T700-T700U NVS Manual-083730700
T700-T700U NVS Manual-083730700
TRADEMARKS
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document are the property of their respective owners and are used herein for identification
purposes only.
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators vii
IMPORTANT SAFETY INFORMATION
Important safety messages are provided throughout this manual for the purpose of avoiding personal injury or
instrument damage. Please read these messages carefully. Each safety message is associated with a safety alert
symbol, and are placed throughout this manual and inside the instrument. The symbols with messages are defined
as follows:
Electrical Ground: This symbol inside the instrument marks the central
safety grounding point for the instrument.
CAUTION
This instrument should only be used for the purpose and in the manner
described in this manual. If you use this instrument in a manner other
than that for which it was intended, unpredictable behavior could ensue
with possible hazardous consequences.
viii Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
CONSIGNES DE SÉCURITÉ
Des consignes de sécurité importantes sont fournies tout au long du présent manuel dans le but d’éviter des
blessures corporelles ou d’endommager les instruments. Veuillez lire attentivement ces consignes. Chaque
consigne de sécurité est représentée par un pictogramme d’alerte de sécurité; ces pictogrammes se retrouvent
dans ce manuel et à l’intérieur des instruments. Les symboles correspondent aux consignes suivantes :
MISE EN GARDE
Cet instrument doit être utilisé aux fins décrites et de la manière décrite dans ce
manuel. Si vous utilisez cet instrument d’une autre manière que celle pour
laquelle il a été prévu, l’instrument pourrait se comporter de façon imprévisible
et entraîner des conséquences dangereuses.
NE JAMAIS utiliser un analyseur de gaz pour échantillonner des gaz
combustibles!
xii Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
2.5.5. Utilities ................................................................................................................................................. 82
2.5.5.1. Datalog View ................................................................................................................................ 82
2.5.5.2. Alerts Log ..................................................................................................................................... 82
2.5.5.3. USB Utilities (Downloads and Updates) ....................................................................................... 82
2.5.5.4. Diagnostics ................................................................................................................................... 85
2.5.6. Setup .................................................................................................................................................... 85
2.6. Setup Menu: Features/Functions Configuration ........................................................................................ 85
2.6.1. Setup>Data Logging (Data Acquisition System, DAS) ........................................................................ 86
2.6.1.1. Configuring Trigger Types: Periodic ............................................................................................. 87
2.6.1.2. Configuring Trigger Types: Conditional ....................................................................................... 88
2.6.1.3. Downloading DAS (Data Acquisition System) Data ..................................................................... 88
2.6.2. Setup>Events ...................................................................................................................................... 89
2.6.3. Setup>Dashboard ................................................................................................................................ 91
2.6.4. Setup>Vars: Internal Variables ............................................................................................................ 91
2.6.5. Setup>Homescreen ............................................................................................................................. 92
2.6.6. Setup>Digital (Status) Outputs ............................................................................................................ 92
2.6.7. Setup>Sequences: Automatic Calibration Operations ........................................................................ 93
2.6.7.1. Setting Up Control Inputs for a Sequence .................................................................................... 95
2.6.7.2. Setting Up Control Outputs for a Sequence ................................................................................. 96
2.6.7.3. Parameters for the Step Types .................................................................................................... 97
2.6.7.4. Deleting or Editing Sequences or Individual Steps in a Sequence .............................................. 97
2.6.8. Setup > Levels: Setting up and using LEADS (Dasibi) Operating Levels ........................................... 98
2.6.8.1. General Information about LEADS Levels ................................................................................... 98
2.6.8.2. Dot commands ............................................................................................................................. 98
2.6.8.3. Programming, Editing, and Activating Levels ............................................................................... 99
2.6.8.4. Programming Levels..................................................................................................................... 99
2.6.8.5. Editing/Deleting Levels ............................................................................................................... 100
2.6.8.6. Activating Levels ......................................................................................................................... 100
2.6.9. Setup > Analog Output ...................................................................................................................... 100
2.6.9.1. Analog Output Voltage Range Configuration ............................................................................. 102
2.6.9.2. Adding a Recorder Offset ........................................................................................................... 102
2.6.9.3. Analog Output Channel Calibration ............................................................................................ 102
2.6.10. Setup > Instrument .......................................................................................................................... 103
2.6.11. Setup > Comm: Communications Ports .......................................................................................... 104
2.6.11.1. COM1/COM2 ............................................................................................................................ 104
2.6.11.2. TCP Port1 ................................................................................................................................. 105
2.6.11.3. TCP Port2 ................................................................................................................................. 105
2.6.11.4. Network Settings ...................................................................................................................... 105
2.6.12. Setup>Gas ....................................................................................................................................... 105
2.7. Transferring Configuration to Other Instruments ...................................................................................... 106
3. OPERATING MODES, BASIC OPERATION, AND CONFIGURATIONS ........................ 107
3.1. STANDBY MODE...................................................................................................................................... 108
3.2. GENERATE MODE ................................................................................................................................... 109
3.2.1. GENERATE > AUTO: Basic Generation of Calibration Mixtures ...................................................... 112
3.2.2. GENERATE > MANUAL: Generating Calibration Mixtures Manually................................................ 114
3.2.2.1. Determining the Source Gas Flow Rate ..................................................................................... 116
3.2.2.2. Determining Diluent Flow Rate ................................................................................................... 117
3.2.2.3. Determining Diluent Flow Rate with O3 Generator Option Installed........................................... 117
3.2.2.4. Setting Source Gas and Diluent Flow Rates Using the GENERATE > MANual Menu.............. 118
3.2.3. GENERATE > PURGE: Activating the Calibrator’s Purge Feature ................................................... 118
3.2.4. GENERATE: Gas Phase Titration (GPT) Calibration ........................................................................ 119
3.2.4.1. Meeting the USEPA Guidelines for GPT calibration .................................................................. 119
3.2.4.2. GPT Theory ................................................................................................................................ 120
3.2.4.3. Determining the Total Flow for GPT Calibration Mixtures .......................................................... 120
3.2.5. GENERATE > GPTZ: Performing a Gas Phase Titration Zero ........................................................ 121
3.2.5.1. GPTZ vs Auto Generate Modes ................................................................................................. 122
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators xiii
3.2.5.2. Calibrator GPTZ Operation ........................................................................................................ 122
3.2.5.3. Initiating a GPTZ......................................................................................................................... 123
3.2.6. GENERATE > GPTPS: Performing a Gas Phase Titration Pre-Set .................................................. 123
3.2.6.1. Calibrator GPTPS Operation ...................................................................................................... 124
3.2.6.2. Initiating a GPTPS ...................................................................................................................... 126
3.2.7. GENERATE > GPT: Performing a Gas Phase Titration .................................................................... 126
3.2.7.1. Calibrator GPT Operation ........................................................................................................... 126
3.2.7.2. Initiating a GPT Calibration Gas Generation .............................................................................. 128
3.2.8. GENERATE > SEQUENCE ............................................................................................................... 129
3.2.9. GENERATE > LEVEL ........................................................................................................................ 129
4. COMMUNICATIONS AND REMOTE OPERATION ......................................................... 130
4.1. Data Terminal/Communication Equipment (DTE DCE) ............................................................................ 130
4.2. Modes, Baud Rate and Serial Communication ......................................................................................... 130
4.2.1. Serial Communication: RS-232 ......................................................................................................... 130
4.2.2. Serial Communication: RS-485 (Option) ........................................................................................... 131
4.3. Ethernet ..................................................................................................................................................... 131
4.4. MODBUS Communications Protocol ........................................................................................................ 131
4.4.1.1. MODBUS Com Port Configuration ............................................................................................. 132
5. CALIBRATION AND VERIFICATION .............................................................................. 134
5.1. Verifying and Calibrating the MFCs .......................................................................................................... 134
5.1.1. Setup for Verifying and Calibrating the MFCs ................................................................................... 135
5.1.2. Verifying and Calibrating the MFCs ................................................................................................... 136
5.2. Verifying and Calibrating the O3 Photometer (Bench) Option ................................................................... 137
5.2.1. Setup for Verifying O3 Photometer (Option) Performance ................................................................. 138
5.2.2. Verifying O3 Photometer (Option) Performance ................................................................................ 138
5.2.3. Setup for Calibrating the O3 Photometer (Bench) Option .................................................................. 139
5.2.3.1. Setup Using Direct Connections ................................................................................................ 140
5.2.3.2. Setup Using a Calibration Manifold ............................................................................................ 141
5.2.3.3. Calibration Manifold Exhaust/Vent Line Requirements .............................................................. 141
5.2.4. Performing O3 Photometer (Option) Calibrations .............................................................................. 142
5.2.5. O3 Photometer Gas Flow Calibration ................................................................................................. 143
5.2.6. O3 Photometer Back Pressure Compensation Calibration ................................................................ 143
5.3. Verifying and Calibrating the O3 Generator Option ................................................................................... 144
5.3.1. Setup for Verification and Calibration the O3 Generator .................................................................... 144
5.3.2. Verifying O3 Generator Performance with External Photometer ....................................................... 144
5.3.3. O3 Generator Option with Photometer Calibration Procedure ........................................................... 145
5.4. Verifying and Calibrating the Gas Pressure Sensors................................................................................ 145
5.4.1.1. Calibrating Diluent, Cal Gas, or Opt O3 Generator Pressure Sensors ....................................... 147
5.4.1.2. Calibrating the Photometer (Option) Sample Gas Pressure Sensor .......................................... 148
6. MAINTENANCE 149
6.1. Maintenance Schedule .............................................................................................................................. 149
6.2. Operational Health Checks ....................................................................................................................... 151
6.3. Software/Firmware Updates ...................................................................................................................... 152
6.3.1. Remote Updates ................................................................................................................................ 152
6.3.2. Manual Reload/Update Procedures................................................................................................... 152
6.3.3. Instrument Display Calibration (for earlier instruments ...................................................................... 153
6.4. Time Zone Changes .................................................................................................................................. 154
6.5. Maintenance Procedures .......................................................................................................................... 155
6.5.1. Auto Leak Check................................................................................................................................ 155
6.5.1.1. Equipment Required ................................................................................................................... 155
6.5.1.2. Setup for Auto Leak Check ........................................................................................................ 155
6.5.1.3. Returning the Calibrator to Service after Performing an Auto Leak Check................................ 159
6.5.2. Cleaning or Replacing the Absorption Tube ...................................................................................... 159
6.5.3. UV Source Lamp Adjustment ............................................................................................................ 160
6.5.4. UV Source Lamp Replacement ......................................................................................................... 161
xiv Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
6.5.5. Ozone Generator UV Lamp Adjustment or Replacement ................................................................. 162
7. TROUBLESHOOTING AND SERVICE ............................................................................ 163
7.1. General Troubleshooting ........................................................................................................................... 163
7.1.1. Fault Diagnosis with Alerts ................................................................................................................ 164
7.1.2. Fault Diagnosis With Dashboard Functions ...................................................................................... 165
7.1.3. Using the Signals for Diagnostic ........................................................................................................ 167
7.1.4. Using the Analog Outputs Menu ........................................................................................................ 167
7.2. Using the Internal Electronic Status LEDs ................................................................................................ 169
7.2.1. CPU Status Indicator ......................................................................................................................... 169
7.2.2. Relay PCA Status LEDs .................................................................................................................... 170
7.2.2.1. I2C Bus Watchdog Status LEDs ................................................................................................. 170
7.2.2.2. O3 Option Status LEDs ............................................................................................................... 170
7.2.3. Valve Driver PCA STATUS LEDs ...................................................................................................... 171
7.3. Subsystem Checkout ................................................................................................................................ 173
7.3.1. Verify Subsystem Calibration ............................................................................................................. 173
7.3.2. AC Main Power .................................................................................................................................. 173
7.3.3. DC Power Supply............................................................................................................................... 174
7.3.4. I2C Bus ............................................................................................................................................... 175
7.3.5. Touchscreen Interface ....................................................................................................................... 175
7.3.6. LCD Display Module .......................................................................................................................... 175
7.3.7. Relay PCA ......................................................................................................................................... 176
7.3.8. Valve Driver PCA ............................................................................................................................... 176
7.3.9. Input Gas Pressure / Flow Sensor Assembly .................................................................................... 176
7.3.9.1. Basic PCA Operation.................................................................................................................. 176
7.3.9.2. Cal Gas Pressure Sensor ........................................................................................................... 176
7.3.9.3. Diluent Pressure Sensor............................................................................................................. 177
7.3.10. Photometer O3 Generator Pressure/Flow Sensor Assembly........................................................... 177
7.3.10.1. Basic PCA operation ................................................................................................................ 177
7.3.10.2. Photometer Pressure Sensor ................................................................................................... 177
7.3.10.3. O3 Generator Pressure Sensor ................................................................................................ 178
7.3.10.4. Photometer Flow Sensor .......................................................................................................... 178
7.3.11. Motherboard..................................................................................................................................... 178
7.3.11.1. A/D Functions ........................................................................................................................... 178
7.3.11.2. Analog Outputs Voltage Test ................................................................................................... 179
7.3.11.3. Digital (Status) Outputs ............................................................................................................ 180
7.3.11.4. Digital Control Inputs ................................................................................................................ 180
7.3.11.5. Control Outputs ........................................................................................................................ 181
7.3.12. CPU ................................................................................................................................................. 181
7.3.13. The Calibrator Doesn’t Appear on the Lan or Internet..................................................................... 182
7.3.14. RS-232 Communications ................................................................................................................. 182
7.3.14.1. General RS-232 Troubleshooting............................................................................................. 182
7.3.15. Temperature Problems .................................................................................................................... 182
7.3.15.1. Box / Chassis Temperature ...................................................................................................... 183
7.3.15.2. Photometer Option Sample Chamber Temperature ................................................................ 183
7.3.15.3. UV Lamp Temperature ............................................................................................................. 183
7.3.15.4. Ozone Generator Temperature ................................................................................................ 183
7.4. TroubleShooting the Optional O3 Photometer .......................................................................................... 184
7.4.1. Dynamic Problems with the Optional O3 Photometer ........................................................................ 184
7.4.1.1. Noisy or Unstable O3 Readings at Zero ..................................................................................... 184
7.4.1.2. Noisy, Unstable, or Non-Linear Span O3 Readings ................................................................... 184
7.4.1.3. Slow Response to Changes in Concentration ............................................................................ 185
7.4.1.4. The Analog Output Signal Level Does Not Agree With Front Panel Readings.......................... 185
7.4.1.5. Cannot Zero ................................................................................................................................ 185
7.4.1.6. Cannot Span ............................................................................................................................... 185
7.4.2. Checking The UV Lamp Power Supply ............................................................................................. 186
7.5. TroubleShooting the Optional O3 generator .............................................................................................. 187
xvi Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
LIST OF FIGURES
Figure 2-1. Calibrator Front Panel Layout .............................................................................................................. 32
Figure 2-2. Calibrator Rear Panel Layout ............................................................................................................... 33
Figure 2-3. Internal Layout, T700 Base Unit .......................................................................................................... 35
Figure 2-4. Internal Layout with O3 Generator and Photometer (options in T700, standard in T700U) ................. 36
Figure 2-5. Calibrator Analog Output Connector .................................................................................................... 38
Figure 2-6. Status Output Connector...................................................................................................................... 39
Figure 2-7. Calibrator Digital Control Input Connectors ......................................................................................... 40
Figure 2-8. Calibrator Digital Control Output Connector ........................................................................................ 41
Figure 2-9. Calibrator Rear Panel Valve Driver Installed (with PSM connected to JP1) ........................................ 42
Figure 2-10. Calibrator Rear Panel Valve Driver Installed (without PSM).............................................................. 42
Figure 2-11. Valve-Driver Interface ........................................................................................................................ 43
Figure 2-12. Option 48C Connections, Customer-supplied PSM to Pin 12 (+) & Pin 9 (-) .................................... 43
Figure 2-13. Option 48E Connections .................................................................................................................... 43
Figure 2-14. Rear Panel Connector Pin-Outs for RS-232 Mode ............................................................................ 45
Figure 2-15. Default Pin Assignments for CPU COMM Port Connector (RS-232). ............................................... 45
Figure 2-16. Jumper and Cables for Multidrop Mode ............................................................................................. 48
Figure 2-17. RS-232-Multidrop PCA Host/Analyzer Interconnect Diagram ........................................................... 49
Figure 2-18. Setup – Connecting the Basic Calibrator to a Sample Manifold ........................................................ 52
Figure 2-19. Setup – Connecting the Calibrator to a Sample Manifold .................................................................. 53
Figure 2-20. Setup – Connecting the Calibrator to a Calibration Manifold ............................................................. 54
Figure 2-21. Setup – Connecting the Calibrator to a Dual Span Gas / Zero Air Manifold...................................... 55
Figure 2-22. T700 Calibrator Pneumatic Diagram – Base Unit .............................................................................. 56
Figure 2-23. T700 Pneumatics for Calibrator with Optional O3 Generator and GPT Chamber ............................. 57
Figure 2-24. Pneumatics for T700U or for T700 with O3 Generator and Photometer Options .............................. 59
Figure 2-25. T700 Basic Calibrator with Multiple Calibration Gas MFCs ............................................................... 61
Figure 2-26. Pneumatics with AllOptions Installed (T700U, 3rd MFC; T700, O3 Generator, Photometer, and GPT
Chamber)........................................................................................................................................... 62
Figure 2-27. Permeation Tube Gas Generator Option ........................................................................................... 63
Figure 2-28. Pneumatic Flow with Permeation Generator ..................................................................................... 64
Figure 2-29. Rear Panel with Dual Output Option .................................................................................................. 67
Figure 2-30. T700 Internal Pneumatics with Optional Dual Gas Output (NOy – Special) ...................................... 68
Figure 2-31. T700U Pneumatic Diagram, with Dual Output and Three MFC Options ........................................... 68
Figure 2-32. Status Screens at Startup .................................................................................................................. 69
Figure 2-33. Typical Home Page Prior to Configuration......................................................................................... 69
Figure 2-34. Viewing Active Alerts Page ................................................................................................................ 70
Figure 2-35. Sample Dashboard Page ................................................................................................................... 71
Figure 2-36. Dashboard Configurator ..................................................................................................................... 71
Figure 2-37. Calibration Gas Inlet Ports Setup ....................................................................................................... 72
Figure 2-38. User Interface Orientation .................................................................................................................. 78
Figure 2-39. Dashboard Page ................................................................................................................................ 79
Figure 2-40. Viewing a Live Plot from Dashboard Page ........................................................................................ 79
Figure 2-41. Navigating to the Active Alerts Page.................................................................................................. 80
Figure 2-42. Active Alerts Cleared.......................................................................................................................... 81
Figure 2-43. Generate Page ................................................................................................................................... 81
Figure 2-44. USB Utilities Pages ............................................................................................................................ 82
Figure 2-45. DAS Download Page ......................................................................................................................... 83
Figure 2-46. Configuration Transfer ....................................................................................................................... 84
Figure 2-47. Sample Diagnostics Menu (differs by calibrator configuration) ......................................................... 85
Figure 2-48. Data Log Configuration ...................................................................................................................... 86
Figure 2-49. Datalog Periodic Trigger Configuration .............................................................................................. 87
Figure 2-50. Datalog - Conditional Trigger Configuration ...................................................................................... 88
Figure 2-51. USB Utility Page................................................................................................................................. 88
Figure 2-52. DAS Data Download .......................................................................................................................... 89
Figure 2-53. Events List .......................................................................................................................................... 89
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators xvii
Figure 2-54. Event Configuration............................................................................................................................ 90
Figure 2-55. Dashboard Configuration ................................................................................................................... 91
Figure 2-56. Vars Configuration ............................................................................................................................. 91
Figure 2-57. Homescreen Configuration ................................................................................................................ 92
Figure 2-58. Digital Outputs Setup ......................................................................................................................... 92
Figure 2-59. Sequence Configuration .................................................................................................................... 95
Figure 2-60. Sequence CC Inputs Setup Page ...................................................................................................... 96
Figure 2-61. Sequence CC Outputs Setup Page ................................................................................................... 97
Figure 2-62. Levels Programming and Editing ..................................................................................................... 100
Figure 2-63. Analog Output Configuration ............................................................................................................ 101
Figure 2-64. Setup for Calibrating the Analog Output Signals ............................................................................. 103
Figure 2-65. Communications Configuration, Network Settings .......................................................................... 105
Figure 2-66. Configuration Transfer ..................................................................................................................... 106
Figure 3-1. Gas Flow with O3 Generator and Photometer Options during Standby Mode .................................. 109
Figure 3-2. Gas Flow through Basic Calibrator in Generate Mode ...................................................................... 110
Figure 3-3. T700U Gas Flow and T700 with O3 Options when Generating Non-O3 Source Gas ........................ 111
Figure 3-4. T700U Gas Flow and T700 with O3 Options when Generating O3 .................................................... 111
Figure 3-5. Modes in the Generate Menu ............................................................................................................ 112
Figure 3-6. Auto Generate Calibration Mixtures ................................................................................................... 113
Figure 3-7. Generate>Manual Menu .................................................................................................................... 114
Figure 3-8. Generate>Manual with Ozone Generator .......................................................................................... 115
Figure 3-9. Gas Flow with O3 Options during Purge mode .................................................................................. 119
Figure 3-10. Gas Flow during GPTZ Mode .......................................................................................................... 123
Figure 3-11. Gas Flow during GPTPS Mode ........................................................................................................ 125
Figure 3-12. Gas Flow during GPT Mode ............................................................................................................ 127
Figure 4-1. MODBUS via Ethernet ....................................................................................................................... 132
Figure 4-2. MODBUS via Serial Communication (example) ................................................................................ 133
Figure 5-1. MFC Performance Statistics .............................................................................................................. 134
Figure 5-2. Location of MFC Outlet Ports ............................................................................................................. 136
Figure 5-3. MFC Calibration ................................................................................................................................. 137
Figure 5-4. Set up for Verifying Optional O3 Photometer Performance ............................................................... 138
Figure 5-5. O3 Photometer Performance Verification ........................................................................................... 139
Figure 5-6. External Photometer Validation Setup – Direct Connections ............................................................ 140
Figure 5-7. External Photometer Validation Setup with Calibration Manifolds ..................................................... 141
Figure 5-8. Bench Cal Page ................................................................................................................................. 142
Figure 5-9. Photometer Flow Calibration Screen ................................................................................................. 143
Figure 5-10. O3 Generator Calibration Setup – Direct Connections .................................................................... 144
Figure 5-11. Pressure Monitor Points in Basic Unit.............................................................................................. 146
Figure 5-12. Pressure Monitor Points with O3 Options and Multiple Cal MFCs Installed .................................... 146
Figure 5-13. Pressure Sensor Calibration Page (Diluent Example) ..................................................................... 147
Figure 5-14. O3 Photometer Pressure Sensor Calibration Page ......................................................................... 148
Figure 6-1. Report Generation Page .................................................................................................................... 151
Figure 6-2. Remote Update Page......................................................................................................................... 152
Figure 6-3. General Utilities Page ........................................................................................................................ 152
Figure 6-4. Touchscreen Calibration Page ........................................................................................................... 153
Figure 6-5. Time Zone Change Requirements ..................................................................................................... 154
Figure 6-6. Bypassing the Photometer Sensor PCA and Pump .......................................................................... 156
Figure 6-7. Gas Port Setup for Auto-Leak Check Procedure ............................................................................... 157
Figure 6-8. Gas Flow for Auto-Leak Check of Base Model Calibrators ............................................................... 158
Figure 6-9. Gas Flow for Auto-Leak Check of Calibrators with O3 Generator and Photometer Option ............... 158
Figure 6-10. Photometer Assembly – Lamp Adjustment / Installation ................................................................. 160
Figure 6-11. O3 Generator UV Lamp Location ..................................................................................................... 162
Figure 7-1. CPU Status Indicator.......................................................................................................................... 169
Figure 7-2. Relay PCA Status LEDS Used for Troubleshooting .......................................................................... 170
Figure 7-3. Valve Driver PCA Status LEDS Used for Troubleshooting ................................................................ 171
Figure 7-4. Location of DC Power Test Points on Relay PCA ............................................................................. 174
xviii Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
Figure 7-5. Analog Outputs Page Example .......................................................................................................... 179
Figure 8-1. Location of Gas Flow Control Assemblies with O3 Generator Installed ............................................. 194
Figure 8-2. Flow Control Assembly & Critical Flow Orifice ................................................................................... 195
Figure 8-3. Electronic Block Diagram ................................................................................................................... 196
Figure 8-4. Calibrator CPU Board Annotated ....................................................................................................... 198
Figure 8-5. Relay PCA .......................................................................................................................................... 199
Figure 8-6. Heater Control Loop Block Diagram. ................................................................................................. 200
Figure 8-7. Status LED Locations – Relay PCA ................................................................................................... 200
Figure 8-8. Status LED Locations – Valve Driver PCA ........................................................................................ 202
Figure 8-9. Power Distribution Block Diagram ..................................................................................................... 205
Figure 8-10. Front Panel Display Interface Block Diagram .................................................................................. 206
Figure 8-11. Schematic of Basic Software Operation .......................................................................................... 207
Figure 8-12. O3 Generator Internal Pneumatics ................................................................................................... 208
Figure 8-13. O3 Generator Valve and Gas Fixture Locations............................................................................... 210
Figure 8-14. O3 Generator – Electronic Block Diagram ....................................................................................... 211
Figure 8-15. O3 Generator Electronic Components Location ............................................................................... 211
Figure 8-16. O3 Generator Temperature Thermistor and DC Heater Locations .................................................. 212
Figure 8-17. O3 Photometer Gas Flow – Measure Cycle ..................................................................................... 215
Figure 8-18. O3 Photometer Gas Flow – Reference Cycle .................................................................................. 215
Figure 8-19. O3 Photometer Absorption Path ....................................................................................................... 216
Figure 8-20. O3 Photometer Layout – Top Cover Removed ................................................................................ 217
Figure 8-21. O3 Photometer Electronic Block Diagram ........................................................................................ 218
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators xix
LIST OF TABLES
Table 1-1. Calibrator Options ................................................................................................................................. 23
Table 1-2. T700 Dilution System Specifications ..................................................................................................... 25
Table 1-3. T700 Electrical and Physical Specifications .......................................................................................... 26
Table 1-4. T700 Optional Ozone (O3) Generator** Specifications ......................................................................... 26
Table 1-5. T700 Optional UV Photometer Specifications ....................................................................................... 27
Table 1-6. T700U Dilution System Specifications .................................................................................................. 27
Table 1-7. T700U NO2 Generation (GPT modes) Specifications ........................................................................... 27
Table 1-8. T700U Ozone Generator Module Specifications .................................................................................. 27
Table 1-9. T700U UV Photometer Option Specifications ....................................................................................... 28
Table 1-10. T700U Electrical and Physical Specifications ..................................................................................... 28
Table 2-1. Instrument Ventilation Clearance Requirements .................................................................................. 31
Table 2-2. Rear Panel Description ......................................................................................................................... 34
Table 2-3. Status Output Pin Assignments ............................................................................................................ 39
Table 2-4. Calibrator Control Input Pin Assignments ............................................................................................. 40
Table 2-5. Calibrator Control Output Pin Assignments .......................................................................................... 41
Table 2-6. External Valve Driver Options ............................................................................................................... 42
Table 2-7. Operating Mode Valve States for Calibrator with O3 Generator ........................................................... 57
Table 2-8. Operating Mode Valve States for Standard T700U or for T700 with O3 Generator and Photometer
Options .............................................................................................................................................. 59
Table 2-9. Calibrator Gas Types ............................................................................................................................ 73
Table 2-10. Calibrator Units of Measure List .......................................................................................................... 73
Table 2-11. Menu Overview ................................................................................................................................... 75
Table 2-12. Calibration Sequences Configuration Attributes ................................................................................. 93
Table 2-13. Analog Output Voltage Range Min/Max ............................................................................................ 102
Table 2-14. Voltage Tolerances for the Analog Output Calibration...................................................................... 103
Table 2-15. COM1/COM2 Configuration .............................................................................................................. 104
Table 2-16. LAN/Ethernet Configuration Properties ............................................................................................. 105
Table 3-1. Calibrator Operating Modes ................................................................................................................ 107
Table 3-2. Status of Internal Pneumatics during STANDBY Mode ...................................................................... 108
Table 3-3. Status of Internal Pneumatics During Generate Mode ....................................................................... 110
Table 3-4. Internal Pneumatics during Purge Mode ............................................................................................. 118
Table 3-5. Status of Internal Pneumatics during GENERATE > GPTZ Mode ..................................................... 122
Table 3-6. Status of Internal Pneumatics during GENERATE > GPTPS Mode ................................................... 124
Table 3-7. Status of Internal Pneumatics during GENERATE > GPT Mode ........................................................ 126
Table 4-1. Ethernet Status Indicators ................................................................................................................... 131
Table 5-1. Examples of MFC Calibration Points .................................................................................................. 135
Table 5-2. Calibrator Pressure Sensor Calibration Setup .................................................................................... 145
Table 6-1. Maintenance Schedule ........................................................................................................................ 150
Table 7-1. Warning Messages in Alerts Page ...................................................................................................... 164
Table 7-2. Test Functions – Indicated Failures .................................................................................................... 166
Table 7-3. DIAG – Analog Output Functions ........................................................................................................ 168
Table 7-4. Dashboard Readings as Diagnostic Tools .......................................................................................... 168
Table 7-5. Relay PCA Watchdog LED Failure Indications ................................................................................... 170
Table 7-6. Relay PCA Status LED Failure Indications ......................................................................................... 170
Table 7-7. Valve Driver Board Watchdog LED Failure Indications ...................................................................... 171
Table 7-8. Relay PCA Status LED Failure Indications ......................................................................................... 172
Table 7-9. DC Power Test Point and Wiring Color Codes ................................................................................... 174
Table 7-10. DC Power Supply Acceptable Levels ................................................................................................ 175
Table 7-11. Relay PCA Control Devices .............................................................................................................. 176
Table 7-12. Analog Output Test Function - Nominal Values Voltage Outputs ..................................................... 179
Table 7-13. Calibrator Control Input Pin Assignments and Digital Inputs Panel .................................................. 180
Table 7-14. Control Outputs Pin Assignments and Functions Check .................................................................. 181
Table 8-1. Relay PCA Status LEDs ...................................................................................................................... 201
Table 8-2. Calibrator Photometer Measurement / Reference Cycle .................................................................... 214
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators xxi
1. INTRODUCTION, SPECIFICATIONS AND APPROVALS
This Section provides an overview of the Dynamic Dilution Calibrator, its features, and its
options.
1.2. FEATURES
Some of the exceptional features of your calibrator are:
• Advanced T-Series electronics
• LCD color graphics display with touch screen interface
• Microprocessor control for versatility
• Bi-directional USB (optional), RS-232, optional RS-485, and
10/100Base-T Ethernet for remote operation
1.3. OPTIONS
The options available for your analyzer are presented in Table 1-1 with name, option
number, a description and/or comments, and if applicable, cross-references to technical
details in this manual, such as setup and calibration. To order these options or to learn more
about them, please contact the Sales Department of Teledyne API at:
TOLL-FREE: +1 800-324-5190
PHONE: +1 858-657-9800
FAX: +1 858-657-9816
EMAIL: [email protected]
WEBSITE: http://www.teledyne-api.com/
* Can select two Cylinder Gas ranges with 3rd MFC Option for wider dynamic range
1.6.1. SAFETY
IEC/EN 61010-1:2010 (3rd Edition), Safety requirements for electrical equipment for
measurement, control, and laboratory use.
CE: 2006/95/EU, Low-Voltage Directive
1.6.2. EMC
EN 61326-1 (IEC 61326-1), Class A Emissions/Industrial Immunity
FCC 47 CFR Part 15B, Class A Emissions
CE: 2004/108/EU, Electromagnetic Compatibility Directive
2.1. UNPACKING
CAUTION – RISK OF PERSONAL INJURY
The calibrator weighs about 18 kg (40 pounds) without options installed. To avoid
personal injury, always use two persons to lift and carry the calibrator.
WARNING!
Never disconnect electronic circuit boards, wiring harnesses or electronic
subassemblies while the unit is under power.
Various rack mount kits are available for this instrument. See Table 1-1 of this manual for
more information.
1 2 3 4 5 6 7 8 D +
User-selectable
User-selectable
User-selectable
User-selectable
User-selectable
User-selectable
User-selectable
User-selectable
EMITTER BUSS
+ 5 VDC
CALIBRATOR
INTERNAL GROUND
Figure 2-6. Status Output Connector
Digital Ground The ground level from the calibrator’s internal DC power supplies.
CONTROL Bit-01
CONTROL Bit-02
CONTROL Bit-03
CONTROL Bit-04
CONTROL Bit-05
CONTROL Bit-06
CONTROL Bit-01
CONTROL Bit-02
CONTROL Bit-03
CONTROL Bit-04
CONTROL Bit-05
CONTROL Bit-06
1 2 3 4 5 6 U + 1 2 3 4 5 6 U +
7 8 9 10 11 12 U + 7 8 9 10 11 12 U +
CONTROL Bit-07
CONTROL Bit-08
CONTROL Bit-09
CONTROL Bit-10
CONTROL Bit-11
CONTROL Bit-12
CONTROL Bit-07
CONTROL Bit-08
CONTROL Bit-09
CONTROL Bit-10
CONTROL Bit-11
CONTROL Bit-12
- 5 VDC Power +
Supply
There are two methods for energizing the control inputs. The internal +5V available from
the pin labeled “+” is the most convenient method. However, if full isolation is required,
an external 5 VDC power supply should be used.
CONTROL OUT
1 2 3 4 5 6 7 8 9 10 11 12 E
Digital Ground The ground level from the calibrator’s internal DC power supplies.
Figure 2-10. Calibrator Rear Panel Valve Driver Installed (without PSM)
Depending upon the capacity of the external supply either four (standard) or eight valves
can be simultaneously energized.
The PCA is constructed such that it plugs through the rear panel into the Control Output
connector, J1008, on the calibrator’s motherboard.
Figure 2-12. Option 48C Connections, Customer-supplied PSM to Pin 12 (+) & Pin 9 (-)
ETHERNET CONNECTION
For network or Internet communication with the analyzer, connect an Ethernet cable from
the analyzer’s rear panel Ethernet interface connector to an Ethernet port. Although the
analyzer is shipped with DHCP enabled by default, it should be manually assigned a static
IP address (Setup>Comm>Network Settings, Section 2.6.11.4).
Note If this option is installed, the rear panel RS232 (COM2) port cannot
be used for anything other than Multidrop communication.
RS-232 CONNECTION
For RS-232 communications with data terminal equipment (DTE) or with data
communication equipment (DCE) connect either a DB9-female-to-DB9-female cable
(Teledyne API part number WR000077) or a DB9-female-to-DB25-male cable (Option
60A), as applicable, from the analyzer’s rear panel RS-232 port to the device. Adjust the
DCE-DTE switch (Figure 2-2) to select DTE or DCE as appropriate (Section 4.1).
The signals from these two connectors are routed from the motherboard via a wiring
harness to two 10-pin connectors on the CPU card, J11 and J12 (Figure 2-15).
Figure 2-15. Default Pin Assignments for CPU COMM Port Connector (RS-232).
P/N WR000024, a DB-9 female to DB-25 male cable. Allows connection to the most
common styles of modems (e.g. Hayes-compatible) and code activated switches.
Both cables are configured with straight-through wiring and should require no additional
adapters
To assist in properly connecting the serial ports to either a computer or a modem, there are
activity indicators just above the RS-232 port. Once a cable is connected between the
analyzer and a computer or modem, both the red and green LEDs should be on.
• If the lights are not lit, locate the small switch on the rear panel to switch
it between DTE and DCE modes.
• If both LEDs are still not illuminated, ensure that the cable properly
constructed.
Note Because the RS-232 Multidrop option uses both the RS232
and COM2 DB9 connectors on the analyzer’s rear panel to
connect the chain of instruments, COM2 port is no longer
available for separate RS-232 or RS-485 operation.
In each instrument with the Multidrop option there is a shunt jumpering two pins on the
serial Multidrop and LVDS printed circuit assembly (PCA), as shown in Figure 2-16. This
shunt must be removed from all instruments except that designated as last in the multidrop
chain, which must remain terminated. This requires powering off and opening each
instrument and making the following adjustments:
1. With NO power to the instrument, remove its top cover and lay the rear panel open
for access to the Multidrop/LVDS PCA, which is seated on the CPU.
2. On the Multidrop/LVDS PCA’s JP2 connector, remove the shunt that jumpers Pins
21 ↔ 22 as indicated in Figure 2-16. (Do this for all but the last instrument in the
chain where the shunt should remain at Pins 21 ↔ 22).
3. Check that the following cable connections are made in all instruments (again refer
to Figure 2-16):
• J3 on the Multidrop/LVDS PCA to the CPU’s COM1 connector
(Be aware that the CPU’s COM2 connector is not used in Multidrop)
• J4 on the Multidrop/LVDS PCA to J12 on the motherboard
• J1 on the Multidrop/LVDS PCS to the front panel LCD
5. Referring to Figure 2-17, use straight-through DB9 male > DB9 female cables to
interconnect the host RS232 port to the first analyzer’s RS232 port. Do the same
from the first analyzer’s COM2 port to the second analyzer’s RS232 port, and from
the second analyzer’s COM2 port to the third analyzer’s RS232 port, etc. Connect
in this fashion up to eight analyzers, subject to the distance limitations of the RS-
232 standard.
6. On the rear panel of each analyzer, adjust the DCE DTE switch (see Figure
2-2 and Section 4.1) so that the green and the red LEDs (RX and TX) of the
COM1 connector (labeled RS232) are both lit. (Ensure you are using the
correct RS-232 cables internally wired specifically for RS-232
communication; see Table 1-1, “Communication Cables” and Section 2.3.1.7,
Connecting the Communications Interfaces, “RS-232 Connection”).
Ensure jumper is
installed between
JP2 pins 21 ↔ 22 in
last instrument of
multidrop chain.
7. BEFORE communicating from the host, power on the instruments and check that
the Machine ID code is unique for each:
c. Once changed, press the Enter button to accept the new ID for that instrument.
8. Next, in the Setup>Comm>>COM1 menu (do not use the COM2 menu for
multidrop), use the Edit button to set COM1 Quiet Mode and COM1 Multidrop to
ENABLED; then press the Accept button.
9. Also check the COM1 Baud Rate to ensure it reads the same for all instruments
(edit as needed and press the Accept button).
CYL1 VENT
CYL2 CAL OUT
CYL3 Sample Inlet
CAL OUT
CYL4
Teledyne API
Mass Flow Gas Analyzer
DILUENT IN
Calibrator
Enclosure Wall
Teledyne API Sample Inlet
CAL
MODEL 701
SOURCE Zero Gas Generator
GAS Teledyne API
Gas Analyzer
If no second Instrument is connected
to this outlet, it MUST be capped
To determine if the gas flow on the vent line is ≥ 5 SLPM, subtract the gas flow for each
instrument connected to the outlets of the calibrator from the TOTAL FLOW setting for
the calibrator (see Section 2.4.5).
If the calibrator has the optional O3 photometer installed remember that this option requires
800 cc/min (0.8 LPM) of additional flow (see Section 2.4.5 or Figure 2-24).
EXAMPLE. Your system has two analyzers each requiring 2 SLPM of cal gas flow, and
the calibrator includes the O3 photometer. If the TOTAL FLOW rate for the
calibrator is set at 10 SLPM:
Therefore, the vent would require a gas line with an O.D. 3/8 inch.
SAMPLING CANE
FILTER SCREEN
BLOWER / PUMP
SAMPLE
MANIFOLD
TEE
H2O TRAP
CAL OUT
CYL2 Teledyne API
CYL3 Gas Analyzer
VENT
CYL4
Mass Flow
DILUENT IN
Calibrator
VENT & extra
CAL OUT Teledyne API MODEL
gas outlets
MUST be capped 701
Zero Gas Generator CAL
SOURCE
GAS
SAMPLING CANE
FILTER SCREEN
BLOWER / PUMP
SAMPLE
MANIFOLD
TEE
H2O TRAP
Sample Inlet
CYL1 VENT
Sample Inlet
CYL2
CAL OUT
Span Gas Inlet
CYL3
CAL OUT
CYL4 Zero Air Inlet
Teledyne API
Mass Flow Gas Analyzer
DILUENT IN
Calibrator
Teledyne API
CAL
MODEL 701
SOURCE Zero Gas Generator CALIBRATION
GAS MANIFOLD If Gas flow on this line is ≥ 5 SLPM
the minimum O.D. must be 3/8 inch
T700 output flow rate must be greater than 5 SLPM.
Minimum O.D. must be 3/8 inch
SAMPLE
ROOF MANIFOLD VENT TO OUTSIDE OF ROOM
TEE
H2O TRAP
Sample Inlet
Exhaust
Exhaust
CYL1 VENT
Span Gas Inlet
CYL2
CAL OUT
CYL3 Zero Air Inlet
CAL OUT Teledyne API
CYL4 1 Gas Analyzer
Mass Flow
DILUENT IN
Calibrator
SPAN CAL MANIFOLD
CAL 1
Teledyne API
SOURCE MODEL 701 ZERO CAL MANIFOLD
GAS Zero Gas Generator
5 SLPM
If Gas flow on these lines is ≥ 5 SLPM
1 the minimum O.D. must be 3/8 inch
Figure 2-21. Setup – Connecting the Calibrator to a Dual Span Gas / Zero Air Manifold
Instrument Chassis
Purge
Valve PHOTOMETER
brn ZERO OUT
DILUENT
PRESSURE SENSOR
Diluent
Mass Flow Controller
PCA
The standard calibrator is equipped with one calibration gas mass flow controller (flow rate
0 – 100 cm3/min) and one diluent gas mass flow controller (flow rate 0-10 LPM). See Table
1-1 for the various flow rate options.
GENERATOR
O3 GAS INPUT
(option)
O3 Generator Assembly
PRESSURE SENSOR
O3
Pressure O3 GEN / PHOTOMETER
Regulator
PRESSURE / FLOW SENSOR PCA
DILUENT grn
INLET grn
(100 cm3/min)
Flow Control
DILUENT
Valve brn
On Back Panel
PHOTOMETER
Purge brn INLET
Valve
brn
DILUENT blk PHOTOMETER
ZERO IN
PRESSURE SENSOR
Valve PHOTOMETER
Mass Flow Controller ZERO OUT
PCA
red
CAL GAS 2
INLET
CAL GAS blk
EXHAUST
PRESSURE
CAL GAS 3 SENSOR blu
INLET GPT
orn PHOTOMETER
Valve OUTLET
GPT blu
Volume blu
VENT
Figure 2-23. T700 Pneumatics for Calibrator with Optional O3 Generator and GPT Chamber
Table 2-7. Operating Mode Valve States for Calibrator with O3 Generator
VALVES MFCS
(X = CLOSED; O = OPEN)
MODE
CYL CYL CYL O3
CYL2 PURGE DILUENT GPT CAL1 CAL21 DILUENT
1 3 4 GEN
Flow Control
PHOTOMETER BENCH
(1.0 LPM) (option)
gry
O3 FLOW
SENSOR
Pressure
Regulator O3 GAS INPUT
PRESSURE SENSOR
GENERATOR
DILUENT
O3 Generator Assembly
INLET grn grn PHOTOMETER
(option)
PRESSURE SENSOR On Back Panel
DILUENT
O3
Valve O3 GEN / PHOTOMETER
PRESSURE / FLOW SENSOR PCA vio PHOTOMETER
INLET
brn
Flow Control REF/MEAS vio
Valve
(800 cm3)
Flow Control
Purge brn brn
(100 cm3)
Valve
wht
DILUENT Diluent PUMP wht PHOTOMETER
PRESSURE SENSOR
PHOTOMETER
O3 Gen
PCA
ZERO OUT
Valve gry
CAL GAS 2
INLET
INTERNAL
CAL GAS blk VENT
PRESSURE red
CAL GAS 3 SENSOR
blk
INLET EXHAUST
GPT
orn
Valve
CAL GAS 4
orn
PHOTOMETER
INLET OUTLET
yel
yel red
GAS INPUT MANIFOLD yel
(on back panel) yel CAL GAS
Cal Gas OUTPUT 1
Mass Flow Controller 1
CAL GAS
GPT blu
OUTPUT 2
Volume
VENT
blu
GAS OUTPUT MANIFOLD
Figure 2-24. Pneumatics for T700U or for T700 with O3 Generator and Photometer Options
Table 2-8. Operating Mode Valve States for Standard T700U or for T700 with O3 Generator and
Photometer Options
VALVES MFCS
PHOT
(X = CLOSED; O = OPEN) PUMP
GAS TYPE
CYL CYL CYL CYL O3
PURGE DILUENT GPT PHOT M/R CAL1 CAL21 DILUENT
1 2 3 4 GEN
Generate
Source Gas
O2 O2 O2 O2 X O X X Reference Phase ON3 ON3 ON OFF
2.3.2.11. T700 PNEUMATIC FLOW FOR MULTIPLE CALIBRATION SOURCE GAS MFCS
When the optional third mass flow controller is installed, the calibrator has both calibration
gas MFCs on the same gas stream, installed in parallel (see Figure 2-25 and Figure 2-26).
The calibrator turns on the MFC with the lowest flow rate that can accommodate the
requested flow and can therefore supply the most accurate flow control. When a flow rate
is requested that is higher than the highest rated MFC (but lower than their combined
maximum flow rating), both controllers are activated.
EXAMPLE:
• Calibrator with one calibration gas MFC configured for 0-5 LPM:
Maximum gas flow = 5 LPM
Minimum gas flow = 500 cm3/min
• Calibrator with two calibration gas MFCs configured for 0-1 LPM and 0-
5 LPM:
Calibration gas flow rates:
5.001 to 6.000 LPM; both MFCs active
1.001 LPM – 5.000 LPM; High MFC active;
0.100 LPM – 1.000 LPM; Low MFC active
While the values for the MFC actual and target flows (i.e., Cal Flow Actual; Cal Flow
Targ) show the sum of all the active MFCs flows, the value for the MFC pressure applies
to only one MFC, not the sum as it is assumed that gas pressure is the same for all MFCs.
(Use the Setup>Dashboard menu to display the flows and pressure).
PRESSURE SENSOR
PRESSURE Cal Gas
CAL GAS 1 SENSOR Mass Flow Controller 1
INPUT GAS
INLET EXHAUST
PCA
yel
yel
Figure 2-25. T700 Basic Calibrator with Multiple Calibration Gas MFCs
O3 FLOW
Pressure
SENSOR
Regulator O3 GAS INPUT
PRESSURE SENSOR
DILUENT grn
GENERATOR
O3 Generator Assembly
INLET PHOTOMETER
grn On Back Panel
PRESSURE SENSOR
DILUENT
O3
Valve O3 GEN / PHOTOMETER
brn PRESSURE / FLOW SENSOR PCA vio PHOTOMETER
INLET
Flow Control REF/MEAS vio
Valve
(800 cm 3)
Flow Control
Purge brn
(10 cm 3)
Valve
wht
brn
DILUENT PUMP wht PHOTOMETER
PRESSURE SENSOR
CAL GAS 4
orn GPT
INLET Valve
yel
yel PHOTOMETER
GAS INPUT MANIFOLD yel OUTLET
(on back panel)
CAL GAS
Cal Gas red OUTPUT 1
Mass Flow Controller 2
yel
CAL GAS
GPT blu
OUTPUT 2
Volume
VENT
blu
yel GAS OUTPUT MANIFOLD
yel
Figure 2-26. Pneumatics with All Options Installed (T700U, 3rd MFC; T700, O3 Generator, Photometer, and
GPT Chamber)
Perm Tube
Oven
Optional
Desorber
PHOTOMETER BENCH
Pressure
Regulator
Flow Control
(1.0 LPM)
gry
grn
O3 FLOW
SENSOR
O3 GAS INPUT
PRESSURE SENSOR
GENERATOR
O3 Generator Assembly
INLET grn Control PRESSURE SENSOR
(100 cm3)
DILUENT Diluent O3 GEN / PHOTOMETER On Back Panel
O3
Valve Mass Flow Controller Perm Tube PRESSURE / FLOW SENSOR PCA
Oven vio vio
REF/MEAS PHOTOMETER
(option) INLET
Valve
brn
Flow Control
Permeation (800 cm3)
Flow Control
Purge Tube
(100 cm3)
Valve
PUMP
DILUENT wht wht PHOTOMETER
PRESSURE SENSOR
Valve PHOTOMETER
O3 Gen
PCA
ZERO OUT
Valve gry
CAL GAS 2
INLET
blk INTERNAL
CAL GAS VENT
PRESSURE GPT red
CAL GAS 3 SENSOR Valve blk
INLET EXHAUST
CAL GAS
GPT blu OUTPUT 2
Volume
VENT
blu
GAS OUTPUT MANIFOLD
2. Set the Perm 1 Flow (this should be done with the flow standard connected at the
outlet of the perm tube oven).
3. Select a gas for the Perm1 Gas (the name of the gas produced by the permeation
tube generator MUST be different from the name of any bottled gas connected to
the calibrator).
4. Set the Perm 1 Rate for specific output (or elution rate).
24.46
Km = , where 24.46 is the molar volume in liters @ 25°C
MW
and MW is the molecular weight.
760mmHg . Km for SO2 = 0.382, NO2 = 0.532, H2S = 0.719, and NH3 =
1.436.
F = total flow rate (sum of 100 cm3/min and diluent flow), LPM.
C = concentration, ppm.
P 24.46
Thus, C= ×
F MW
Where, Temperature at 50°C = 323
Note This output cannot be used for ozone generation using the
photometer feedback. It can be used for standard dilution
calibrations as well as GPT using ozone.
When the dual gas output option is enabled, the output must be selected when generating
gas. In the Generate menu, select A or B in the Output field to select the output for
calibration.
Figure 2-30 depicts the pneumatic flow for the Calibrator with the optional dual gas output
at the output valve.
Figure 2-31. T700U Pneumatic Diagram, with Dual Output and Three MFC Options
Repeat the above steps for each of the Calibrator’s four gas inlet ports. If no gas is present
on a particular port, leave it set at the default setting of NONE.
Note The minimum total flow should equal 150% of the flow
requirements of all of the instruments to which the
calibrator will be supplying calibration gas.
Example: If the calibrator is expected to supply calibration
gas mixtures simultaneously to a system composed of
three analyzers, each requiring 2 LPM, the proper Total
Flow output should be set at:
(2 + 2 + 2) x 1.5 = 9.000 LPM
Note Set the TOTAL FLOW rate between 10% and 100% (avoid
<10% or >100%) of the diluent MFC’s full scale rating.
Note The last page on display prior to drilling into a menu remains on
display until a choice in the menu is selected.
Three of the dashboard parameters can be set up for continuous display as meters located
below the concentration display of the Home page through the Setup>Homescreen menu
(Section 2.6.5).
2.5.4. GENERATE
The Generate menu provides the ability to:
• Generate either ozone or zero air
• Execute a Sequence (configured in the Setup menu)
• Execute a Level (configured in the Setup menu)
• Place the instrument into Standby mode (suspend generating gas)
The Generate menu is presented in Section 3.2. To configure Sequences, see
Section 2.6.7or to configure Levels, see Section 2.6.8
2. To copy the data to the flash drive, press the Start button next to “Download DAS Data
from Instrument.” (The Cancel button will be enabled).
3. When complete, as indicated in the Status field, the Cancel button becomes the Done
button: press Done and then remove the flash drive.
UPDATING FIRMWARE
It is possible to check for firmware updates, reload current firmware, and to update
firmware remotely. Because this is a maintenance item and there is more than one way to
implement an update, instructions are provided in Section 6.3.
GENERATING A REPORT
The Report page is used typically for monitoring the functionality of the instrument. A new
report is generated every 24 hours and can be downloaded, and it can be uploaded to a
Cloud service for TAPI Technical Support. Because it is used in maintenance and
troubleshooting, the Report feature is presented in Section 6.2.
Note Some Diagnostics items do not appear in the menu unless the
instrument has been placed in Standby mode (Home>Generate
menu).
2.5.6. SETUP
The Setup menu is used to configure the instrument’s software features, gather information
on the instrument’s performance, and configure and access data from the Datalogger, the
instrument’s internal data acquisition system (DAS). Section 2.6 provides details for the
menus under Setup.
8. Press USB Utilities menu to open the utility page (Figure 2-51).
9. Insert a flash drive into a front panel USB port and wait for the Status field to
indicate that the drive has been detected and available buttons are enabled
(Figure 2-52).
10. To copy the data to the flash drive, press the Start button next to “Download
DAS Data from Instrument.” (The Cancel button will be enabled).
11. Wait for the Status field to indicate that the transfer is complete and the Cancel
button becomes the Done button.
12. Press the Done button; then remove the flash drive.
(The Update Firmware field is for checking for and installing firmware updates when the
instrument is connected to the Internet, and is presented in Section 6.2. The
Upload/Download Configuration field is for transferring instrument configuration from/to
other instruments, and is presented in Section 2.7).
2.6.2. SETUP>EVENTS
Events are occurrences that relate to any operating function, and will trigger Alerts
(Section 2.5.3). Events can provide diagnostic information about the instrument, typically
referred to as “Warnings”, or they can provide additional instrument functionality, such as
concentration alarms. The instrument comes from the factory with a number of pre-defined
warning Events, while the Setup>Events Configuration page provides the capability to
create additional, user-defined Events. Events are listed in the Events page (Figure 2-53)
under the Setup menu.
Note Last in = first out: the last step input into the program during
configuration under “Edit Steps” is the first step executed, which
means that multiple steps must be input in their reverse order;
advanced planning is recommended.
Note When the start time is set for a date/time that has passed,
the sequence will properly calculate the next run time
based on that past date/time.
100 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
2. In the Min Max fields input the minimum and maximum values for the slected
function’s range.
3. In the Calibration Type field, select either AUTO or MANUAL.
• AUTO sets the software to automatically calibrate not only the user-
selected Signal Out function, but also the available MFCs.
• MANUAL allows fine and coarse adjustments when calibrating the user-
selected Signal Out function.
4. In the Range field* select the desired full-scale value of the signal output (see
Section 2.6.9.1).
5. In the Recorder Offset field* input a bipolar voltage offset if needed to
compensate for noise (see Section 2.6.9.2). This field is not available when
Range is set to Current loop.
6. For the Allow Overrange box, either check to allow ± 5% overrange, or leave
blank if your recording device is sensitive to excess voltage or current.
7. Press the Apply button.
8. Go to the Analog Output Cal menu to calibrate the new settings (see
Section 2.6.9.3).
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 101
2.6.9.1. ANALOG OUTPUT VOLTAGE RANGE CONFIGURATION
In its standard configuration, the analog outputs is set to output a 0 – 5 VDC signals. Several
other output ranges are available (see Table 2-13). Each range is usable from -5% to + 5%
of the rated span.
102 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
V OUT + V IN +
V OUT - V IN -
Recording
ANALYZER
Device
Adjust the signal levels of the analog output in the Setup>Analog Outputs>Analog Output
Cal menu.
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 103
2.6.11. SETUP > COMM: COMMUNICATIONS PORTS
This menu is for specifying the various communications configurations.
2.6.11.1. COM1/COM2
Configure the instrument’s COM1 or COM2 ports to operate in modes listed in Table 2-15.
Table 2-15. COM1/COM2 Configuration
MODE DESCRIPTION
Baud Rate Set the baud rate for the COM1 or COM2 port being configured.
Command Prompt
Enable/disable a command prompt to be displayed when in terminal mode.
Display
Data Bits Set the data bits to 7 or 8 (typically set in conjunction with Parity and Stop bits).
Echo and Line
Enable/disable character echoing and line editing.
Editing
Choose SOFTWARE handshaking for data flow control (do NOT use
SOFTWARE handshaking mode when using MODBUS RTU for Protocol mode;
select only HARDWARE or OFF for MODBUS RTU),
Handshaking Mode or HARDWARE for CTS/RTS style hardwired transmission handshaking. (This
style of data transmission handshaking is commonly used with modems or
terminal emulation protocols).
Or choose to turn OFF handshaking.
Hardware Error
Enable/disable hardware error checking.
Checking
Enable/disable the hardware First In – First Out (FIFO) for improving data transfer
Hardware FIFO
rate for that COM port.
Modem Connection Select either a modem connection or a direct cable connection.
Modem Init String Input an initialization string to enable the modem to communicate.
Enable/disable multidrop mode for multi-instrument configuration on a single
Multidrop communications channel. Multidrop requires a unique ID for each instrument in
the chain (Setup>Vars>Instrument ID).
Select odd, or even, or no parity (typically set in conjunction with Data Bits and
Parity
Stop Bits).
Select among the communications protocols: TAPI, MODBUS RTU, or MODBUS
Protocol
ASCII (MODBUS: Section 4.4)
Enable/disable Quiet mode, which suppresses any feedback from the analyzer
(such as warning messages) to the remote device and is typically used when the
Quiet Mode port is communicating with a computer program where such intermittent
messages might cause communication problems.
Such feedback is still available but a command must be issued to receive them.
Enable/disable the rear panel COM2 Port for RS-485 communication. RS-485
RS-485 mode has precedence over Multidrop mode if both are enabled. Also, RS-485
configuration disables the rear panel USB port.
Enable/disable the requirement for a password for this serial port to respond. The
Security
only command that is active is the request-for-help command (? CR).
Stop bits Select either 0 or 1 stop bit (typically set in conjunction with Parity and Data bits).
104 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
2.6.11.2. TCP PORT1
TCP Port1 allows choosing whether or not to display the command prompt, editing the Port
1 number for defining the terminal control port by which terminal emulation software
addresses the instrument, such as Internet or NumaView™ Remote software, and enabling
or disabling security on this port.
2.6.12. SETUP>GAS
Gas configuration was detailed during the Startup procedures in Section 2.4.4.
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 105
2.7. TRANSFERRING CONFIGURATION TO OTHER INSTRUMENTS
Once an instrument is configured, the same configuration can be copied to other
instruments of the same Model.
106 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
3. OPERATING MODES, BASIC OPERATION, AND CONFIGURATIONS
This Section starts with a description of the basic modes of operation in order to begin
operation right away, and then provides configuration instructions for other functions.
Standby is the most common of the calibrator’s software operating modes (Section 3.1);
use this mode to configure the calibrator and perform other procedures. Generate is another
common mode (Section 3.2); use this mode produce calculated calibration gas mixtures.
Note that the ozone generator in the T700U can operate in a high range or a low range.
High range is similar to the standard T700 with an ozone generator option. Low range is
more like a fractional mode in that it is used for producing low levels of ozone during a
GPT calibration. The T700U low range operation is automatically invoked based on the O3
concentration and total flow specified, i.e., when O3 output is < 500 PPB*LPM.
Table 3-1 presents descriptions of the modes. Sections 3.1 through 3.2.9 provide details.
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 107
3.1. STANDBY MODE
When the calibrator is in Standby mode (Generate>Standby), it and all of its subsystems
(including the O3 generator and photometer options, if installed) are inactive, although
Dashboard functions and Alerts continuously update as displayed in the front panel. All
internal valves are closed except the diluent inlet valve. The mass flow controllers are also
turned off.
• Some functions are not available unless the instrument is in Standby
mode, e.g., Setup>Gas or Utilities>Diagnostics>Pressure Cal.
• Some functions that conflict with the accurate creation of calibration gas
mixtures automatically place the calibrator into Standby mode when
activated.
• The MFC pressures are not monitored in Standby mode since the MFCs
are turned OFF in this mode. This prevents erroneous Alerts from
appearing.
Table 3-2 shows the status of the calibrator’s various pneumatic components when the
calibrator is in Standby mode.
Standby X X X X X O D D
Reference
Phase
OFF OFF OFF OFF
1 Only present if multiple cal gas MFC option is installed.
108 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
Instrument Chassis
O3 FLOW
SENSOR
Pressure
Regulator O3 GAS INPUT
PRESSURE SENSOR
DILUENT
O3 Generator Assembly
GENERATOR
INLET grn PHOTOMETER
grn
PRESSURE SENSOR On Back Panel
DILUENT
O3
Valve O3 GEN / PHOTOMETER
PRESSURE / FLOW SENSOR PCA vio PHOTOMETER
INLET
brn
Flow Control REF/MEAS vio
OFF (800 cm3)
Valve
Flow Control
Purge brn brn
(100 cm3)
Valve
wht
PUMP
DILUENT Diluent OFF wht PHOTOMETER
PRESSURE SENSOR
O3 Gen PHOTOMETER
PCA
CAL GAS
GPT blu
OUTPUT 2
Volume
VENT
blu
GAS OUTPUT MANIFOLD
Figure 3-1. Gas Flow with O3 Generator and Photometer Options during Standby Mode
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 109
Instrument Chassis
brn
Purge
Valve PHOTOMETER
brn ZERO OUT
DILUENT
CAL GAS 1 PRESSURE SENSOR PRESSURE
INLET SENSOR EXHAUST
INPUT GAS
Diluent
Mass Flow Controller
PCA
Table 3-3 shows the status of the calibrator’s various pneumatic components when the
calibrator is in Generate mode:
Generate Reference
O2 O2 O2 O2 X O D D ON3 ON3 ON OFF
Source Gas Phase
110 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
Instrument Chassis
O3 FLOW
Pressure
SENSOR
Regulator O3 GAS INPUT
PRESSURE SENSOR
DILUENT
GENERATOR
O3 Generator Assembly
INLET grn PHOTOMETER
grn
PRESSURE SENSOR On Back Panel
DILUENT
O3
Valve O3 GEN / PHOTOMETER vio PHOTOMETER
brn PRESSURE / FLOW SENSOR PCA INLET
REF/MEAS
vio
Flow Control Valve
(800 cm3)
Flow Control
Purge brn brn
(100 cm3)
Valve wht
DILUENT Diluent OFF wht PHOTOMETER
PRESSURE SENSOR
O3 Gen
PCA
PHOTOMETER
CAL GAS 2 Valve
CAL GAS ZERO OUT
INLET gry
PRESSURE
SENSOR INTERNAL
red blk VENT
CAL GAS 3 blk
INLET EXHAUST
orn GPT
Valve
CAL GAS 4
orn
PHOTOMETER
INLET OUTLET
yel
yel red
GAS INPUT MANIFOLD yel
(on back panel) yel CAL GAS
Cal Gas OUTPUT 1
Mass Flow Controller 1
CAL GAS
GPT blu
OUTPUT 2
Volume
VENT
blu
GAS OUTPUT MANIFOLD
Figure 3-3. T700U Gas Flow and T700 with O3 Options when Generating Non-O3 Source Gas
Instrument Chassis
Pressure
Regulator O3 GAS INPUT
O3 FLOW
SENSOR
PRESSURE SENSOR
DILUENT
GENERATOR
O3 Generator Assembly
REF/MEAS vio
Flow Control Valve
ON (800 cm 3)
Flow Control
Valve
wht
DILUENT Diluent ON wht PHOTOMETER
PRESSURE SENSOR
O3 Gen
PCA
PHOTOMETER
CAL GAS 2 Valve
CAL GAS ZERO OUT
INLET gry
PRESSURE
SENSOR INTERNAL
red blk VENT
CAL GAS 3 blk
INLET EXHAUST
orn GPT
Valve
CAL GAS 4
orn OFF PHOTOMETER
INLET OUTLET
yel
yel red
GAS INPUT MANIFOLD yel
(on back panel) yel CAL GAS
Cal Gas OUTPUT 1
Mass Flow Controller 1
CAL GAS
GPT blu
OUTPUT 2
Volume
VENT
blu
GAS OUTPUT MANIFOLD
Figure 3-4. T700U Gas Flow and T700 with O3 Options when Generating O3
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 111
Modes in the Generate menu are illustrated in Figure 3-5, briefly described in Table 3-1,
and detailed in Sections 3.2.1 through 3.2.9.
112 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
Note In the T700U, when generating very low levels of ozone, care
must be taken to ensure that the concentration-flow product is
kept above the 20 ppb*LPM minimum value. This value is the
target concentration (in ppb) multiplied by the total flow value.
Example: To determine the minimum flow rate required to
generate 3 ppb:
3 ppb * X LPM > 20 ppb*LPM
or
X LPM > (20 ppb * LPM) / (3 ppb) = 6.7 LPM
Therefore, the flow rate should be a minimum of 6.7 LPM to
generate 3 ppb.
These equations can be used to determine the minimum flow
rate for any desired concentration.
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 113
Using this information, the Calibrator automatically calculates and sets the individual flow
rates for the Diluent and chosen component gases to create the desired calibration mixture.
In addition, if the Calibrator is equipped with the optional O3 Generator (with or without
optional Photometer), and O3 is to be included in the calibration mixture (e.g. using the
GPT or GPTPS features), the user also needs to set the ozone generator mode and set point
see Figure 3-8.
However, start with computations for the desired settings, as presented in this section.
114 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
Figure 3-8. Generate>Manual with Ozone Generator
Note The minimum total flow should equal 150% of the flow
requirements of all of the instruments to which the
calibrator will be supplying calibration gas.
Example: If the calibrator is to supply calibration gas
mixtures simultaneously to a system composed of three
analyzers, each requiring 2 LPM, the proper Total Flow
output should be set at: (2 + 2 + 2) x 1.5 = 9.000 LPM.
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 115
3.2.2.1. DETERMINING THE SOURCE GAS FLOW RATE
To determine the required flow rate of the component source gas, use the following
formula:
Equation 3-1
C f × Totalflow
GASflow =
Ci
WHERE:
Cf = target concentration of diluted gas
Ci = concentration of the source gas
GASflow = source gas flow rate
EXAMPLE:
• A target concentration of 200 ppm of SO2 is needed.
• The Concentration of the SO2 Source is 600 ppm
• The requirement of the system are 9.000 LPM
• The required source gas flow rate would be:
GASflow = (200 ppm x 9.000 LPM) ÷ 600 ppm
GASflow = 1800.000 ppm/LPM) ÷ 600 ppm
GASflow = 3.000 LPM
116 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
3.2.2.2. DETERMINING DILUENT FLOW RATE
To determine the required flow rate of the diluent gas use the following formula:
Equation 3-2
DILflow = Totalflow - GASflow
WHERE:
GASflow = source gas flow rate (from Equation 6-1)
Totalflow = total gas flow requirements of the system
DILflow = required diluent gas flow
EXAMPLE:
• If the requirement of the system is 9.000 LPM,
• The source gas flow rate is set at 3.00 LPM.
• The required source gas flow rate would be:
DILflow = 9.0 LPM – 3.0 LPM
DILflow = 6.0 LPM
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 117
3.2.2.4. SETTING SOURCE GAS AND DILUENT FLOW RATES USING THE
GENERATE > MANUAL MENU
After determining the flow values with the equations provided above, press the MANUAL
button and edit the flow values as needed for the Cal and Dil fields, respectively (Figure 3-7).
118 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
T700 Chassis
O3 FLOW
SENSOR
Pressure
Regulator O3 GAS INPUT
PRESSURE SENSOR
DILUENT
O3 Generator Assembly
GENERATOR
INLET grn PHOTOMETER
grn
PRESSURE SENSOR On Back Panel
DILUENT
O3
Valve O3 GEN / PHOTOMETER vio PHOTOMETER
brn PRESSURE / FLOW SENSOR PCA INLET
REF/MEAS vio
Flow Control Valve
(800 cm3)
Flow Control
Purge brn brn
(100 cm3)
Valve wht
DILUENT Diluent PUMP wht PHOTOMETER
PRESSURE SENSOR
O3 Gen
PCA
PHOTOMETER
CAL GAS 2 Valve
ZERO OUT
INLET gry
CAL GAS INTERNAL
PRESSURE red blk VENT
CAL GAS 3 SENSOR blk
INLET EXHAUST
GPT
orn
Valve
CAL GAS 4
orn
PHOTOMETER
INLET OUTLET
yel
yel red
GAS INPUT MANIFOLD yel
(on back panel) yel CAL GAS
Cal Gas OUTPUT 1
Mass Flow Controller 1
CAL GAS
GPT blu
OUTPUT 2
Volume
VENT
blu
GAS OUTPUT MANIFOLD
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 119
3.2.4.2. GPT THEORY
The principle of GPT is based on the rapid gas phase reaction between NO and O3, which
produces quantities of NO2 as shown by the following equation:
Equation 4-4
→ NO2 + O2 + hν ( light )
NO + O3
It has been empirically determined that under controlled circumstances the NO-O3 reaction
is very efficient (<1% residual O3), therefore the concentration of NO2 resulting from the
mixing of NO and O3 can be precisely predicted and controlled as long as the following
conditions are met:
• The amount of O3 used in the mixture is known.
• The amount of NO used in the mixture is AT LEAST 10% greater than the
amount of O3 (per EPA requirements) in the mixture.
• The volume of the mixing chamber is known (130 cc, as previously stated).
• The NO and O3 flow rates (from which the time the two gases are in the mixing
chamber) are low enough to give a residence time of the reactants in the mixing
chamber of >2.75 ppm min.
Given the above conditions, the amount of NO2 being output by the calibrator will be equal
(at a 1:1 ratio) to the amount of O3 added.
Once the user has determined the appropriate flow and NO gas bottle required, performing
the GPT is as simple as entering the following parameters in the GPT menu:
• desired Ozone concentration
• desired NO concentration
• desired Total Flow Rate (see recommendation in Section 3.2.4.3 below)
Since the O3 flow rate of the calibrator’s O3 generator is a set fixed value (typically about
0.105 LPM), the calibrator will calculate the additional flow required from the zero air
MFC from the user’s Total Gas Flow entry in the Generate menu. The NO MFC flow rate
will be determined based on the NO concentration and the total flow rate.
For multi-point (M-P) NO2 checks, TAPI recommends keeping the NO concentration and
Total Flow Rate constant and only adjusting the Ozone concentration for each of the NO2
concentrations needed, keeping in mind the guidelines mentioned above.
120 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
Note It is not recommended to set any flow rate to <10% or
>100% of the full scale rating of that associated mass flow
controller.
For calibrators with multiple MFCs installed, their
combined flow potential is available within limits:
<10% of the lowest rated MFC or >100% of the combined
full-scale ratings for both mass flow controllers. The
calibrator automatically selects the MFC with the lowest
flow rate that can accommodate the requested flow,
thereby affording the most precise flow control. If no
single MFC can accommodate the requested flow rate,
then multiple mass flow controllers are used.
Given this information, the calibrator determines the NO gas flow by the formula:
Equation 4-5
C NO 2 × Totalflow
NO GASflow =
C NO
WHERE:
CNO2 = target concentration for the NO2 output
CNO = concentration of the NO gas input
NO GASflow = NO source gas flow rate
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 121
3.2.5.1. GPTZ VS AUTO GENERATE MODES
It may appear that the GPTZ and AUTO Generation modes are performing the same
function: generating NO cal gas at a specified concentration and flow rate. However, there
is an important difference in the flow configuration of these two modes.
In GPTZ mode, the total flow includes flow from the (un-energized) O3 generator. This
flow is not directly measured by the calibrator. The O3 generator flow is measured at the
factory and programmed into the calibrator and assumed to be constant thereafter. Since
pressure and temperature changes between the factory cal and the customer’s ambient
conditions cannot be accounted for, there may be small discrepancies between the actual
O3 generator flow and the assumed flow that is used in the dilution calculations that the
calibrator performs. Since these small flow discrepancies are present in both the GPTZ
and GPT modes, they do not affect the accuracy of the converter efficiency calculations.
For the best overall dilution accuracy, for span calibrations for instance, the AUTO mode
should still be used.
Table 3-5. Status of Internal Pneumatics during GENERATE > GPTZ Mode
VALVES2 PHOT
MFCs3
MODE
(X = CLOSED; O = OPEN; D = DEENERGIZED; E = ENERGIZED) PUMP
CYL CYL CYL CYL O3
PURGE DILUENT GPT PHOT M/R CAL1 CAL21 DILUENT
1 2 3 4 GEN
122 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
Instrument Chassis
Pressure
Regulator O3 GAS INPUT
O3 FLOW
SENSOR
PRESSURE SENSOR
DILUENT
GENERATOR
O3 Generator Assembly
INLET grn PHOTOMETER
grn
PRESSURE SENSOR On Back Panel
DILUENT
O3
Valve O3 GEN / PHOTOMETER vio PHOTOMETER
brn PRESSURE / FLOW SENSOR PCA INLET
ON Flow Control
REF/MEAS
Valve
vio
(800 cm 3)
Flow Control
Purge brn brn
(100 cm 3)
Valve
wht
DILUENT Diluent OFF wht PHOTOMETER
PRESSURE SENSOR
O3 Gen
PCA
PHOTOMETER
CAL GAS 2 Valve
CAL GAS ZERO OUT
INLET gry
PRESSURE
SENSOR INTERNAL
red blk VENT
CAL GAS 3 blk
INLET EXHAUST
orn GPT
Valve
CAL GAS 4
orn ON PHOTOMETER
INLET OUTLET
yel
yel red
GAS INPUT MANIFOLD yel
(on back panel) yel CAL GAS
Cal Gas OUTPUT 1
Mass Flow Controller 1
CAL GAS
GPT blu
OUTPUT 2
Volume
VENT
blu
GAS OUTPUT MANIFOLD
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 123
Once the exact O3 concentration being output by the generator is determined, the
calibrator’s software adjusts the O3 drive voltage up or down (“O3 Gen Drive” parameter
can be viewed in the Dashboard and/or a Home Page Meter), so that the output of the
generator matches as closely as possible the target concentration requested. This adjusted
generator setting will be used during any subsequent real GPT operation that uses the same
target NO2 value.
In order to keep the resulting concentration of O3 consistent with the GPT mixture being
simulated, the instrument’s software adjusts the flow rate of the diluent gas to substitute an
amount of diluent gas equal to the amount of NO gas that would normally be used.
Table 3-6. Status of Internal Pneumatics during GENERATE > GPTPS Mode
VALVES2 PHOT
MFCs3
MODE
(X = CLOSED; O = OPEN; D = DEENERGIZED; E = ENERGIZED) PUMP
CYL CYL CYL CYL O3
PURGE DILUENT GPT PHOT M/R CAL1 CAL21 DILUENT
1 2 3 4 GEN
124 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
Instrument Chassis
Pressure
Regulator O3 GAS INPUT
O3 FLOW
SENSOR
PRESSURE SENSOR
DILUENT
GENERATOR
O3 Generator Assembly
INLET grn PHOTOMETER
grn
PRESSURE SENSOR On Back Panel
DILUENT
O3
Valve O3 GEN / PHOTOMETER vio PHOTOMETER
brn PRESSURE / FLOW SENSOR PCA INLET
ON Flow Control
REF/MEAS
Valve
vio
(800 cm3)
Flow Control
Purge brn brn
(100 cm3)
Valve wht
DILUENT Diluent ON wht PHOTOMETER
PRESSURE SENSOR
O3 Gen
PCA
PHOTOMETER
CAL GAS 2 Valve
CAL GAS ZERO OUT
INLET gry
PRESSURE
SENSOR INTERNAL
red blk VENT
CAL GAS 3 blk
INLET EXHAUST
orn GPT
Valve
CAL GAS 4
orn OFF PHOTOMETER
INLET OUTLET
yel
yel red
GAS INPUT MANIFOLD yel
(on back panel) yel CAL GAS
Cal Gas OUTPUT 1
Mass Flow Controller 1
CAL GAS
GPT blu
OUTPUT 2
Volume
VENT
blu
GAS OUTPUT MANIFOLD
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 125
3.2.6.2. INITIATING A GPTPS
To activate the GPTPS feature you will need to know the values for the following
parameters that will be entered for the subsequent GPT (if a multi-point GPT will be run,
then a separate GPTPS should be run for each O3 concentration point:
• The Total Gas Flow for the mixture output
• The Target O3 concentration (equal to the target NO2 concentration being
simulated)
• The NO source gas concentration
In the Generate menu, press the GPTPS button and edit the applicable fields, then press the
Generate button.
Table 3-7. Status of Internal Pneumatics during GENERATE > GPT Mode
VALVES
MFCs PHOT
(X = Closed; O = Open; D = Deenergized; E = Energized)
MODE PUMP
CYL CYL CYL CYL O3
PURGE DILUENT GPT PHOT M/R CAL1 CAL21 DILUENT
1 2 3 4 GEN
Reference
GPT O2 O2 O2 O2 X O E E Phase ON3 ON3 ON OFF
1
Only present if multiple cal gas MFC option is installed.
2
The valve associated with the cylinder containing NO source gas is open.
3
In instrument with multiple MFCs the CPU chooses which MFC to use depending on the target gas flow requested.
126 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
Instrument Chassis
Pressure
Regulator O3 GAS INPUT
O3 FLOW
SENSOR
PRESSURE SENSOR
DILUENT
GENERATOR
O3 Generator Assembly
INLET grn PHOTOMETER
grn
PRESSURE SENSOR On Back Panel
DILUENT
O3
Valve O3 GEN / PHOTOMETER vio PHOTOMETER
brn PRESSURE / FLOW SENSOR PCA INLET
ON Flow Control
REF/MEAS
Valve
vio
(800 cm3)
Flow Control
Purge brn brn
(100 cm3)
Valve wht
DILUENT Diluent OFF wht PHOTOMETER
PRESSURE SENSOR
O3 Gen
PCA
PHOTOMETER
CAL GAS 2 Valve
CAL GAS ZERO OUT
INLET gry
PRESSURE
SENSOR INTERNAL
red blk VENT
CAL GAS 3 blk
INLET
orn GPT EXHAUST
ON Valve
CAL GAS 4
orn
PHOTOMETER
INLET OUTLET
yel
yel red
GAS INPUT MANIFOLD yel
(on back panel) yel CAL GAS
Cal Gas OUTPUT 1
Mass Flow Controller 1
CAL GAS
GPT blu
OUTPUT 2
Volume
VENT
blu
GAS OUTPUT MANIFOLD
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 127
3.2.7.2. INITIATING A GPT CALIBRATION GAS GENERATION
20 ppb • LPM
FT ≥
O3Conc
• NO Flow Requirements
To achieve a reasonable response time during the GPT and to
satisfy the EPA requirement(1) (2) that the residence time in the GPT
reaction chamber be less than two minutes, the NO flow rate should
be greater than 45 cc/min. Therefore, larger dilution flows may be
required to achieve low concentrations of NO. An appropriate NO
gas bottle concentration must be used in order to achieve this flow
rate.
In the Generate menu, press the GPT button and edit the applicable fields, then press the
Generate button.
128 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
3.2.8. GENERATE > SEQUENCE
Sequences, a set of calibration steps for serial execution, are configured in the
Setup>Sequences menu (Section 2.6.7). To execute a Sequence, navigate to the Generate
menu (Figure 3-5), press the SEQUENCE button, and select the desired Sequence, then
press the Generate button.
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 129
4. COMMUNICATIONS AND REMOTE OPERATION
The instrument rear panel connections include an Ethernet port, a USB port (option) and
two serial communications ports (labeled RS232, which is the COM1 port, and COM2)
located on the rear panel (refer to Figure 2-2). These ports allow the ability to communicate
with, issue commands to, and receive data from the analyzer through an external computer
system or terminal.
This Section provides pertinent information regarding communication equipment, the
communications ports, and communications protocol. Data acquisition is set up through
the Datalogger (Section 2.6).
130 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
Note When the rear panel COM2 port is in use, except for
multidrop communication, the rear panel USB port cannot
be used. (Alternatively, when the USB port is enabled,
COM2 port cannot be used except for multidrop).
A code-activated switch (CAS), can also be used on either port to connect typically
between 2 and 16 send/receive instruments (host computer(s) printers, data loggers,
analyzers, monitors, calibrators, etc.) into one communications hub. Contact Teledyne API
Sales (front cover, this manual) for more information on CAS systems.
4.3. ETHERNET
When using the Ethernet interface, the analyzer can be connected to any standard 10BaseT
or 100BaseT Ethernet network via low-cost network hubs, switches or routers. The
interface operates as a standard TCP/IP device on port 3000. This allows a remote computer
to connect through the network to the analyzer using NumaView™ Remote, terminal
emulators or other programs.
The Ethernet connector has two LEDs that are on the connector itself, indicating its current
operating status.
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 131
4.4.1.1. MODBUS COM PORT CONFIGURATION
MODBUS communications can be configured for transmission over Ethernet or serial
COM port through the Setup>Comm menu. Make the appropriate cable connections
(Ethernet or COM port) between the instrument and a PC.
Ethernet: MODBUS is available on TCP port 502. By default, port 502 is assigned to
the instrument’s TCP Port 2. In the Setup>Comm> TCP Port menu, check
to see that it is set to “502” (Figure 4-1).
Serial COM: Both COM1 (labeled “RS232” on the instrument’s rear panel) and COM2
are configurable for RS-232 or RS-485 communication with either
MODBUS RTU or MODBUS ASCII transmission modes. In the
Setup>Comm COM1[COM2] menu, edit the Protocol parameter to select a
MODBUS transmission mode; edit Baud Rate, Parity, Data Bits, etc., if
necessary (see descriptions in Table 2-15).
Press the Accept button to apply the settings. (Figure 4-2 shows an example
for MODBUS RTU).
132 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
Figure 4-2. MODBUS via Serial Communication (example)
Next, for the settings to take effect, power off the analyzer, wait 5 seconds, and power it
on again.
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 133
5. CALIBRATION AND VERIFICATION
Basic electronic calibration of the Dynamic Dilution Calibrator is performed at the factory.
Normally there is no need to perform this factory calibration in the field; however, the
performance of several of the instrument’s key subsystems should be verified periodically
and adjusted if necessary. These subsystems are:
• Mass Flow Controllers: The accuracy of the mass flow controller outputs is
intrinsic to achieving the correct calibration mixture concentrations; therefore,
the accuracy of their output should be checked and if necessary adjusted
every 6 months (see Section 5.1).
• O3 Photometer: If your calibrator is equipped with the optional O3
photometer, its performance should be periodically verified against and
external transfer standard (see Section 5.2).
• O3 Generator: If your calibrator is equipped with the optional O3 generator, it
should be periodically calibrated (see Section 5.3).
134 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
The Flow Table for each MFC sets its output at each of 20 equally spaced control points
along its entire performance range. In the Utilities>Diagnostics menu view the FlowTable
field for each MFC by clicking the Edit Table button. For each calibration point, the
following is displayed:
• The drive voltage in 20 equal, incremental steps from 0 mVDC to 5000
mVDC;
• The expected flow rate corresponding to each drive voltage point (each equal
to1/20th of the full scale for the selected mass flow controller).
This table can also be used to calibrate the output of the MFCs by adjusting either the
control voltage of a point or its associated flow output value (see Section 5.1.2).
2. Open the calibrator’s front panel for easiest access to the MFC output ports.
3. Attach the flow meter directly to the output port of the MFC to be checked/tested.
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 135
Input Gas
GPT
Chamber
Pressure
Sensor
PCA
PHOTOMETER GPT
Valve
Front Panel
136 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
Figure 5-3. MFC Calibration
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 137
5.2.1. SETUP FOR VERIFYING O3 PHOTOMETER (OPTION) PERFORMANCE
Note This operation requires an external reference photometer.
PHOTOMETER INLET
PHOTOMETER OUTLET
PHOTOMETER ZERO IN
PHOTOMETER ZERO OUT
Max Length=3 meters ( or 10 feet)
EXHAUST
CYL1
CYL2 VENT
Enclosure Wall
DILUENT IN
Calibrator
138 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
Figure 5-5. O3 Photometer Performance Verification
Calibrating the optional internal photometer requires a different set up than that used during
the normal operation of the calibrator. There are two ways to make the connections between
these instruments and the calibrator: either with direct connections (Section 5.2.3.1) or with
calibration manifolds (Section 5.2.3.2).
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 139
5.2.3.1. SETUP USING DIRECT CONNECTIONS
Create the setup as illustrated in Figure 5-6, which shows the external Zero air and O3
sources as well as the reference photometer connected directly to the fixtures on the
calibrator’s rear panel.
REFERENCE
PHOTOMETER
External O3 Source
PHOTOMETER INLET
PHOTOMETER OUTLET
Capped
PHOTOMETER ZERO IN
PHOTOMETER ZERO OUT
Capped
Vent line
EXHAUST
CYL1 Max Length=3 meters ( or 10 feet)
Calibration CYL2
VENT
Source Gas CYL3
CAL OUT
connections are CYL4
CAL OUT
as shown in
If the gas flow on this
Section 3.2 line is ≥ 5 SLPM
DILUENT IN the minimum O.D.
Calibrator must be 3/8 inch
Enclosure Wall
CAL OUT gas outlet
connections to
manifolds/instruments
Note A minimum of 1.1 LPM is required for the external zero air
source.
140 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
5.2.3.2. SETUP USING A CALIBRATION MANIFOLD
Create the setup as illustrated in Figure 5-7, which shows the external zero air and O3
sources as well as the reference photometer connected to the calibrator via calibration
manifolds for both Zero air and O3.
Enclosure Wall
To other calibrators or
instruments
PHOTOMETER INLET
Capped PHOTOMETER OUTLET Max Length=3 meters
( or 10 feet)
Vent line PHOTOMETER ZERO IN
Max Length=3 meters PHOTOMETER ZERO OUT Capped
( or 10 feet) EXHAUST
CYL1
CYL2 VENT
Calibration CYL3
Source Gas CAL OUT Must be vented with at least
CYL4 3 ft of 1/4 inch tubing. If the
connections are CAL OUT gas flow on this line is
as shown in ≥ 5 SLPM the minimum O.D.
Enclosure Wall
Section 3.2 must be 3/8 inch
DILUENT IN
Calibrator
CAL OUT gas outlet
connections to
manifolds/instruments
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 141
5.2.4. PERFORMING O3 PHOTOMETER (OPTION) CALIBRATIONS
To calibrate the photometer, first set the Vars>O3 Gen Mode to BNCH (bench):
1. Navigate to the Utilities>Diagnostics menu.
2. Select the Bench Cal function.
142 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
5.2.5. O3 PHOTOMETER GAS FLOW CALIBRATION
Note A separate flow meter is required for the procedure.
To calibrate the flow of gas through the calibrator’s optional photometer bench.
1. Turn OFF power to the calibrator.
2. Attach the flow meter directly to the EXHAUST port of the calibrator.
3. Turn ON power to the calibrator.
4. In the Utilities>Diagnostics menu press the button in the Actual Flow field to input
the external flow meter’s reading.
5. Press the Calibrate button.
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 143
5.3. VERIFYING AND CALIBRATING THE O3 GENERATOR OPTION
Figure 5-10 shows the reference photometer connected directly to the fixtures on the rear
panel.
REFERENCE
PHOTOMETER
Calibration CYL3
Source Gas If the gas flow on
CYL4 CAL OUT
this line is
connections CAL OUT ≥ 5 SLPM the
are as shown minimum O.D.
in Section 3.2 DILUENT IN must be 3/8 inch
Enclosure Wall
Calibrator
CAL OUT gas outlet
connections to
manifolds/instruments
144 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
4. Press the concentration button and/or the units buttons to adjust their values
as needed.
5. Press the Total Flow button to adjust the value for the target flow.
6. Press the Generate button, and then the AUTO button.
Note The readings recorded from the AUTO generate function
and the reference photometer should be within 1% of each
other.
The Dynamic Dilution Calibrator has several sensors that monitor the pressure of the gases
flowing through the instrument. The data collected by these sensors is used to compensate
the final concentration calculations for changes in atmospheric pressure and is stored in the
CPU’s memory as various test functions:
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 145
Instrument Chassis
Pressure
Monitor
DILUENT On Back Panel
INLET
PHOTOMETER
INLET
DILUENT
brn
Valve
PHOTOMETER
ZERO IN
brn
Purge
Valve PHOTOMETER
brn ZERO OUT
DILUENT
PRESSURE SENSOR
CAL GAS 1 PRESSURE
INLET SENSOR EXHAUST
INPUT GAS
Diluent
Mass Flow Controller
PCA
Instrument Chassis
Pressure
Flow Control PHOTOMETER BENCH
Monitor (1.0 LPM)
gry
O3 FLOW
Pressure
SENSOR
DILUENT
O3 Generator Assembly
INLET PHOTOMETER
grn On Back Panel
PRESSURE SENSOR
DILUENT
O3
brn
Valve O3 GEN / PHOTOMETER
PRESSURE / FLOW SENSOR PCA vio PHOTOMETER
INLET
Pressure Flow Control REF/MEAS vio
Valve
Monitor (800 cm3)
Flow Control
Purge brn
(10 cm3)
Valve
wht
brn
DILUENT PUMP wht PHOTOMETER
PRESSURE SENSOR
CAL GAS 4
orn GPT
INLET Valve
yel
yel PHOTOMETER
GAS INPUT MANIFOLD yel OUTLET
(on back panel)
CAL GAS
Cal Gas red OUTPUT 1
Mass Flow Controller 2
Pressure yel
CAL GAS
Monitor
GPT blu
OUTPUT 2
Volume
VENT
blu
yel GAS OUTPUT MANIFOLD
yel
Figure 5-12. Pressure Monitor Points with O3 Options and Multiple Cal MFCs Installed
146 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
5.4.1.1. CALIBRATING DILUENT, CAL GAS, OR OPT O3 GENERATOR PRESSURE
SENSORS
1. Turn off the calibrator and open the top cover.
2. For the sensor being calibrated, insert a “T” pneumatic connector and pressure
monitor at the location described in Table 5-2 and shown in Figure 5-11 and Figure
5-12.
3. Turn on the calibrator, and in the Diagnostics>Pressure Cal menu (Figure 5-13)
highlight the pressure sensor to be calibrated.
4. In the Actual Pressure field (press to bring up keypad) input the value obtained from
pressure meter.
5. (Enable the valve if interface shows an Enable button).
6. Press the Calibrate button, and then confirm that the calibration is to be carried out.
The Status field should read “Success”.
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 147
5.4.1.2. CALIBRATING THE PHOTOMETER (OPTION) SAMPLE GAS PRESSURE
SENSOR
148 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
6. MAINTENANCE
Predictive diagnostic functions including failure warnings and alarms built into the
calibrator’s firmware allow the user to determine when repairs are necessary without
performing painstaking preventative maintenance procedures.
Follow the maintenance schedule provided in this section.
CAUTION
Risk of electrical shock. Disconnect power before performing any of
the following operations that require entry into the interior of the
calibrator.
CAUTION
The operations outlined in this Section are to be performed by
qualified maintenance personnel only.
Weekly or after
Verify Test Record and
any Maintenance No
Functions analyze
or Repair
Pump
Diaphragm1 No Replacement Required. Under Normal Circumstances this Pump Will Last the Lifetime of the Instrument.
The report can also be set to generate periodically and sent to a Web services “cloud” where
it is available for viewing by Teledyne API technical support personnel. Set this function
with two Vars:
Setup>Vars>Upload Report to Cloud: set to True.
Setup>Vars>Report Upload>Interval: edit the number of hours between report uploads.
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 151
6.3. SOFTWARE/FIRMWARE UPDATES
There are two ways to check for and acquire updates: either remotely or manually.
3. Insert a flash drive into a front panel USB port and wait for the Status field to
indicate that the drive has been detected.
4. In the Update Firmware field, press the Check button for the instrument to
determine whether the firmware on the flash drive is more recent than what is
152 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
currently installed. Once it’s been determined that the firmware is new, the
Install button will be enabled; if the firmware version on the flash drive is the
same as or older than the current firmware of the instrument, the Install button
will not be enabled.
5. Press the Install button, and note the messages in the Status field at the
bottom of the page. Use the Cancel button if necessary.
6. When complete, as indicated in the Status field, press the Done button, which
replaces the Cancel button, and remove the flash drive.
7. Power off and restart the instrument to complete the new firmware installation.
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 153
6.4. TIME ZONE CHANGES
There is an option to change between 12-hour and 24-hour format in the Setup>Vars menu
(System Time Format), effectively changing the Time Zone requires a specific procedure
as follows:
1. In Setup>Instrument>Date/Time Settings select the applicable Time Zone.
2. Allow adequate time for the selected Time Zone to be properly accepted.
3. Verify: return to Home page then back to the Date/Time Settings page, and
check that the selected Time Zone is now highlighted.
4. Without making any other changes, power OFF the instrument and power ON
again.
5. Once restarted, return to the Date/Time Settings page where the newly
selected Time Zone should be highlighted. (If not, it means that not enough
time had passed for the instrument to accept the change before the power was
cycled OFF).
6. After the Time Zone is implemented first (Steps 1 through 5), then other
changes to the date and/or time can be made, and recycling the power is not
necessary.
154 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
6.5. MAINTENANCE PROCEDURES
The following procedures are to be performed periodically as part of the standard
maintenance of the calibrator.
1. Using a #6 nut driver, remove hex nut at the photometer’s gas outlet.
2. Using a #6 nut driver, remove hex nut from the end of the T-fitting mounted on top
of the photometer (or, in older models, on back of O3 Gen/Photometer
Pressure/Flow Sensor board mounted to floor of chassis), and reconnect it to the
photometer’s gas outlet. (The other end of this tube is connected to the O3
generator valve). Now continue to Step 3.
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 155
Figure 6-6. Bypassing the Photometer Sensor PCA and Pump
156 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
3. Using the 1/8” cap, securely cover the outlet of the internal vent (see Figure 6-6)
located just behind the valve relay PCA.
4. Use the 1/4" caps to cover the following gas outlet ports on the calibrator’s rear
panel (see Figure 6-7).
• EXHAUST port (Only required for calibrators with O3 generators
installed).
• both CAL GAS OUT ports
• the VENT port
“T” Fitting
5. If a bottle of source gas is connected to the CYL 1 port, close the bottle’s gas outlet
and disconnect it from the port.
6. Using a “T” type pneumatic fitting, connect a gas line from the zero air gas source to
the Diluent In and to the CYL 1 port u (see Figure 6-7).
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 157
Instrument Chassis
PRESSURE SENSOR
CAL GAS 1 PRESSURE
INLET SENSOR EXHAUST
INPUT GAS Diluent
Mass Flow Controller
CAP
CAL GAS 3 SENSOR
OUTPUT 1
INLET
orn
blu CAL GAS
CAP
orn OUTPUT 2
CAL GAS 4
INLET
yel
CAP
GAS INPUT MANIFOLD yel VENT
yel blu
(on back panel)
Cal Gas GAS OUTPUT MANIFOLD
Mass Flow Controller
yel
Figure 6-8. Gas Flow for Auto-Leak Check of Base Model Calibrators
Instrument Chassis
O3 GAS INPUT
O3 FLOW
Pressure
SENSOR
PRESSURE
Regulator
SENSOR
DILUENT grn
GENERATOR
O3 Generator Assembly
INLET PHOTOMETER
grn
PRESSURE SENSOR On Back Panel
DILUENT
O3
Purge brn
(10 cm 3)
Valve wht
brn wht PHOTOMETER
DILUENT OFF
/ ZERO IN
PRESSURE SENSOR
Cal Gas
CAL GAS VENT
Mass Flow Controller 1 red
PRESSURE
CAL GAS 3 SENSOR
INLET blk
EXHAUST
orn
CAL GAS 4
orn GPT
INLET Valve
yel
yel PHOTOMETER
GAS INPUT MANIFOLD yel OUTLET
(on back panel)
CAL GAS
CAP
blu OUTPUT 2
Volume
CAP
VENT
blu
yel GAS OUTPUT MANIFOLD
yel
Figure 6-9. Gas Flow for Auto-Leak Check of Calibrators with O3 Generator and Photometer Option
158 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
6.5.1.3. RETURNING THE CALIBRATOR TO SERVICE AFTER PERFORMING AN AUTO
LEAK CHECK
1. Remove all of the caps from the EXHAUST, CAL GAS OUTPUTS (2) and the VENT
port and from the internal vent.
2. On instruments with an optional O3 photometer, reconnect the internal gas lines so
that the Sensor PCA and pump are functional.
3. Remove the tee from the DILUENT IN and CYL 1.
4. Reconnect the ZERO AIR SOURCE to the DILUENT IN.
5. Reconnect Cal Gas bottle to CYL 1 and open the bottle’s outlet port.
6. Replace the calibrator’s top cover.
7. The calibrator is now ready to be used.
CAUTION
Do not cause the tube to bind against the metal housings.
The tube may break and cause serious injury.
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 159
10. If there is any noticeable damage to these o-rings, they should be replaced.
11. Re-assemble the tube into the lamp housing and perform an Auto Leak Check on
the instrument.
160 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
6.5.4. UV SOURCE LAMP REPLACEMENT
This procedure details the steps for replacement of the UV source lamp in the optical bench
assembly. This procedure should be done whenever the lamp can no longer be adjusted as
described in Section 6.5.3.
CAUTION
The UV lamp contains mercury (Hg), which is considered hazardous
waste. The lamp should be disposed of in accordance with local
regulations regarding waste containing mercury.
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 161
6.5.5. OZONE GENERATOR UV LAMP ADJUSTMENT OR REPLACEMENT
This procedure details the steps for replacement and initial adjustment of the ozone
generator lamp. If you are adjusting an existing lamp, skip to Step 8.
1. Turn off the calibrator.
2. Remove the cover from the calibrator.
3. Locate the O3 generator (see Figure 2-4).
UV Lamp
Set Screws
Lamp
O-ring
O3 Generator
Body
4. Remove the two setscrews on the top of the O3 generator and gently pull out the old
lamp.
5. Inspect the o-ring beneath the nut and replace if damaged.
6. Install the new lamp in O3 generator housing, ensuring that it is fully seated.
7. Tighten the two setscrew
8. Turn on calibrator and allow it to stabilize for at least 30 minutes.
9. Replace the calibrator’s cover.
10. Perform an auto-leak check (See Section 6.5.1).
11. Perform an Ozone Generator calibration (see Section 5.3).
.
162 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
7. TROUBLESHOOTING AND SERVICE
This Section contains a variety of methods for identifying and solving performance
problems with the calibrator.
ATTENTION
The operations outlined in this Section must be performed by qualified
maintenance personnel only.
WARNING
• Risk of electrical shock. Some operations need to be
carried out with the instrument open and running.
• Exercise caution to avoid electrical shocks and
electrostatic or mechanical damage to the calibrator.
• Do not drop tools into the calibrator or leave those after
your procedures.
• Do not shorten or touch electric connections with metallic
tools while operating inside the calibrator.
• Use common sense when operating inside a running
calibrator.
2. View and compare Dashboard functions’ values to factory values. Note any major
deviations from the factory values and take corrective action.
3. Use the internal electronic status LEDs to determine whether the electronic
communication channels are operating properly.
• Verify that the DC power supplies are operating properly by checking the
voltage test points on the relay PCA.
• Note that the calibrator’s DC power wiring is color-coded and these colors
match the color of the corresponding test points on the relay PCA.
• Follow the procedures defined in Section 2.4.2 to confirm that the
calibrator’s vital functions are working (power supplies, CPU, relay PCA,
etc.).
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 163
7.1.1. FAULT DIAGNOSIS WITH ALERTS
The most common and/or serious instrument failures will result in a warning message being
displayed as an Alert. Table 7-1 lists warning messages, along with their meaning and
recommended corrective action.
It should be noted that if more than two or three warning messages occur at the same time,
it is often an indication that some fundamental sub-system (power supply, relay PCA,
motherboard) has failed rather than indication of the specific failures referenced by the
warnings. In this case, it is recommended that proper operation of power supplies (See
Section 7.3.3), the relay PCA (See Section 7.3.7), and the motherboard (See Section7.3.11)
be confirmed before addressing the specific warning messages.
164 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
ALERT FAULT CONDITION POSSIBLE CAUSES
Value output during the - Faulty UV source lamp
Photometer’s reference - Noisy UV detector
PHOTO LAMP STABILITY cycle changes from - Faulty UV lamp power supply
WARNING measurements to
measurement more than - Faulty ± 15 VDC power supply
25% of the time.
Occurs when Ref is Possible failure of:
PHOTO REFERENCE
<2500 mVDC - UV Lamp
WARNING2
or >4950 mVDC. - UV Photo-Detector Preamp
Motherboard not detected - This warning only appears on Serial I/O COMM Port(s)
on power up. Front Panel Display will be frozen, blank or will not
REAR BOARD NOT DET
respond.
- Failure of motherboard
- Zero or source air supply is incorrectly set up or
improperly vented.
REGULATOR PRESSURE Regulator pressure is - Incorrectly adjusted O3 zero air pressure regulator
WARNING < 15 PSIG or > 25 PSIG. - Leak or blockage exists in the calibrator’s internal
pneumatics
- Failed O3 Generator Input pressure sensor
The CPU cannot - I2C Bus failure
RELAY BOARD WARN communicate with the - Failed relay PCA
Relay PCA. - Loose connectors/wiring
- This message occurs at power on.
The computer has - If it is confirmed that power has not been interrupted
SYSTEM RESET rebooted. - Failed +5 VDC power
- Fatal error caused software to restart
- Loose connector/wiring
The CPU is unable to - I2C Bus failure
VALVE BOARD WARN communicate with the valve - Failed valve driver PCA
board. - Loose connectors/wiring
1 Only applicable for calibrators with the optional the O3 generator installed.
2 Only applicable for calibrators with the optional photometer installed.
3 On instrument with multiple Cal Gas MFCs installed, the MFC FLOW WARNING occurs when the flow rate requested is
<10% of the range of the lowest rated MFC (i.e. all of the cal gas MFC are turned off).
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 165
Table 7-2. Dashboard Functions – Indicated Failures
FUNCTION DIAGNOSTIC RELEVANCE AND CAUSES OF FAULT CONDITIONS.
Gas flow problems directly affect the concentration accuracy of the calibrator’s calibration gas
O3 Flow1 mixtures.
- Check for Gas Flow problems.
Check the O3 generator heater and temperature sensors.
O3 Gen Drive1
Possible causes of faults are the same as O3 GEN LAMP TEMP WARNING from Table 7-1.
Incorrect Lamp temperature can affect the efficiency and durability of the O3 generators UV lamp.
O3 LampTemp1
Possible causes of faults are the same as O3 GEN LAMP TEMP WARNING from Table 7-1.
Affects proper flow rate of Cal gas MFCs.
Cal Gas Press
Possible causes of faults are the same as MFC PRESSURE WARNING from Table 7-1.
Affects proper flow rate of Diluent gas MFCs.
Diluent Press
Possible causes of faults are the same as MFC PRESSURE WARNING from Table 7-1.
REG PRES Same as REGULATOR PRESSURE WARNING from Table 7-1.
Box Temperature typically runs ~7°C warmer than ambient temperature. If the Box Temperature
is out of range, ensure that the:
Box Temp - the exhaust fan is running.
- there is sufficient space on the exterior sides and rear of the instrument to allow adequate
ventilation.
If the value displayed is too high (>4950 mV) the UV Source has become brighter. Adjust the
variable gain potentiometer on the UV Preamp Board in the optical bench.
If the value displayed is too low:
- < 200mV – Bad UV lamp or UV lamp power supply.
- < 2500mV – Lamp output has dropped, adjust UV Preamp Board or replace lamp.
O3 Meas2
& If the value displayed is constantly changing:
O3 Ref2 - Bad UV lamp.
- Defective UV lamp power supply.
- Failed I2C Bus.
If the O3 Ref value changes by more than 10mV between zero and span gas:
- Defective/leaking M/R switching valve.
Gas flow problems directly affect the accuracy of the photometer measurements and therefore the
Photo Flow2 concentration accuracy of cal gas mixtures involving O3 and GPT mixtures.
- Check for Gas Flow problems.
Poor photometer temp control can cause instrument noise, stability and drift. Temperatures
Photo Lamp Temp2 outside of the specified range or oscillating temperatures are cause for concern.
Possible causes of faults are the same as PHOTO LAMP TEMP WARNING from Table 7-1.
The pressure of the gas in the photometer’s sample chamber is used to calculate the
Photo Press2 concentration of O3 in the gas stream. Incorrect sample pressure can cause inaccurate readings.
- Check for Gas Flow problems. See Section Table 7-1.
166 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
FUNCTION DIAGNOSTIC RELEVANCE AND CAUSES OF FAULT CONDITIONS.
The temperature of the gas in the photometer’s sample chamber is used to calculate the
concentration of O3 in the gas stream. Incorrect sample temperature can cause inaccurate
readings.
Possible causes of faults are:
- Bad bench lamp heater
Photo Samp Temp2
- Failed sample temperature sensor
- Failed relay controlling the bench heater
- Failed Relay PCA
- I2C Bus malfunction
- Hot lamp
Values outside range indicate:
Contamination of the Zero Air or Span Gas supply.
Instrument is miss-calibrated.
Photo Slope2
Blocked Gas Flow.
Faulty Sample Pressure Sensor or circuitry.
Bad/incorrect Span Gas concentration.
Values outside range indicate:
Photo Offset2
Contamination of the Zero Air supply.
1 Only appears when the optional O3 generator is installed.
2 Only appears when the optional O3 photometer is installed
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 167
Table 7-3. DIAG – Analog Output Functions
SUB MENU FUNCTION
Analog Output 1: Diluent MFC Drive These channels are used by the calibrator internally as drive
Analog Output 2: Cal1 MFC Drive voltages for instruments with analog MFCs.
Analog Output 3: Cal2 MFC Drive (Option) The settings are preconfigured at the factory and not user-editable.
Analog Output 4: [user-selected function] This is the analog output, user-configured in the Setup>Analog
Outputs>Analog Output Cfg1 menu, with the following parameters:
• Signal Out: function selected for output.
• Min Max: allowable value range for the Signal Out function.
• Calibration Type. Sets the channel for automatic or manual
calibration
• Range1: signal type (voltage or current loop) and full-scale value
of the output.
• Recorder Offset1: bipolar voltage offset (not available when
Range is set to Current loop).
• Allow Overrange: ± 5% over-range feature enabled or disabled
for this output channel.
1After making changes to this output, recalibrate from the Setup>Analog Outputs>Analog Output Cal menu.
168 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
FULL CAUSES OF EXTREMELY
PARAMETER DESCRIPTION ZERO
SCALE HIGH / LOW READINGS
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 169
7.2.2. RELAY PCA STATUS LEDS
There are seven LEDs located on the Relay PCA. Some are not used on this model.
If D1 is blinking, then the other LEDs can be used in conjunction with DIAG Menu Signal
I/O to identify hardware failures of the relays and switches on the Relay.
170 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
D91 Photometer • Faulty +12 VDC Supply (PS2)
O3-PUMP-ON N/A • Faulty Connectors/Wiring
Green Pump Status
D61,2 GPT Valve
GPT_VALVE N/A
Yellow Status
D151 Photometer Voltage displayed should change.
PHOTO_LAMP_HEATER PHOTO_LAMP_TEMP If not:
Yellow Heater Status
• Failed Heater
D162 O3 Generator • Faulty Temperature Sensor
O3_GEN_HEATER O3_GEN_TEMP • Failed AC Relay
Green Heater Status
• Faulty Connectors/Wiring
1 Only applies on calibrators with photometer options installed.
2 Only applies on calibrators with O3 generator options installed.
Figure 7-3. Valve Driver PCA Status LEDS Used for Troubleshooting
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 171
Table 7-8. Relay PCA Status LED Failure Indications
ACTIVATED BY
LED FUNCTION SIGNAL I/O DIAGNOSTIC TECHNIQUE
PARAMETER
D3 Cal Gas CYL1 CYL_VALVE_1
D4 Cal Gas CYL2 CYL_VALVE_2 Valve should audibly change states and LED should glow.
If not:
D5 Cal Gas CYL3 CYL_VALVE_3 • Failed valve
D6 Cal Gas CYL4 CYL_VALVE_4 • Failed valve driver IC on relay PCA
Purge Valve • Failed valve driver board
D9 PURGE_VALVE
Status • Faulty +12 VDC power supply (PS2)
Diluent Valve • Faulty connectors/wiring
D10 INPUT_VALVE
Status
172 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
7.3. SUBSYSTEM CHECKOUT
The preceding sections of this manual discussed a variety of methods for identifying
possible sources of failures or performance problems within the calibrator. In most cases,
this included a list of possible components or subsystems that might be the source of the
problem. This Section describes how to check individual components or subsystems to
determine if which is actually the cause of the problem being investigated.
WARNING
Should the AC power circuit breaker trip, investigate and correct the condition
causing this situation before turning the calibrator back on.
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 173
7.3.3. DC POWER SUPPLY
If you have determined that the calibrator’s AC mains power is working, but the unit is still
not operating properly, there may be a problem with one of the instrument’s switching
power supplies. The supplies can have two faults, namely no DC output, and noisy output.
To assist tracing DC Power Supply problems, the wiring used to connect the various printed
circuit assemblies and DC Powered components and the associated test points on the relay
PCA follow a standard color-coding scheme as defined in Figure 7-4 and Table 7-9.
A voltmeter should be used to verify that the DC voltages are correct per the values in
Table 7-10, and an oscilloscope, in AC mode, with band limiting turned on, can be used to
evaluate if the supplies are producing excessive noise (> 100 mV p-p).
174 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
Table 7-10. DC Power Supply Acceptable Levels
CHECK RELAY PCA TEST POINTS
POWER
VOLTAGE FROM TEST POINT TO TEST POINT MIN V MAX V
SUPPLY ASSY
NAME # NAME #
PS1 +5 Dgnd 1 +5 2 4.8 5.25
PS1 +15 Agnd 3 +15 4 13.5 16V
PS1 -15 Agnd 3 -15V 5 -14V -16V
PS1 Agnd Agnd 3 Dgnd 1 -0.05 0.05
PS1 Chassis Dgnd 1 Chassis N/A -0.05 0.05
PS2 +12 +12V Ret 6 +12V 7 11.75 12.5
PS2 Dgnd +12V Ret 6 Dgnd 1 -0.05 0.05
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 175
7.3.7. RELAY PCA
The Relay PCA can be most easily checked by observing the condition of the status LEDs
on the Relay PCA (see Section 7.2.2), and using the Utilities>Diagnostics>Digital Outputs
menu to toggle each LED ON or OFF.
If D1 on the Relay PCA is flashing and the status indicator for the output in question
(Heater power, Valve Drive, etc.) toggles properly using the Signal I/O function, then the
associated control device on the Relay PCA is bad. Several of the control devices are in
sockets and can be easily replaced. Table 7-11 lists the control device associated with a
particular function.
Expected mVDC =
( Pressure
34.18psig )
x 4250mvDC + 750mvDC ± 10%rdg
176 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
EXAMPLE. If the measured pressure is 25 PSIG, the expected voltage level between
TP4 and TP1 would be between 3470 mVDC and 4245 mVDC.
EXAMPLE. If the measured pressure is 30 PSIG, the expected voltage level between
TP4 and TP1 would be between 4030 mVDC and 4930 mVDC.
• If this voltage is out of range, then either pressure transducer S1 is bad, the
board is bad, or there is a pneumatic failure preventing the pressure
transducer from sensing the absorption cell pressure properly.
Expected mVDC =
( Pressure
30.0In-Hg-A )
x 4660mvDC + 250mvDC ± 10%rdg
EXAMPLE. If the measured pressure is 20 In-Hg-A, the expected voltage level between
TP4 and TP1 would be between 2870 mVDC and 3510 mVDC.
EXAMPLE. If the measured pressure is 25 In-Hg-A, the expected voltage level between
TP4 and TP1 would be between 3533 mVDC and 4318 mVDC.
• If this voltage is out of range, then either pressure transducer S1 is bad, the
board is bad or there is a pneumatic failure preventing the pressure
transducer from sensing the absorption cell pressure properly.
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 177
7.3.10.3. O3 GENERATOR PRESSURE SENSOR
1. Measure the pressure on the inlet side of S2 with an external pressure meter.
2. Measure the voltage across TP5 and TP1.
• Evaluate the reading in the same manner as for the cal gas pressure sensor
(see Section 7.3.9).
7.3.11. MOTHERBOARD
178 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
7.3.11.2. ANALOG OUTPUTS VOLTAGE TEST
To verify that Analog Output 4, if configured, is working properly, connect a voltmeter to
the rear panel ANALOG OUT connector and perform an output step test as follows:
1. Navigate to the Utilities>Diagnostics>Analog Outputs page.
Table 7-12. Analog Output Test Function - Nominal Values Voltage Outputs
FULL SCALE OUTPUT OF VOLTAGE RANGE
100MV 1V 5V 10V
SIGNAL NOMINAL OUTPUT VOLTAGE
%
0 0 0 0 0
20 20 mV 0.2 1 2
40 40 mV 0.4 2 4
60 60 mV 0.6 3 6
80 80 mV 0.8 4 8
100 100 mV 1.0 5 10
If one or more of the readings fails to be within range, it is likely that there has been a
failure of the either or both of the DACs and their associated circuitry on the motherboard.
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 179
7.3.11.3. DIGITAL (STATUS) OUTPUTS
To test the status output electronics:
1. Connect a jumper between the “D“ pin and the “” pin on the rear panel STATUS
output connector.
2. Connect a 1000 ohm resistor between the “+” pin and the pin corresponding to the
status output that is being tested.
3. Connect a voltmeter between the “” pin and the pin of the output being tested (as
mapped in the Setup>Digital Outputs menu).
4. Under the Utilities>Diagnostics menu, scroll through the inputs and outputs until you get
to the output in question and observe whether it toggles ON or OFF.
5. Alternatively, highlight the Output in the Utilities>Diagnostics menu and toggle it ON or
OFF while observing the voltage on the voltmeter. It should vary between 0 volts for ON
and 5 volts for OFF.
Table 7-13. Calibrator Control Input Pin Assignments and Digital Inputs Panel
CONNECTOR INPUT CORRESPONDING
Top 1 Control Input 01
Top 2 Control Input 02
Top 3 Control Input 03
Top 4 Control Input 04
Top 5 Control Input 05
Top 6 Control Input 06
Bottom 7 Control Input 07
Bottom 8 Control Input 08
Bottom 9 Control Input 09
Bottom 10 Control Input 10
Bottom 11 Control Input 11
Bottom 12 Control Input 12
The control input bits can be tested by applying a trigger voltage to an input and watching
status changes of the associated function in the Utilities>Diagnostics>Digital Inputs:
EXAMPLE: to test the rear panel CONTROL IN pin “1”:
1. In the Utilities>Diagnostics>Digital Inputs menu view the output named Control Input 01.
2. Connect a jumper from the “+” pin on the appropriate connector to the “U” on the same
connector.
3. Connect a second jumper from the “” pin on the connector to the “1” pin.
4. The status of Control Input 01 should change to read “ON”.
180 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
7.3.11.5. CONTROL OUTPUTS
To test the Control Output electronics:
1. Connect a jumper between the “E“ pin and the “” pin on the status output connector.
2. Connect a 1000 ohm resistor between the “+” pin and the pin for the status output that is
being tested.
3. Connect a voltmeter between the “” pin and the pin of the output being tested (see
Table 7-14).
4. Scroll the Utilities>Diagnostics>Digital Outputs menu until you get to the output in
question.
5. Alternately turn on and off the output noting the voltage on the voltmeter.
• It should vary between 0 volts for ON and 5 volts for OFF.
7.3.12. CPU
There are two major types of CPU board failures, a complete failure and a failure associated
with the Disk On Module (DOM). If either of these failures occurs, contact the factory.
For complete failures, assuming that the power supplies are operating properly and the
wiring is intact, the CPU is faulty if on power-on, the watchdog LED on the motherboard
is not flashing.
In some rare circumstances, this failure may be caused by a bad IC on the motherboard,
specifically U57, the large, 44 pin device on the lower right hand side of the board. If this
is true, removing U57 from its socket will allow the instrument to start up but the
measurements will be invalid.
If the analyzer stops during initialization (the front panel display shows a fault or warning
message), it is likely that the DOM, the firmware or the configuration and data files have
been corrupted.
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 181
7.3.13. THE CALIBRATOR DOESN’T APPEAR ON THE LAN OR INTERNET
Most problems related to Internet communications via the Ethernet card will be due to
problems external to the calibrator (e.g. bad network wiring or connections, failed routers,
malfunctioning servers, etc.) However, there are several symptoms that indicate the
problem may be with the Ethernet card itself.
If neither of the Ethernet cable’s two status LED’s (located on the back of the cable
connector) is lit while the instrument is connected to a network:
Verify that the instrument is being connected to an active network jack.
Check the internal cable connection between the Ethernet card and the CPU board.
182 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
7.3.15.1. BOX / CHASSIS TEMPERATURE
The box temperature sensor can’t be directly accessed with a voltmeter to check its
resistance. Instead, the Box Temp voltage signal must be configured in the Setup>Analog
Outputs>Analog Output Cfg menu first: Map the Signal Out field to Box Temp and scale
it 0.0 degC (Min) to 100.0 degC (Max); set the Calibration type to AUTO. Start calibration
in the Analog Output Cal menu. Compare the Home>Dashboard>Box Temp value to the
Utilities>Diagnostics>Analog Outputs>Analog Output 4: Box Temp voltage. That voltage
signal on a scale of 0 to 5,000 mV should be relative to the scaled temperature value. For
example, at ~30oC (6-7° above room temperature) the signal should be ~1450 mV.
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 183
Utilities>Diagnostics>Digital Outputs menu as described above, turn the
UV Lamp Heater on and off. Check the DC voltage present between pin
1 and 2 on J14 of the Relay Board.
If the FET Driver has failed, there should be no change in the voltage
across pins 1 and 2.
• If the FET Driver checks out OK, the thermistor temperature sensor in
the lamp assembly may have failed. Unplug the connector to the Ozone
Generator Heater/Thermistor PCB, and measure the resistance of the
thermistor between pins 5 and 6 of the 6-pin connector.
184 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
• Check for operation of the A/D circuitry on the motherboard. See
Section 7.3.11.1.
• Confirm the Sample Temperature, Sample Pressure and Sample Flow
readings are correct. Check and adjust as required.
7.4.1.4. THE ANALOG OUTPUT SIGNAL LEVEL DOES NOT AGREE WITH FRONT
PANEL READINGS
• Confirm that the recorder offset (see Section 2.6.9.2) is set to zero.
• Perform an Analog Output calibration (see Section 2.6.9.3).
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 185
7.4.2. CHECKING THE UV LAMP POWER SUPPLY
Note A schematic and physical diagram of the Lamp Power
Supply can be found in Appendix B.
WARNING
HAZARDOUS VOLTAGE PRESENT - USE CAUTION.
It is not always possible to determine with certainty whether a problem is the result of the
UV Lamp or the Lamp Power Supply. However, the following steps will provide a
reasonable confidence test of the Lamp Power Supply.
1. Unplug the cable connector at P1 on the Lamp Power Supply and confirm that +15VDC
is present between Pins 1 and 2 on the cable connector.
2. If this voltage is incorrect, check the DC test points on the relay PCA as described in
Section 7.3.3.
3. Remove the cover of the photometer and check for the presence of the following
voltages on the UV lamp power supply PCA (see Figure 8-20):
• +4500 mVDC ±10 mVDC between TP1 and TP4 (grnd)
• If this voltage is incorrect, either the UV lamp power supply PCA is faulty or
the I2C bus is not communicating with the UV lamp power supply PCA.
• +5VDC between TP3 and TP4 (grnd)
• If this voltages is less than 4.8 or greater than 5.25 either the 5 VDC power
supply or the UV lamp power supply PCA are faulty.
• If the above voltages check out, it is more likely that a problem is due to the
UV Lamp than due to the Lamp Power Supply.
• Replace the Lamp and if the problem persists, replace the Lamp Power
Supply.
186 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
7.5. TROUBLESHOOTING THE OPTIONAL O3 GENERATOR
The only significant components of the O3 generator that might reasonable malfunction is
the power supply assembly for the UV source lamp and the lamp itself.
WARNING
Hazardous voltage present - use caution.
It is not always possible to determine with certainty whether a problem is the result of the
UV Lamp or the Lamp Power Supply, however, the following steps will provide a
reasonable confidence test of the Lamp Power Supply.
1. Ensure that the calibrator is in STANDBY mode.
2. Unplug the cable connector at P1 on the Lamp Power Supply and confirm that +15VDC
is present between Pins 1 and 2 on the cable connector.
3. If this voltage is incorrect, check the DC test points on the relay PCA as described in
Section 7.3.3.
4. Remove the cover of the photometer and check for the presence of the following
voltages on the UV lamp power supply PCA (see Figure 8-20):
• +800 mVDC ±10 mVDC between TP1 and TP4 (grnd)
• If this voltage is incorrect, either the UV lamp power supply PCA is faulty or
the I2C bus is not communicating with the UV lamp power supply PCA.
• +5VDC between TP3 and TP4 (grnd)
• If this voltages is less than 4.8 or greater than 5.25 either the 5 VDC power
supply or the UV lamp power supply PCA are faulty.
• If the above voltages check out, it is more likely that a problem is due to the
UV Lamp than due to the Lamp Power Supply.
• Replace the Lamp and if the problem persists, replace the Lamp Power
Supply.
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 187
7.6. REPLACING THE DISK-ON-MODULE
Replacing the Disk-on-Module (DOM) will cause loss of all DAS data; it may also cause
some of the instrument configuration parameters to be lost unless the replacement DOM
carries the exact same firmware version. Whenever changing the version of installed
software, the memory must be reset. Failure to ensure that memory is reset can cause the
analyzer to malfunction, and invalidate measurements. After the memory is reset, the A/D
converter must be re-calibrated, and all information collected in Step 1 below must be re-
entered before the instrument will function correctly. Also, zero and span calibration
should be performed.
1. Document all analyzer parameters that may have been changed, such as range, auto-
cal, analog output, serial port and other settings before replacing the DOM
2. Turn off power to the instrument, fold down the rear panel by loosening the mounting
screws.
3. When looking at the electronic circuits from the back of the analyzer, locate the Disk-on-
Module in the right-most socket of the CPU board.
4. The DOM should carry a label with firmware revision, date and initials of the
programmer.
5. Remove the nylon standoff clip that mounts the DOM over the CPU board, and lift the
DOM off the CPU. Do not bend the connector pins.
6. Install the new Disk-on-Module, making sure the notch at the end of the chip matches
the notch in the socket.
7. It may be necessary to straighten the pins somewhat to fit them into the socket. Press
the DOM all the way in and reinsert the offset clip.
8. Close the rear panel and turn on power to the machine.
9. If the replacement DOM carries a firmware revision, re-enter all of the setup information.
188 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
7.8. FREQUENTLY ASKED QUESTIONS (FAQS)
The following list of FAQs is from the Teledyne API’s Technical Support Department’s
most commonly asked questions relating to the Dynamic Dilution Calibrator.
QUESTION ANSWER
My ozone reading is not Look at the Photo Ref/Meas. These are most likely too
what I should expect - low and need to be adjusted up to 4500mV. Another
why? possible cause would be no gas flow to the photometer
causing the O3 reading to be out of range - low
When I generate ozone, it Perform an O3 Gen Adjust (Section 6.5.5), and then an
takes a long time to settle O3 Gen Calibration (Section 5.3). Re-run points.
out, or it fluctuates
around the value until
finally stabilizing.
How often should I It does not require rebuilding; the entire pump should be
rebuild the photometer replaced every two years.
pump on my calibrator?
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 189
8. PRINCIPLES OF OPERATION
WHERE:
Cf = final concentration of diluted gas
Ci = source gas concentration
GASflow = source gas flow rate
Totalflow = the total gas flow through the calibrator
WHERE:
GASflow = source gas flow rate
Diluentflow = zero air flow rate
For instruments with multiple source gas MFC total Flow is:
Equation 8-3
Totalflow = GASflow MFC1 + GASflow MFC2 …+ GASflow MFCn + Diluentflow rate
This dilution process is dynamic. The CPU not only keeps track of the temperature and
pressure of the various gases, but also receives data on actual flow rates of the various
MFCs in real time so the flow rate control can be constantly adjusted to maintain a stable
output concentration.
The calibrator’s level of control is so precise that bottles of mixed gases can be used as
source gas. Once the exact concentrations of all of the gases in the bottle are programmed
into the calibrator, it will create an exact output concentration of any of the gases in the
bottle.
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 190
8.1.1. GAS PHASE TITRATION MIXTURES FOR O3 AND NO2
Because ozone is a very reactive and therefore under normal ambient conditions a short-
lived gas, it cannot be reliably bottled, however, an optional O3 generator can be included
in the calibrator that allows the instrument to be use to create calibration mixtures that
include O3.
This ability to generate O3 internally also allows the Dynamic Dilution Calibrator to be
used to create calibration mixture containing NO2 using a gas phase titration process (GPT)
by precisely mixing bottled NO of a known concentration with O3 of a known n
concentration and diluent gas (zero air).
The principle of GPT is based on the rapid gas phase reaction between NO and O3 that
produces quantities of NO2 as according to the following equation:
Equation 8-4
→ NO2 + O2 + hν ( light )
NO + O3
Under controlled circumstances, the NO-O3 reaction is very efficient (<1% residual O3),
therefore the concentration of NO2 resulting from the mixing of NO and O3 can be
accurately predicted and controlled as long as the following conditions are met:
• The amount of O3 used in the mixture is known.
• The amount of NO used in the mixture is AT LEAST 10% greater than
the amount O3 in the mixture.
• The volume of the mixing chamber is known.
• The NO and O3 flow rates (from which the time the two gases are in the
mixing chamber) are low enough to give a residence time of the
reactants in the mixing chamber of >2.75 ppm min.
Given the above conditions, the amount of NO2 being output by the calibrator will be equal
to (at a 1:1 ratio) the amount of O3 added.
Since:
• The O3 flow rate of the O3 generator is a fixed value (typically about
0.105 LPM);
• The GPT chamber’s volume is known,
• The source concentration of NO is a fixed value,
Once the TOTAL FLOW is determined and entered into the calibrator’s memory and
target concentration for the O3 generator are entered into the calibrator’s software, the
calibrator adjusts the NO flow rate and diluent (zero air) flow rate to precisely create the
appropriate NO2 concentration at the output.
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 191
In this case, Totalflow is calculated as:
Equation 10-4
DILflow = Totalflow - NO GASflow - O3 flow
WHERE:
NOGASflow = NO source gas flow rate (For calibrators with multiple source gas
MFC, NOGASflow is the sum of the flow rate for all of the active cal
gas MFCs)
Totalflow = total gas flow requirements of the system.
O3 flow = the flow rate set for the O3 generator.
DILflow = required diluent gas flow
Again, this is a dynamic process. An optional photometer can be added to the calibrator
that allows the CPU to track the chemiluminescent reaction created when the NO and O3
interact to measure the decrease in NO concentration as NO2 is produced. This information,
along with the other data (gas temperature and pressure, actual flow rates, etc.) is used by
the CPU to establish a very accurate NO2 calibration mixture.
By closing all of the four source gas input valves so that only zero air is allowed into the
calibrator, the entire pneumatic system can be purged with zero air without having to
manipulate the MFCs.
For an instrument in which the O3 generator and GPT pneumatics are installed, a glass
volume carefully selected per the U.S. E.P.A. guidelines is used to optimize NO2 creation.
See Figure 2-22 and Section 2.3.2 for descriptions of the internal pneumatics for the
calibrator.
192 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
8.2.1.1. DILUENT AND SOURCE GAS FLOW CONTROL
Diluent and source gas flow in the calibrator are directly and dynamically controlled by
using a highly accurate Mass Flow Controller (MFC). These MFCs include internal
sensors, which determine the actual flow of gas though each, and feedback control circuitry
that uses this data to adjust the flow as required. The MFCs consist of a shunt, a sensor, a
solenoid valve and the electronic circuitry required to operate them.
The shunt divides the gas flow such that the flow through the sensor is a precise percentage
of the flow through the valve.
The MFC’s internal sensor operates on a unique thermal-electric principle. A metallic
capillary tube is heated uniformly by a resistance winding attached to the midpoint of the
capillary. Thermocouples are welded at equal distances from the midpoint of the tube. At
zero air flow the temperature of both thermocouples will be the same. When flow occurs
through the tubing, heat is transferred from the tube to the gas on the inlet side and from
the gas back to the tube on the outlet side creating an asymmetrical temperature
distribution. The thermocouples sense the changes of temperature in the capillary tube and
produce a mVDC output signal proportional to that change, which is proportional to the
rate of flow through the MFC’s valve.
The electronic circuitry reads the signal output by the thermal flow sensor measured
through a capillary tube. This signal is amplified so that it is varies between 0.00 VDC and
5.00 VDC. A separate 0 to 5 VDC command voltage is also generated that is proportional
to the target flow rate requested by the CPU. The 0-5VDC command signal is electronically
subtracted from the 0-5VDC flow signal. The amount and direction of the movement is
dependent upon the value and the sign of the differential signal.
The MFC’s valve is an automatic metering solenoid type; its height off the seat is controlled
by the voltage in its coil. The controller’s circuitry amplifies and the differential signal
obtained by comparing the control voltage to the flow sensor output and uses it to drive the
solenoid valve.
As the solenoid valve opens and closes to vary the flow of gas through the shunt, the valve,
and the sensor, in an attempt to minimize the differential between the control voltage for
the target flow rate and the flow sensor output voltage that’s generated by the actual flow
rate of gas through the controller.
This process is heavily dependent on the capacity of the gas to heat and cool. Since the heat
capacity of many gases is relatively constant over wide ranges of temperature and pressure,
the flow meter is calibrated directly in molar mass units for known gases. Changes in gas
composition usually only require application of a simple multiplier to the air calibration to
account for the difference in heat capacity and thus the flow meter is capable of measuring
a wide variety of gases.
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 193
Instrument Chassis
O3 FLOW
Pressure
SENSOR
Regulator O3 GAS INPUT
PRESSURE SENSOR
DILUENT
GENERATOR
O3 Generator Assembly
INLET grn PHOTOMETER
grn
PRESSURE SENSOR On Back Panel
DILUENT
O3
Valve O3 GEN / PHOTOMETER
PRESSURE / FLOW SENSOR PCA vio PHOTOMETER
INLET
brn
REF/MEAS vio
Flow Control
Valve
(800 cm 3)
Flow Control
Purge brn brn
(100 cm 3)
Valve
wht
DILUENT Diluent PUMP wht PHOTOMETER
PRESSURE SENSOR
PHOTOMETER
O3 Gen
PCA
ZERO OUT
Valve gry
CAL GAS 2
INLET
INTERNAL
CAL GAS blk VENT
PRESSURE red
CAL GAS 3 SENSOR
blk
INLET EXHAUST
GPT
orn
Valve
CAL GAS 4
orn
PHOTOMETER
INLET OUTLET
yel
yel red
GAS INPUT MANIFOLD yel
(on back panel)
Cal Gas
yel O3 FLOW CAL GAS
OUTPUT 1
Mass Flow Controller 1
CONTROL
ASSEMBLIES
CAL GAS
GPT blu
OUTPUT 2
Volume
VENT
blu
GAS OUTPUT MANIFOLD
Figure 8-1. Location of Gas Flow Control Assemblies with O3 Generator Installed
194 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
Figure 8-2. Flow Control Assembly & Critical Flow Orifice
The actual flow rate of gas through the orifice (volume of gas per unit of time), depends on
the size and shape of the aperture in the orifice. The larger the hole, the more gas molecules
(moving at the speed of sound) pass through the orifice.
With a nominal pressure of 10 in-Hg-A in the sample/reaction cell, the necessary ratio of
reaction cell pressure to pump vacuum pressure of 2:1 is exceeded and accommodating a
wide range of variability in atmospheric pressure and accounting for pump degradation.
This extends the useful life of the pump. Once the pump degrades to the point where the
sample and vacuum pressures is less than 2:1, a critical flow rate can no longer be
maintained.
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 195
8.3. ELECTRONIC OPERATION
ANALOG RS232 COM2 USB COM
IN Male Female port Ethernet
(I2C Bus)
Analog Outputs
or USB
(Selected
Aout 1
Control Inputs
Touchscreen
MFC2 1 - 12
Cal Gas
Display
Analog Outputs
External Digital I/O
(D/A)
MFC1
(Diluent)
Power Up
Circuit PC 104
Diluent
Pressure Sensor
CPU Card
Sensor Inputs
Cal Gas
Disk on
Converter
Pressure Sensor
Module
A/D
O3 Generator Input
Pressure Sensor
Flash
Photometer Sample Gas
Pressure Sensor Box
Chip
Temperature CPU
Status
LED
GPT Valve
(Optional)
2
Thermistor Interface I C Bus
O3 Generator O3 Generator
Valve
UV (Optional)
Lamp RELAY
PCA
Photometer
M/R Valve
Photometer Photometer I2C (Optional)
O3 Generator Sample Gas UV Lamp Status
Temperature Temperature LED
Lamp Supply
Photometer
Valve Driver Lamp Heater
O3 Generator UV Lamp
Temperature PCA I2C
Photometer Status O3 Generator
Detector LED
Lamp Heater
Preamp
Photometer
Absorption tube Photometer Pump
Photometer Purge CAL GAS 2
Lamp Power Valve INLET
Detector CAL GAS 1
Supply INLET
Photometer
196 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
The core of the calibrator is a microcomputer (referred to as the CPU) that controls various
internal processes, interprets data, makes calculations, and reports results using specialized
firmware developed by Teledyne API. It communicates with the user as well as receives
data from and issues commands to a variety of peripheral devices via a separate printed
circuit assembly called the motherboard.
The motherboard is directly mounted to the inside rear panel and collects data, performs
signal conditioning duties and routes incoming and outgoing signals between the CPU and
the calibrator’s other major components.
Data are generated by the various subcomponents, such as flow data from the MFCs, O3
concentration from the optional photometer. Analog signals are converted into digital data
by a unipolar, analog-to-digital converter, located on the motherboard.
A variety of sensors report the physical and operational status of the calibrator’s major
components, again through the signal processing capabilities of the motherboard. These
status reports are used as data for the concentration calculations and as trigger events for
certain control commands issued by the CPU. They are stored in memory by the CPU and
in most cases can be viewed but the user via the front panel display.
The CPU communicates with the user and the outside world in a variety of manners:
• Through the calibrator’s front panel LCD touchscreen interface;
• RS232 and RS485 serial I/O channels;
• Via Ethernet;
• Various digital and analog outputs, and
• A set of digital control input channels.
Finally, the CPU issues commands via a series of relays and switches (also over the I2C
bus) located on a separate printed circuit assembly to control the function of key
electromechanical devices such as heaters, motors and valves.
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 197
8.3.1. CPU
The unit’s CPU card (Figure 8-4) is installed on the motherboard located inside the rear
panel. It is a low power (5 VDC, 720mA max), high performance, Vortex86SX-based
microcomputer running Windows CE. Its operation and assembly conform to the PC-104
specification and features the following:
The CPU includes two types of non-volatile data storage: an embedded 2MB flash chip
and a Disk on Module (DOM).
198 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
8.3.2. RELAY PCA
The relay PCA is one of the central switching and power distribution units of the calibrator;
it communicates with the motherboard over the I2C bus and can be used for detailed
trouble-shooting of power problems and valve or heater functionality.
This is the base version of the Relay PCA. It does not include the AC relays and is used in
instruments where there are no AC powered components requiring control. A plastic
insulating safety shield covers the empty AC Relay sockets.
WARNING
Never remove this safety shield while the instrument is plugged in and
turned on. The contacts of the AC relay sockets beneath the shield
carry high AC voltages even when no relays are present
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 199
8.3.2.2. HEATER CONTROL
The relay PCA controls the various DC heaters related to the O3 generator and photometer.
MOTHERBOARD
A/D
Converter
Thermistor(s)
(V/F)
(e.g. photometer sample gas temp.;
photometer UV lamp temp.; O3 generator
lamp temp.; ect.)
DC
Control
Logic
O3 Generator PHOTOMETER
Lamp Heater Lamp Heater
200 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
Table 8-1. Relay PCA Status LEDs
LED COLOR DESCRIPTION FUNCTION
D1 Red Watchdog Circuit; I2C bus operation. Blinks when I2C bus is operating properly
D2-6 SPARE
When lit the valve opens the REFERENCE
D71 Green Photometer Meas/Ref Valve
gas path
When lit the valve open to O3 generator gas
D82 Green O3 generator Valve status
path
D9 Green Photometer Pump status When lit the pump is turned on.
D61,2 Yellow GPT Valve status When lit the valve opens the GT Chamber
D10 - 14 SPARE
When lit the photometer UV lamp heater is
D151 Yellow Photometer Heater Status
on
When lit the O3 generator UV lamp heater is
D162 Yellow O3 Generator Heater Status
on
1 Only applies on calibrators with photometer options installed.
2 Only applies on calibrators with O3 generator options installed.
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 201
8.3.3. VALVE DRIVER PCA
A valve driver PCA controls the valves that operate the main source gas and diluent gas
inputs. Like the relay board, this PCA communicates with the CPU through the
motherboard over the I2C bus.
202 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
8.3.4. MOTHERBOARD
This is the largest electronic assembly in the calibrator and is the base for the CPU board
and all I/O connectors. This PCA provides a multitude of functions including A/D
conversion, digital input/output, PC-104 to I2C translation, temperature sensor signal
processing and is a pass through for the RS-232 and RS-485 signals.
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 203
8.3.4.5. EXTERNAL DIGITAL I/O
The external digital I/O performs two functions.
The STATUS outputs carry logic-level (5V) signals through an optically isolated 8-pin
connector on the rear panel. These outputs convey on/off information about certain
conditions, such as SYSTEM OK, and can be used to interface with certain types of
programmable devices.
The CONTROL outputs can be used to initiate actions by external peripheral devices in
conjunction with individual steps of a calibration sequence.
The CONTROL inputs can be initiated by applying 5V DC power from an external source
such as a PLC or data logger (Section 2.6.7.1). Zero and span calibrations can be initiated
by contact closures on the rear panel.
204 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
SENSOR SUITES
AC POWER
Sensor Control
& I/O Logic
DC POWER
ANALOG SENSOR
Photometer UV Detector
Pre-Amplifiers LOGIC DEVICES
& Amplifiers
(e.g. CPU, I2C bus,
Motherboard, etc.)
AC
POWER IN
MFC3
2nd Cal Gas
PS 1
(Optional)
+5 VDC
MFC2
Cal Gas ±15 VDC ON / OFF
RELAY SWITCH
MFC1
(Diluent) PCA
Solenoid PS 2
GAS
TEMPERATURE
Drivers (+12 VDC)
SENSORS
GAS
PRESSURE Cooling
SENSORS OPTIONAL VALVES
• GPT valve,
Fan CAL GAS 1
• O3 Gen valve VALVE
Photometer • Photometer M/R Photometer
UV Lamp P/S valve, etc.)
Pump Solenoid CAL GAS 2
Drivers VALVE
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 205
LCD Display
and
Touchscreen
Back-Light
+5V Supply
TFT BIAS Supply PWM
10.4, -7.0, 16, 4V
Remote
Local
USB & 5V
LAN COM4 USB4
Lang. BLController
Utility Cont.
USB-1 USB-2
The LCD display is controlled directly by the CPU board. The touchscreen is interfaced to
the CPU by means of a touchscreen controller that connects to the CPU via the internal
USB bus and emulates a computer mouse.
206 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
8.4. SOFTWARE OPERATION
The calibrator’s core module is a high performance, X86-based microcomputer running
Windows CE. On top of the Windows CE shell, special software developed by Teledyne
API interprets user commands from various interfaces, performs procedures and tasks and
stores data in the CPU’s memory devices. Figure 8-11 shows a block diagram of this
software functionality.
Windows CE
API FIRMWARE
CALIBRATOR
HARDWARE
Interface Handling
• Gas mixture • Sensor input Data
Algorithms Touchscreen
• Measurement • Analog Output Data
Algorithms for • RS232 & RS485 PC/104 BUS
photometer • External Digital I/O
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 207
8.5. O3 GENERATOR OPERATION
To GPT
Chamber O3 Gen 6O2 + hv185 = 3O3
Valve
O3
Out
Flow
Control
To O3 Assembly
Exhaust
208 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
8.5.2. O3 GENERATOR – PNEUMATIC OPERATION
Pneumatic flow through the O3 generator is created by supplying zero air (diluent) to it
under pressure. The zero air source must be capable of maintaining a continuous flow rate
of at least 100 cm3/min unless the optional photometer is also installed, in which case the
minimum continuous flow rate must be at least 1.1 LPM.
Input and output gas flow is directed by two valves, both of which must be open:
• The diluent inlet valve: This valve is located on the back panel and
allows diluent / zero air into the calibrator.
• The O3 generation valve. This valve is located on the body of the O3
generator is downstream from the generator chamber itself and directs
the output of the generator to either the GPT mixing chamber or the
exhaust vent at the back of the calibrator.
The rate of flow through the O3 generator is controlled by a 100 cm3/min flow control
assembly positioned between the O3 generation chamber and the O3 generation valve. A
self-adjusting pressure regulator on the zero air (diluent ) supply gas line maintains the
pressure across the critical flow orifice of the flow control assembly (see Section 8.2.1.3).
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 209
Figure 8-13. O3 Generator Valve and Gas Fixture Locations
210 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
MOTHER
Thermistor Interface
BOARD PC 104
CPU Card
O3 Generator Input
Pressure Sensor Disk on
Converter
Module
A/D
O3 Generator UV Lamp
O3 Generator
Lamp Heater
Temperature
Sensor Inputs
Flash
Chip
UV
Lamp
I2C Bus
O3 Generator
Lamp Supply
O3 Generator
RELAY PCA
O3 Generator GPT
I2C
Valve Status Valve
LED
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 211
8.5.3.1. O3 GENERATOR TEMPERATURE CONTROL
In order to operate at peak efficiency the UV lamp of the calibrator’s O3 generator is
maintained at a constant 48ºC. If the lamp temperature falls below 43ºC or rises above 53ºC
a warning is issued by the calibrators CPU.
This temperature is controlled as described in the Section on the Relay PCA
(Section 8.3.2). The location of the thermistor and heater associated with the O3 generator
is shown in Figure 8-16:
UV Lamp
O3 Generator
Heater Control PCA
(Heater is located beneath
the PCA)
UV Lamp
Thermistor
212 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
light after it passes through the gas in the tube with and without O3 present. The ratio of
the UV light intensity between the measure phase (O3 present) and the reference phase (no
O3 present) is a key component, along with other data such as the current temperature and
pressure of the gas, to the CPU’s calculating the O3 content.
I = I0 e -αLC at STP
Where:
α is the absorption coefficient that tells how well O absorbs light at the specific
3
wavelength of interest.
To solve this equation for C, the concentration of the absorbing Gas (in this case O3), the
application of algebra is required to rearrange the equation as follows:
Equation 8-6
Io 1
C = ln ×
I αL at STP
Unfortunately, both ambient temperature and pressure influence the density of the sample
gas and therefore the number of ozone molecules present in the absorption tube thus
changing the amount of light absorbed.
In order to account for this effect the following addition is made to the equation:
Equation 8-7
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 213
Io 1 Τ 29.92 inHg
C = ln × × ×
I αL 273 o Κ Ρ
Where:
I 10 9 Τ 29.92 inHg
C = ln o × × ×
I αL 273 o Κ Ρ
The calibrator photometer:
• Measures each of the variables: ambient temperature and ambient gas
pressure; the intensity of the UV light beam with and without O3 present;
• Inserts known values for the length of the absorption path and the
absorption coefficient;
• Calculates the concentration of O3 present in the sample gas.
214 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
Instrument Chassis
O3 FLOW
Pressure
SENSOR
Regulator O3 GAS INPUT
PRESSURE SENSOR
DILUENT
O3 Generator Assembly
GENERATOR
INLET PHOTOMETER
grn grn
PRESSURE SENSOR On Back Panel
DILUENT
O3
Valve O3 GEN / PHOTOMETER
PRESSURE / FLOW SENSOR PCA vio PHOTOMETER
INLET
brn
Flow Control REF/MEAS vio
Valve
(800 cm3)
Flow Control
Purge brn brn
(100 cm3)
Valve
wht
DILUENT Diluent PUMP wht PHOTOMETER
PRESSURE SENSOR
PHOTOMETER
O3 Gen
PCA
ZERO OUT
Valve gry
CAL GAS 2
INLET
INTERNAL
CAL GAS blk VENT
PRESSURE red
CAL GAS 3 SENSOR blk
INLET EXHAUST
GPT
orn
Valve
CAL GAS 4
orn
PHOTOMETER
INLET OUTLET
yel
yel red
GAS INPUT MANIFOLD yel
(on back panel) yel CAL GAS
Cal Gas OUTPUT 1
Mass Flow Controller 1
CAL GAS
GPT blu
OUTPUT 2
Volume
VENT
blu
GAS OUTPUT MANIFOLD
Instrument Chassis
Pressure
SENSOR
DILUENT
O3 Generator Assembly
INLET PHOTOMETER
grn grn
PRESSURE SENSOR On Back Panel
DILUENT
O3
Valve
wht
DILUENT Diluent PUMP wht PHOTOMETER
PRESSURE SENSOR
PHOTOMETER
O3 Gen
PCA
ZERO OUT
Valve gry
CAL GAS 2
INLET
INTERNAL
CAL GAS blk VENT
PRESSURE red
CAL GAS 3 SENSOR blk
INLET EXHAUST
GPT
orn
Valve
CAL GAS 4
orn
PHOTOMETER
INLET OUTLET
yel
yel red
GAS INPUT MANIFOLD yel
(on back panel) yel CAL GAS
Cal Gas OUTPUT 1
Mass Flow Controller 1
CAL GAS
GPT blu
OUTPUT 2
Volume
VENT
blu
GAS OUTPUT MANIFOLD
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 215
8.6.1.3. THE ABSORPTION PATH
In the most basic terms, the calibrator photometer uses a high energy, mercury vapor lamp
to generate a beam of UV light. This beam passes through a window of material specifically
chosen to be both non-reactive to O3 and transparent to UV radiation at 254nm and into an
absorption tube filled with sample gas.
Because ozone is a very efficient absorber of UV radiation the absorption path length
required to create a measurable decrease in UV intensity is short enough (approximately
42 cm) that the light beam is only required to make one pass through the Absorption Tube.
Therefore, no complex mirror system is needed to lengthen the effective path by bouncing
the beam back and forth.
Finally, the UV passes through a similar window at the other end of the absorption tube
and is detected by a specially designed vacuum diode that only detects radiation at or very
near a wavelength of 254nm. The specificity of the detector is high enough that no extra
optical filtering of the UV light is needed.
The detector reacts to the UV light and outputs a current signal that varies in direct
relationship with the intensity of the light shining on it. This current signal is amplified and
converted to a 0 to 5 VDC voltage analog signal voltage sent to the instrument’s
motherboard where it is digitized. The CPU to be uses this digital data in computing the
concentration of O3 in the absorption tube.
Window Window
UV Detector
ABSORPTION TUBE
216 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
8.6.2. PHOTOMETER LAYOUT
The photometer is where the absorption of UV light by ozone is measured and converted
into a voltage. It consists of several sub-assemblies:
• A mercury-vapor UV lamp. This lamp is coated in a material that optically
screens the UV radiation output to remove the O3 producing 185nm
radiation. Only light at 254nm is emitted.
• An AC power supply to supply the current for starting and maintaining
the plasma arc of the mercury vapor lamp.
• A thermistor and DC heater attached to the UV Lamp to maintain the
Lamp at an optimum operating temperature.
• 42 cm long quartz absorption tube.
• A thermistor attached to the quartz tube for measuring sample gas
temperature.
• Gas inlet and outlet mounting blocks that route sample gas into and out
of the photometer.
• The vacuum diode, UV detector that converts UV light to a DC current.
• A preamplifier assembly, which convert the Detector’s current output into
a DC Voltage then amplifies it to a level readable by the A-to-D converter
circuitry of the instrument’s motherboard.
•
UV Lamp Power Sample Gas UV Lamp Thermistor
UV Detector Absorption Tube Transformer Thermistor (UV Lamp Heater Behind Thermistor)
Power Connector
from
+15 VDC power supply Sample Gas
Outlet
UV Detector Sample Gas Inlet UV Lamp Power UV Lamp Heater
Preamp PCA Supply UV Lamp
Control PCA
(200 VAC @ 30 kHz)
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 217
flow control assembly containing a critical flow orifice directly upstream of the pump but
down stream from the absorption tube.
The critical flow orifice installed in the pump supply line is tuned to create a flow of 800
cm3/min. A pressure sensor and a flow sensor, located on the O3 generator/photometer
pressure flow sensor pca, monitor the pressure and flow rate of the gas passing through the
photometers absorption tube.
See Figure 8-17 and Figure 8-18 for depictions of the airflow related to the photometer.
Converter Disk on
Module
Flash
Photometer 2 Chip
Sample Gas
I C Bus
Thermistor Interface
Pressure
Sensor
RELAY PCA
Photometer M/R
Valve
Photometer I2C y (Located on 03
Detector Status Generator Assembly)
Photometer LED
Preamp Photometer UV Lamp
Sample Gas Temperature
Temperature
Photometer
Lamp Heater
Photometer
Like the O3 generator, the O3 photometer and its subcomponents act as peripheral devices
operated by the CPU via the motherboard. Communications to and from the CPU are
handled by the motherboard.
Outgoing commands for the various devices such as the photometer pump, the UV lamp
power supply, or the UV Lamp heater are issued via the I2C bus to circuitry on the relay
PCA which turns them ON/OFF. The CPU also issues commands over the I2C bus that
cause the relay PCA to cycle the measure/reference valve back and forth.
Incoming data from the UV light detector is amplified locally then converted to digital
information by the motherboard. Output from the photometer’s temperature sensors is also
amplified and converted to digital data by the motherboard. The O3 concentration of the
sample gas is computed by the CPU using this data (along with gas pressure and flow data
received from the calibrator’s pressure sensors.
218 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
8.6.4.1. O3 PHOTOMETER TEMPERATURE CONTROL
In order to operate at peak efficiency, the UV lamp of the calibrator’s O3 photometer is
maintained at a constant 58ºC. This is intentionally set at a temperature higher than the
ambient temperature of the calibrator’s operating environment to ensure that local changes
in temperature do not affect the UV Lamp. If the lamp temperature falls below 56ºC or
rises above 61ºC a warning is issued by the calibrator’s CPU.
This temperature is controlled as described in the Section on the relay pca (Section 8.3.2.2).
The following functions report these temperatures and are viewable from the instrument’s
front panel:
• Photo Lamp Temp - The temperature of the UV Lamp reported in ºC.
• Photo Samp Temp - The temperature of the Sample gas in the
absorption tube reported in ºC.
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 219
GLOSSARY
Note: Some terms in this glossary may not occur elsewhere in this manual.
TERM DESCRIPTION/DEFINITION
an Ethernet standard that uses twisted (“T”) pairs of copper wires to
10BaseT
transmit at 10 megabits per second (Mbps)
100BaseT same as 10BaseT except ten times faster (100 Mbps)
name of a remote control program offered by Teledyne-API to its
APICOM
customers
ASSY Assembly
CAS Code-Activated Switch
Corona Discharge, a frequently luminous discharge, at the surface of a
conductor or between two conductors of the same transmission line,
CD
accompanied by ionization of the surrounding atmosphere and often
by a power loss
Converter Efficiency, the percentage of light energy that is actually
CE
converted into electricity
CEM Continuous Emission Monitoring
Chemical formulas that may be included in this document:
CO2 carbon dioxide
C3H8 propane
CH4 methane
H2O water vapor
HC general abbreviation for hydrocarbon
HNO3 nitric acid
H2S hydrogen sulfide
NO nitric oxide
NO2 nitrogen dioxide
NOx nitrogen oxides, here defined as the sum of NO and NO2
nitrogen oxides, often called odd nitrogen: the sum of NOx plus other
NOy compounds such as HNO3 (definitions vary widely and may include
nitrate (NO3), PAN, N2O and other compounds as well)
NH3 ammonia
O2 molecular oxygen
O3 ozone
SO2 sulfur dioxide
metric abbreviation for cubic centimeter (replaces the obsolete
cm3
abbreviation “cc”)
CPU Central Processing Unit
DAC Digital-to-Analog Converter
DAS Data Acquisition System
DCE Data Communication Equipment
220 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
TERM DESCRIPTION/DEFINITION
DFU Dry Filter Unit
Dynamic Host Configuration Protocol. A protocol used by LAN or
Internet servers to automatically set up the interface protocols between
DHCP
themselves and any other addressable device connected to the
network
DIAG Diagnostics, the diagnostic settings of the analyzer.
Disk On Module, a 44-pin IDE flash drive with up to 256MB storage
DOM
capacity for instrument’s firmware, configuration settings and data
DOS Disk Operating System
DRAM Dynamic Random Access Memory
DR-DOS Digital Research DOS
DTE Data Terminal Equipment
Electrically Erasable Programmable Read-Only Memory also referred
EEPROM
to as a FLASH chip or drive
ESD Electro-Static Discharge
ETEST Electrical Test
a standardized (IEEE 802.3) computer networking technology for local
Ethernet area networks (LANs), facilitating communication and sharing
resources
Fluorinated Ethylene Propylene polymer, one of the polymers that
FEP
Du Pont markets as Teflon®
Flash non-volatile, solid-state memory
Fabry-Perot Interface: a special light filter typically made of a
FPI transparent plate with two reflecting surfaces or two parallel, highly
reflective mirrors
GFC Gas Filter Correlation
a clocked, bi-directional, serial bus for communication between
I2C bus
individual analyzer components
Integrated Circuit, a modern, semi-conductor circuit that can contain
IC many basic components such as resistors, transistors, capacitors etc
in a miniaturized package used in electronic assemblies
IP Internet Protocol
IZS Internal Zero Span
LAN Local Area Network
LCD Liquid Crystal Display
LED Light Emitting Diode
LPM Liters Per Minute
MFC Mass Flow Controller
M/R Measure/Reference
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 221
TERM DESCRIPTION/DEFINITION
the mass, expressed in grams, of 1 mole of a specific substance.
Conversely, one mole is the amount of the substance needed for the
molar mass to be the same number in grams as the atomic mass of
that substance.
MOLAR MASS
EXAMPLE. The atomic weight of Carbon is 12 therefore the molar
mass of Carbon is 12 grams. Conversely, one mole of carbon equals
the amount of carbon atoms that weighs 12 grams.
Atomic weights can be found on any Periodic Table of Elements.
NDIR Non-Dispersive Infrared
National Institute of Standards and Technology - Standard Reference
NIST-SRM
Material
PC Personal Computer
Printed Circuit Assembly, the PCB with electronic components, ready
PCA
to use
PC/AT Personal Computer / Advanced Technology
PCB Printed Circuit Board, the bare board without electronic component
Per-Fluoro-Alkoxy, an inert polymer; one of the polymers that Du Pont
PFA
markets as Teflon®
Programmable Logic Controller, a device that is used to control
PLC
instruments based on a logic level signal coming from the analyzer
PLD Programmable Logic Device
PLL Phase Lock Loop
Photo Multiplier Tube, a vacuum tube of electrodes that multiply
PMT
electrons collected and charged to create a detectable current signal
P/N (or PN) Part Number
PSD Prevention of Significant Deterioration
Poly-Tetra-Fluoro-Ethylene, a very inert polymer material used to
PTFE handle gases that may react on other surfaces; one of the polymers
that Du Pont markets as Teflon®
PVC Poly Vinyl Chloride, a polymer used for downstream tubing
Rdg Reading
specification and standard describing a serial communication method
between DTE (Data Terminal Equipment) and DCE (Data Circuit-
RS-232
terminating Equipment) devices, using a maximum cable-length of 50
feet
specification and standard describing a binary serial communication
RS-485 method among multiple devices at a data rate faster than RS-232 with
a much longer distance between the host and the furthest device
SAROAD Storage and Retrieval of Aerometric Data
SLAMS State and Local Air Monitoring Network Plan
Standard Liters Per Minute of a gas at standard temperature and
SLPM
pressure
STP Standard Temperature and Pressure
222 Teledyne API Models T700 and T700U Calibrators 083730700C DCN8250
TERM DESCRIPTION/DEFINITION
Transfer Control Protocol / Internet Protocol, the standard
TCP/IP
communications protocol for Ethernet devices
TEC Thermal Electric Cooler
TPC Temperature/Pressure Compensation
Universal Serial Bus: a standard connection method to establish
USB communication between peripheral devices and a host controller, such
as a mouse and/or keyboard and a personal computer or laptop
VARS Variables, the variable settings of the instrument
V-F Voltage-to-Frequency
Z/S Zero / Span
083730700C DCN8250 Teledyne API Models T700 and T700U Calibrators 223
APPENDIX A: MODBUS Register Map
D D
Analog Control RS-232 RS-485
OutJ1020 In 11004 Jl013 JI0IO& 1011
AC POWER
AC POWER SWITCH
Motherboard ENTRANCE 1---+-.+----1 �
058021400
�
04671
-------0 ·-------------------------
VALVE
MD OPT Jl07 nDRIVER BD 036490100
05469
-----,I 06746 J12
r-------1 r-------1
....,_:
UV LAMP
I
:I I I I UV LAMP
r-_-_-_-_-_-
..___t-_- _-_-_-_-_-_-_-_-_-_-_-_.-+-----------f.lo..+...J n J20----0n
DRIVER 04775
Mi
J106 J27
-,
: : Jl5 I I 03 I I
-;---t-t----;------;-;'---�-�- r------, L _______ J L _______ J
I \
C I Bench Htr
041440000 I
r-------1 r-------1 C
ANALOG IN OPT \
UV LAMP I
L--� 03829 '-------...J I I UV LAMP
06760 : 06737
r------, n DRIVER J2D------Dn 04776
I \ I BENCH
I I I
'' I 03 Gen Htr L _______ J L _______ J
'"------------ \ 041440100 I
,------,
I CAL2 : i---- J12 I \
L _____ J Meas/Ref Viv 1
04105 Jl3
\ 05522 t
..
... ... ... ...
,------"""
'-------...J
"' .,.,... 1
Jl4 /,, Pump ...,,\ 03 Valve '
Jl5 05522 )
J2
I \
LCD w/Touchscreen I \ '\... ______ ...J
J9 Cntrl Mod
LCD Interface
06790 i 04702 j
07215 06697 JI0 0
L _______________ J
I
J1
PRINTED DOCUMENTS ARE UNCONTROLLED
KEY:
1. All part numbers in Italic identify
cables that are refered to in the
A accompanying document 069140100.
2. All items in Dashed boxes are
optional.
SCALE
1/1 F"ILE Q 6 g 1 4 SHEET 1 OF 1
1 2 4