchased with the Option Functionality
and/or the Data Logger Functionality if desired.
Call AZI Customer Service, at (800) 528-7411 from the United States and Canada or (602)
470-1414 if you have any questions. If you prefer, you may send e-mail to [email protected]
The Jerome® 631-X Hydrogen Sulfide Analyzer is an ambient air analyzer with a range of 0.003
ppm to 50 ppm (parts per million).
CAUTION:
The Jerome® 631-X is for vapor use only.
DO NOT allow the probe or the instrument's intake
to be exposed to any liquid, dust
or other foreign material.
The 631-X is designed to be easy to operate for quick and accurate analysis of hydrogen sulfide
vapor levels. It has few maintenance requirements. However, please take a moment to read this
manual before attempting operation. If you have any questions about your application or
operation, please call AZI Customer Service at (800) 528-7411 or (602) 470-1414 or e-mail
[email protected] for assistance.
631-X Features
• Accurate analysis of hydrogen sulfide in seconds
• Wide detection range allows multiple applications
• Survey mode for rapid source detection of hydrogen sulfide concentrations
• Rechargeable internal battery pack for portability
• Automatic backlight for LCD during low light conditions
• Microprocessor ensures a linear response throughout the entire range of the sensor
• Inherently stable gold film sensor
Optional Accessories
• Data Logger to record field monitoring information
• Jerome® Communication Software (JCS) Kit for unattended fixed-point sampling and
downloading information from the Data Logger to a computer.
• Option Functionality (factory installed option) for external fresh air solenoid support, auto-
zeroing, DC power operation, timed regeneration, 4-20 mA or 0-2 V analog output, and
timed sampling
• Functional Test Module (FTM) (P/N Z2600 0918 or Z2600 0930) and Accessory Kit
(Y2600 0920), for field verification of instrument functionality.
• Field Carrying Cases, hard sided P/N Y411 0904 or soft P/N 1400 0052, for versatile
handling and additional storage
• Maintenance Kit, P/N Y631 0905 for routine maintenance and upkeep
The Jerome® 631-X can be operated from 100-120 or 200-240 VAC. To change the default
voltage range, refer to “Setting the Input Voltage” on page 21.
3. PRINCIPLE OF OPERATION
A thin gold film, in the presence of hydrogen sulfide, undergoes an increase in electrical resistance
proportional to the mass of hydrogen sulfide in the sample.
When the SAMPLE button is pressed, an internal pump pulls ambient air over the gold film sensor
for a precise period. The sensor absorbs the hydrogen sulfide. The instrument determines the
amount absorbed and displays the measured concentration of hydrogen sulfide in ppm. During
normal sampling, the ambient air sample is diluted in the flow system at a ratio of 100:1. When
sampling in Range 0, (where low levels of hydrogen sulfide are expected) undiluted air samples
are drawn across the gold film sensor.
The instrument’s microprocessor automatically re-zeroes the digital meter at the start of each
sample cycle and freezes the meter reading until the next sample cycle is activated, thus
eliminating drift between samples.
During the sample mode cycle, bars on the LCD represent the percentage of sensor saturation.
Depending on the concentrations, 50 to 500 samples may be taken before the sensor reaches
saturation. At that point, a 10-minute heat cycle must be initiated to remove the accumulated
hydrogen sulfide from the sensor. During the sensor regeneration cycle, both solenoids are closed
to cause air to pass through a scrubber filter and provide clean air for the regeneration process.
The flow system’s final scrubber filter prevents contamination of the environment.
The heat generated during the regeneration may cause some low level thermal drift. To ensure
maximum sample accuracy, wait 30 minutes after regeneration before zeroing and using the
instrument.
The Zero Air Filter removes mercury vapor, mercaptans, and hydrogen sulfide from the air
sample. Readings with the filter installed should be near zero.
Because air that is cooler than the instrument will cause low readings and warmer air will cause
higher readings, the Zero Air Filter should be used to equilibrate the unit to ambient air
temperature. Continuous sampling with clean air will not cause saturation of the gold film sensor
but will equalize temperatures faster to allow accurate analysis to begin sooner. For best results,
be sure that the instrument is at the same temperature as the environment before testing.
The Zero Air Filter can also be used to identify contamination within the instrument. If the
readings do not reduce to near zero with the filter installed, contamination should be suspected. If
the readings do drop to near zero with the filter installed but elevate with the filter removed, the
presence of hydrogen sulfide at the sampled location is confirmed.
For more information on the use of the Zero Air Filter, contact customer service at 1-800-528-
7411, 1-602-470-1414, or visit our web site at http://www.azic.com.
LCD Codes
Before each day's use of the Jerome® 631-X, perform the following steps to verify proper
instrument operation:
• Press the power ON button.
The digital meter displays 000.
(Disregard the digital meter's initial momentary reading.)
Recharge or replace the battery pack if the LO BAT indicator REMAINS ON. Refer to
“Charging Batteries” on page 17 and/or “Replacing the Battery Pack” on page 21.
To ensure the instrument's electronics have stabilized, allow a 1-minute warm up
before beginning the next step.
• Use the Zero Air Filter to equilibrate the instrument to ambient air temperature.
Install the Zero Air Filter in the instrument’s intake.
Sample continuously until the readings stabilize.
• Thirty minutes after sensor regeneration is complete, zero the instrument. See page 13.
NOTE: For maximum accuracy, such as when testing with the Functional Test Module,
wait 30 minutes after the sensor regeneration cycle to re-zero the unit. For immediate
use, the unit can be re-zeroed immediately after sensor regeneration. See the notes on
page 13.
Sensor regeneration is needed to clear the 631-X sensor of any accumulated hydrogen sulfide.
This simple procedure should be done:
CAUTION:
Ensure the voltage selector on the back of the instrument, near the power
cord inlet connector, points to the local AC power value. See “Setting the
Input Voltage” on page 21.
To clean and protect the sensor, the supplied AC power must be 100 to
120 VAC or 220 to 240 VAC, depending on the available power source.
• Attach the power cord to the 631-X and plug it into AC power. AC power is required to
thermally regenerate the sensor.
• Press the power ON button.
• Press the REGEN button.
The digital meter flashes .H.H.H for the duration of the 10-minute cycle and displays
.0.0.0 when the cycle is completed.
• A minimum 30-minute wait after the sensor regeneration cycle is complete ensures
maximum sample accuracy. However, the unit can be used immediately following the
sensor regeneration if necessary. When the sensor regeneration is complete, press ZERO
and adjust the ZERO ADJUST pot until 0 appears on the display. Install the zero air
filter in the intake and take several samples or lock the instrument into survey mode (see
page 15). After approximately one minute, stop sampling and check the ZERO. Adjust
to 0. Repeat sampling through the zero air filter until reading remains on 0.
NOTE: The digital meter will read .P.P.P after REGEN is activated if the power cord is not
plugged in or if the instrument's fuse needs to be replaced. Connect the power cord, or if
necessary, replace the fuse. See “Changing the Fuse” on page 22.
• To ensure air entering the instrument is clean, install the zero air filter in the instrument’s
intake and sample until the readings stabilize.
• While pressing the ZERO button, turn the ZERO ADJUST
potentiometer (shown at right) using the trimmer tool until
the digital meter reads 0.
If the LCD reads H, turn the ZERO ADJUST counter-
clockwise;
If the LCD reads L, turn the ZERO ADJUST clockwise.
CAUTION:
Do not turn the ZERO ADJUST potentiometer between samples.
Turn the ZERO ADJUST only after a sensor regeneration cycle, otherwise
invalid readings will result.
• Press the power OFF button and disconnect the power cord.
• The Jerome® 631-X is ready for sampling.
CAUTION:
®
The Jerome 631-X is intended for vapor use only. DO NOT
allow the probe or the instrument's intake to be exposed to
liquids, dust or other foreign material. Moisture or liquids
drawn into the instrument can damage the sensor and flow
system.
This is the standard operation mode and is used for optimum accuracy.
• Allow a 1-minute warm up before beginning the next step to ensure the instrument's
electronics have stabilized.
Note: The Jerome® 631-X operates approximately six (6) hours on a fully charged battery.
The survey mode takes samples every 3 to 20 seconds automatically. The length of time varies
with the hydrogen sulfide concentration. Use this mode to locate the source of hydrogen sulfide,
such as a leak, a hot spot, or to assess areas of potentially high hydrogen sulfide concentrations.
After the survey mode is activated, the 631-X samples continuously.
• Allow a 1-minute warm up before beginning the next step to ensure the instrument's
electronics have stabilized.
• The instrument remains in the survey mode until one of the following occurs:
The sensor is saturated.
A LO BAT (low battery) signal is encountered.
An HL (high hydrogen sulfide level) is encountered.
The instrument is turned OFF.
NOTE: Approximately 100 samples at 0.5 ppm may be taken before the sensor saturates and
regeneration is required.
• When a generator is used to power the Jerome® 631-X, a high quality line conditioner or
voltage regulator is required to ensure a pure sine wave and regulated voltage is applied to
the instrument. The gold film sensor may be damaged by voltage that varies in amplitude
or by surges, spikes, and/or noise on the power line.
A special version of the Jerome® 631-X and a DC Power Kit are available to operate the
instrument from a secondary DC source. The source may be a car/truck battery or a storage cell
used in conjunction with solar panels.
There are certain inherent limitations to NiCad batteries. The primary limitation is a memory
effect that occurs when the batteries are partially discharged and then recharged, repeatedly. This
memory leads to a drastic reduction in the usable battery life. To prevent this memory effect,
periodically allow the battery pack to discharge completely, and then recharge the battery pack.
• When the batteries fail to hold a charge, the battery pack should be replaced.
Battery life under normal usage is approximately 1 year, depending on the number of
charge and discharge cycles.
To keep the Jerome® 631-X operating at peak performance, follow the maintenance schedule
below as a guide. Since maintenance is more a function of application and amount of use rather
than time, your requirements may be different from the listed schedule. Call AZI Customer
Service at 800-528-7411, 602-470-1414, or e-mail [email protected] for additional guidance for
your environment and operation.
REFER TO
PART/COMPONENT MAINTENANCE CYCLE
PAGE
At least once per month, after 1 month's storage,
Charge batteries Page 17
or when LO BAT appears
Change 0.25 inch fritware Weekly or as needed Page 19
Change internal filters and
After 6 months of use or as needed Page 20
tubing
Replace zero air filter 1 Annually
Factory calibration Annually Page 23
Appendix
Calibration check Monthly or as needed
A, Page 36
Annually or as needed. Page 21
Replace batteries The battery pack contains NiCad batteries.
Dispose of properly.
NOTE: Install the zero air filter into the instrument's intake during storage.
1
Zero air filters, LFS and LFD scrubber filters contain Resisorb® or AddSorb® VA13. Call AZI Customer Service at
800-528-7411, 602-470-1414, or e-mail [email protected] for a copy of the Safety Data Sheet (SDS). Dispose of all
filters properly.
The Jerome® 631-X's flow system is the crucial link between the sensor and the sample. For the
instrument to perform correctly, the flow system must be properly maintained. The user
maintainable components of this system are the intake filter (0.25 inch fritware), two scrubber
filters and connecting tubing.
Check the Preventive Maintenance Calendar on page 18, for a suggested schedule for changing
fritware and scrubber filters. The Tygon® tubing in the system must be free of crimps for proper
flow.
Replace the 0.25 inch fritware filter once each week or as needed. In dusty environments, the
fritware filter may need to be replaced as often as once a day. Replacement 0.25-inch fritware
filters are available from AZI, Consumable Sales at 800-528-7411 or 602-470-1414.
• Unscrew and remove the intake.
• Push the old fritware filter disc out of the intake with your
trimmer tool.
CAUTION:
The stem coming from the instrument onto which the outer intake housing is
attached must be securely held in place. If loose, the tubing inside the
instrument can become twisted when the intake housing is replaced. It may
be necessary to open the instrument and tighten the hold-down nuts inside
the instrument. Call AZI Customer Service at 800-528-7411, 601-470-1414,
or e-mail [email protected] if you have any questions
CAUTION:
Scrubber filters contain Resisorb® or AddSorb® VA13. Used filters,
especially the scrubber filter may contain hydrogen sulfide also. Use
proper methods when disposing of used filters. Call AZI Customer
Service at 800-528-7411, 601-470-1414, or e-mail [email protected] for a
copy of the Resisorb® or AddSorb® VA13 SDS or for other questions.
• Connect the new filters to the Tygon® tubing, ensuring all straight hose barbs point toward
the intake/pump corner of the case and elbow hose barbs point toward the sensor housing as
shown in the illustration.
Push the Tygon® as far as it will go onto the filter fittings.
• Push the filters into the mounting clips.
• Remove any crimps or twists in the tubing and ensure that tubing connections are secure. If
the tubing is loose, readings may not be accurate. Replace any tubing that has deteriorated
due to heat and/or age.
• Close the case and replace the screws.
• Dispose of all filters in accordance with state and federal environmental regulations.
Instruments are factory set and calibrated to use the power setting requested on the order.
However, the voltage setting is easily changed to use either 110 or 220 VAC.
If the instrument display reads .P.P.P when the instrument is connected to AC power or when
REGEN is pressed, or if the battery will not charge, the fuse may need to be replaced. The AC
line power could also be less than 100 VAC (220 VAC). Check the fuse with an ohmmeter and
the AC line power with a voltage meter.
The Jerome® 631-X's gold film sensor is inherently stable and does not require frequent
calibration. The interval between calibrations depends upon the application and frequency of use;
however, the recommended interval is every 12 months.
The Jerome® 631-X has been factory calibrated using laboratory equipment containing NIST
traceable permeation tubes. In order to calibrate the Jerome® 631-X, a sophisticated calibration
system is required that ensures stability of the calibration gas source, eliminates any pressure in
the calibration gas stream, and controls the temperature of the calibration environment.
Calibration requires the controlled environment, gas source, and computer software available only
at the factory or authorized repair/calibration facility.
We strongly recommend you take advantage of our calibration and maintenance service at Arizona
Instrument. Call Customer Service at (800) 528-7411 or (602) 470-1414 to arrange re-calibration.
A certificate of calibration is issued from AZI when your instrument is factory calibrated.
The Functional Test Module, AZI P/N Z2600 0918 or Z2600 0930, is used to determine if your
instrument is functioning correctly between recommended annual factory calibrations. It allows
you to have complete confidence in the sample results. This test verifies proper instrument
operation through the introduction of a known concentration of hydrogen sulfide into the Jerome®
analyzer.
If your application requires frequent verification of instrument function, this test demonstrates the
unit’s operation and function. Recording FTM results in an instrument log provides a quality
control/quality assurance record of instrument function between regular calibrations. If test results
fall within the expected range, you may assume the instrument is functioning correctly.
See APPENDIX A - 631-X FUNCTIONAL TEST MODULE on page 36 for more information
about the FTM procedures. Complete instructions for use are supplied with the test kit, AZI P/N
Z2600 0918 or Z2600 0930.
To order the FTM, contact your AZI Sales Representative at (800) 528-7411 or (602) 470-1414.
Line voltage less than 100 Check line voltage settings. Refer
VAC (or less than 200 VAC to page 21.
for 220V instruments).
Data output 1. RS-232 Serial, Baud Rate 1200 for use with Data
Logger, and/or Jerome® communication program.
2. RS-232 Serial data format with 0 & 20mA current
logic levels; Baud Rate 1200 (special industrial
applications) and Analog 20 mA output.
The 631-X I/O port (25 pin D-sub) provides the following functions:
• Serial data communication
Interface type: RS-232C full duplex, DCE
Parameters: 1200 Baud, 1 start bit, 8 data bits, 2 stop bits, no parity
Pin assignments:
Pin 1 Protective ground
Pin 2 Data in
Pin 3 Data out
Pin 7 Data ground
2
When the instrument is used for continuous auto-sampling, the estimated life of the gold film sensor decreases and
the sensor will become a maintenance item. For example, sensor life is reduced to approximately six months if the
instrument is run continuously with a 30-minute sample interval and a 48-hour regeneration interval or reduced to
three months when using a 15-minute sample interval and a 24-hour regeneration interval.
Potential interferences to the Jerome® hydrogen sulfide analyzers are rare and most of these can be
eliminated with proper maintenance procedures. However, erroneously high readings can
sometimes occur. Here are a few things to be aware of when using the instrument:
The gold film sensors used in the Jerome® hydrogen sulfide analyzers do not respond to the
following compounds:
• Hydrocarbons
• CO, CO2, and SO2
• Water vapor (Note that water vapor condensation on the gold film can cause
irreparable harm to the sensor and must be avoided.)
However, the following compounds may cause the gold film sensor to respond:
• Chlorine
• Ammonia
• NO2
• Most mercaptans (organic sulfur compounds or “thiols”)
Special filters designed to remove chlorine or ammonia gas are available from Arizona Instrument
and may be ordered as Chlorine Filter, AZI P/N Z2600-3940 or Ammonia Filter, AZI P/N 990-
0183. Visit the “Tech Notes” section at www.azic.com for more information concerning the
chlorine and ammonia filters.
Filter replacement at regular intervals, or when unexpectedly high readings are encountered in
areas of these potential interferents, may resolve these problems.
Y631 0901 631 Accessory Kit (See pictures beginning on page 32)
1400 2002 Probe
1400 3010 Tubing Adapter, 1/4” to 1/8”
2300 0001 Trimmer Tool
2600 3039 0.25 Fritware
6000 4003 Line Cord, 115 VAC - USA and Canada
Alt. 200-0003 Line Cord, 220-240 VAC - England
Alt. 200-0008 Line Cord, 220-240 VAC - Europe
Z2600 3905 Zero Air Filter
Y631 0905 631 Maintenance Kit (See pictures beginning on page 32)
345-0050 1' of 1/8” Tygon® clear tubing
345-0244 2' of 1/16” Tygon® clear tubing
345-0257 6” of 1/16” Tygon® Fluran black tubing
2600 3039 0.25 inch fritware
Z2600 3905 Zero Air Filter
Z2600 3930 Scrubber Filter
Z2600 3933 LFS Scrubber Filter
Z2600 3934 LFD Scrubber Filter
Z4000 0907 Battery Pack Assembly
Note: The Battery Pack Assembly for 220V / XE models is a different part number and must be
ordered separately:
Z4000 0908 Battery Pack Assembly (220V / XE models)
Page 30 of 50 AZI Customer Service 800-528-7411 or 602-470-1414
Jerome® Data Logger & JCS
Includes the external Jerome®
Data Logger and Jerome®
Y990-0259 Communication Software
(JCS) Kit (see below)
Y990-0258
For customers with prior
(software
version of the JCS.
upgrade only)
Jerome® Communication
6000 1055
Cable
For current prices and delivery information, call AZI Customer Service at
(800) 528-7411 or (602) 470-1414.
Service includes filter replacement, component testing, and instrument calibration to NIST
traceable standards.
The Jerome® Hydrogen Sulfide Functional Test Module (FTM) provides a fast and easy method of
verifying that Jerome® 631-X Hydrogen Sulfide Analyzers are functioning correctly.
Simple Operation
The Functional Test Module includes a permeation tube containing hydrogen sulfide. When
activated, the test module releases this H2S from the permeation tube at a specific, known
concentration. The H2S flows over the gold film sensor of the Jerome® analyzer, which then
measures the amount of exposure to the gas. The flow rate and temperature of this release are
factory set to provide a concentration of approximately 250 ppb (0.250 ppm) ±20% when using
FTM Z2600 0918 or approximately 30 ppb ± 20% when using the Low-Level FTM (Z2600 0930).
The user then compares the reading on the Jerome® analyzer with the known concentration from
the module. If the H2S level shown on the analyzer’s display falls within the expected range for
the FTM being used, the instrument is functioning properly. If the level is not in the expected
range, it should be returned to the factory for NIST-traceable calibration.
See page 30 for a list of the components that make up the FTM and its accessory kit.
The FTM, with the exception of the permeation tube, carries a limited one-year warranty to be free
from defects or workmanship. The permeation tube is warranted for 90 days. Refer to the FTM
Operation Manual AZI P/N 700-0095 for complete operation and warranty information.
The Jerome® Communications Software (JCS) is used with 631-X Hydrogen Sulfide Analyzers
that feature the communications configuration option, available in both SMV and Non-SMV
instruments.
• The JCS allows the user to program the instrument for unattended monitoring and to
download recorded data stored in the Jerome® Data Logger.
• Automatic sampling can be initiated every one (1) to sixty (60) minutes with programmable
audible alarm levels.
The Jerome® Communications Software (JCS) operates with the Jerome® 431-X Mercury Vapor
and Jerome® 631-X Hydrogen Sulfide Analyzers that have the “Communications Configuration”
option installed. The software can control instrument sampling for unattended continuous
operation, collect data, graph this data in real time and perform statistical analysis.
The software can also program the Jerome® Data Logger. This optional accessory enables data
storage during manual sampling or portable automatic sampling without being attached to a
computer. The Data Logger initiates automatic sampling, triggers alarms and stores data. The
logged data may then be downloaded to the computer when it is convenient. The Data Logger
stores up to 1,000 data points. On SMV units with Data Logger functionality, this functionality is
integrated into the instrument, while Non-SMV units use an external Data Logger (AZI# 6100
0010) that attaches to the back of the instrument.
Before using this software, familiarization with the operation of the Jerome® Hydrogen Sulfide
Analyzer or Mercury Vapor Analyzer is important. Also, prior to installation of this software you
should be familiar with the personal computer and operating system you are using. If you have
any questions about how to proceed, call AZI Customer Service at (800) 528-7411 or (602) 470-
1414 or send an e-mail to [email protected] for assistance.
System Requirements
• Jerome® 631-X with the “Communications Option.” These Jerome® instruments have a
DB-25 connector and related internal hardware and firmware.
• Windows® 7 or 8
• At least one free serial port (or two free USB ports if using a RS-232/USB converter)
• One free USB port
The software can also program the Jerome® Data Logger used with the Jerome® analyzer. The
computer programs the Data Logger that either attaches to the DB-25 connector on the rear of
Non-SMV instruments or is integrated into the instrument in SMV instruments with Data Logger
functionality. The Data Logger initiates automatic sampling, triggers alarms and stores data. This
optional accessory enables portable automatic sampling without a dedicated computer.
The DIP switch identified as SW2 on the 631-X control board is located at the top center of the board.
CAUTION:
Switch the instrument’s power to OFF before opening the instrument
and changing DIP switch settings.
On Non-SMV instruments, the Option Functionality is provided by the Option Circuit Board
mounted on the Main Circuit Board. On SMV instruments equipped with the Option
Functionality, the Option Functionality is integrated into the Main Circuit Board.
Proper use of this board requires that the base instrument be fully functional and set correctly for
the intended operation.
DIP Switch
SW 100
Jumper JMP3
(may be behind
ribbon cable)
NOTE: SMV units do not have R101 or equivalent component.
Auto-Zero
With the Option Functionality installed, the 631-X has a limited auto-zero function. This function
cannot be disabled and is transparent to the user. The instrument can be manually zeroed as
described in “Zero Adjust” on page 13. However, if the instrument is to be operated by personnel
not familiar with the procedure or if it is operated unattended, the auto-zero function should
satisfactorily zero the unit after each sensor regeneration.
Page 40 of 50 AZI Customer Service 800-528-7411 or 602-470-1414
Instrument Zeroing
The Jerome® 631-X has three ways to zero the sensor reading before samples are taken if the
Option Functionality is installed.
(1) The instrument automatically re-zeroes between samples so that each sample is a unique
reading. To take a sample, simply press the SAMPLE button.
(2) The manually adjusted zero, using the switch on the top of the 631-X is used to re-establish a
baseline between the reference and sensor gold films only after a sensor regeneration. This
zero is manually adjusted by pressing the ZERO button and turning the potentiometer on the
top of the instrument until the display reads 0. Adjust only after sensor regeneration; it is
normal for H to be displayed after sampling.
(3) The 631-X Option Functionality provides an auto-zero feature following regeneration that is
invisible to the user.
• In some cases, the instrument cannot resume sampling after regeneration. .L.L.L appears
on the display when the ZERO button is pressed and the error message “manual bridge
adjust needed” is added to the notes column of the JCS text file when the JCS is used. If
this problem persists, it may be necessary to re-set the auto-zero.
• When necessary to re-adjust the auto-zero point:
Ensure the instrument has been regenerated and 30 minutes have passed since the
regeneration completed before proceeding.
Turn the instrument off.
Make a note of the original DIP switch settings of SW100 on the Option Circuit
Board (Non-SMV units) or on the Main Circuit Board (SMV units).
On the Main Circuit Board DIP switch SW2, turn DIP switch 4 to ON.
Set the DIP switch SW100, to 1,2,6 OFF; 3,4,5 ON.
Turn the instrument ON.
Press and hold the ZERO button and adjust the potentiometer on top of the
instrument until the number 20 is displayed, then release the ZERO button.
Non-SMV units only:
Switch SW100 DIP #1 from OFF to ON three times, leaving it set to ON. (i.e.
starting from OFF, switch it ON, OFF, ON, OFF, ON).
Press and hold the ZERO button while turning the potentiometer on the option
board until the number 20 is displayed. Note the display may flicker one digit.
All units: Return all switches to their original position.
NOTE: The higher the auto-zero number, the lower the sensor capacity and the more sensor
regenerations are needed.
If the unit is to be operated unattended for extended periods, AZI recommends that the sensor be
regenerated regularly. Operation under JCS or Data Logger control automatically regenerates
saturated sensors. Regeneration will not occur as shown when sample streams have a very low
concentration of H2S. The Option Functionality can control regeneration on a regular basis, every
6, 12 or 24 hours.
The regeneration intervals are set through a combination of switch settings as shown in the
following table:
Auto-Sample
If a Data Logger is either not connected (on Non-SMV units), not activated (on SMV units) or is
operating in the manual sampling mode the following automatic sampling rates may be selected
with SW100 DIP switch settings:
This auto-sample function will not function if a Data Logger is connected and operating in
automatic sampler mode programmed through the JCS.
The analog output signal at pin 18 of the 25 pin connector can be configured to provide the
instrument's native mode 0-2 Volt output or the optional 4-20 mA output by setting a single
jumper. Refer to the tables below for jumper placement. (Pin 23 is the ground pin for the analog
output function. Pin 18 is positive with respect to the ground pin).
• The 0-2 Volt output circuit can drive loads of 10K ohms or higher.
• The 4-20 mA output is a passive transmitter and requires the connected receiver to supply
between 10 and 28 volts DC.
The 631-X must have the auto ranging feature disabled in order to get accurate analog output
readings. The approximate range of the H2S concentration must be known before the instrument
can be set into that specific range (0, 1, 2 or 3). The analog output signal is based on each
individual range and not the entire range (0-50 ppm).
Note that neither analog output circuit is floating. The negative terminals of both circuits are
connected to the instrument's common ground buss.
Example Calculations:
• Example 1: Locked in Range 1 (0.10 to 1.00 ppm)
o 631-X reading Current
0.10 ppm or less 4mA
1.00 ppm 20mA
An external three-way solenoid can be used to provide fresh air or conditioned air during sensor
regeneration. This may be necessary if the sample stream lacks molecular oxygen. A low current
six volt DC solenoid, connected between pins 19 and 11 of the 25 pin rear panel connector, will be
energized during the regeneration cycle if the Option Functionality switch SW100 #6 is placed in
the OFF position.
If needed, the circuit may be built from the following components and configured as shown in the
following diagram. It will only function if the 631-X instrument has the Option Functionality.
* These are types not stocked by AZI, but should be available overnight from many AMP stocking
distributors such as Digi-Key Corporation. There are multiple suitable alternatives such as Radio
Shack’s 276-1547 and 276-1549.
TO INSTRUMENT TO SAMPLE
SOURCE
TO FRESH AIR
1/16" TUBE SOURCE
PIN 1 PIN 1
Instruments with the 631-X Option Functionality can be used with any +12 VDC source for
continuous operation, if the AZI Power Inverter Kit, P/N Y031 0902 is purchased. To preserve
the life of the DC power source, usually a car or truck battery, the power inverter will switch on
automatically to supply the AC necessary for regeneration only. The external switch on the
inverter should always be OFF to preserve battery life during normal sampling.
To work with the power inverter kit, place Option Functionality switch SW100 DIP #6 to the ON
position.
Installation
• Ensure that the instrument’s Option Functionality switches are set correctly for the intended
operation with the SW100 DIP #6 set to “ON” for DC operation.
• Mount the DC Power Adaptor board (AZI# 1000 0089) to the rear of the instrument and
tighten the mounting screws.
o On Non-SMV instruments, mount the external Data Logger on the Adaptor board.
• Place or mount the DC/AC power inverter in a secure position near the instrument.
• Connect the cable from the DC/AC power inverter to the matching connecter on the
interface board. Note that the connectors are keyed to prevent improper connection.
• Plug the instrument’s AC power cord into the power inverter and connect it to the
instrument.
When the instrument starts a regeneration with Option Functionality switch SW100 DIP #6 ON,
the instrument sends a signal to close the relay on the DC Power Adaptor board. This switches the
power inverter ON using the inverter’s internal switch.
NOTE: When this mode is enabled, Non-SMV instruments do NOT check for 115 VAC for the
regeneration. If there is no AC power to the instrument, and a regeneration is initiated, the
instrument will flash .H.H.H (rather than .P.P.P), however the sensor will not heat, nor will the
sensor be cleaned.
• Due to the wide variety of applicable DC power sources, the battery wires are not supplied.
Refer to the manual supplied with the inverter for proper battery wire sizing and
connections.
• Connect cables from the external 12-volt power source and the DC power cable assembly to
the appropriate positive (+) and negative (-) terminals on the inverter as shown in the
diagram above.
• Connect the yellow wire from the DC power cable to the “REMOTE” terminal on the
power inverter as shown in the diagram above.
• If the external 12volt lines are not powered, power them now. (Connect them to the
battery)
• Connect the instrument’s AC power cord between the instrument and
the front of the power inverter.
• Turn the instrument “ON.” (Note, the external 12V supply will also
charge the instrument internal battery).
• Press the “REGEN” switch on the instrument. Inverter operation can
be verified in either of two ways:
Immediately after pressing “REGEN” the inverter will intermittently
“sing.” This tone slowly becomes nearly continuous and then ends
after 64 seconds.
If the area is noisy, use a voltmeter to verify that approximately 115
volts is present for about 64 seconds, starting when the “REGEN”
switch is pressed.
• Allow the instrument to complete its regeneration before turning it off.
• With the instrument turned off, complete the installation (i.e. connect or activate Data
Logger, communications cables, or other devices and ensure that the DIP switches for the
instrument and Option Functionality are set correctly).
Arizona Instrument LLC (seller) warrants to buyer that Jerome® products delivered pursuant to
this agreement shall, at the time of delivery, and for a period of one (1) year thereafter (the Internal
Battery Pack, where applicable, is warranted for a period of ninety [90] days only), to be free from
defects in material or workmanship and shall conform to seller's specifications or such other
specifications as seller has agreed to in writing. Seller's obligations with respect to claims under
this warranty shall be limited, at seller's option, either to the replacement of defective or non-
conforming product or to an appropriate credit for the purchase price thereof subject to the
provisions of seller's Warranty Policy as amended from time to time, said Policy being
incorporated herein by reference. All defective parts replaced by AZI become the property of
AZI.
Returned products under warranty claims will be shipped to seller’s plant by buyer at buyer's
expense and shall be accompanied by a statement of the reason for the return and an approved
Return Material Authorization Number issued by seller. Buyer remains responsible for payment
for products not accepted for warranty adjustment, handling costs, and freight costs associated
therewith.
Notwithstanding the foregoing, no warranty shall be enforceable in the event that product has been
subjected to environmental or stress testing by buyer or any third party without written approval of
seller prior to such testing. Further, no warranty shall be enforceable if the alleged defect is found
to have occurred because of misuse, neglect, improper installation, repair, alteration, accident, or
improper return handling procedure by buyer.
Notwithstanding the foregoing, if any product covered by order(s) placed hereunder is designated
as “developmental,” “prototype” or “experimental,” no warranty whatsoever except a warranty of
title to component materials, will be applicable thereto and buyer shall indemnify seller for any
claims for liability asserted seller in connection therewith.
The foregoing state the entire liability of seller in connection with products supplied hereunder.
If you have any questions regarding the operation of this instrument, please call our toll free
number (800) 528-7411. Internationally, call (602) 470-1414 or fax (480) 804-0656.