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ASTM B564 (2011) - Standard Specification For Nickel Alloy Forgings

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100% found this document useful (1 vote)
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ASTM B564 (2011) - Standard Specification For Nickel Alloy Forgings

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Designation: B564 – 11

Standard Specification for


Nickel Alloy Forgings1
This standard is issued under the fixed designation B564; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.

1. Scope* 1.1.2 Nickel-iron-chromium-tungsten alloy UNS N06674 is


1.1 This specification2 covers forgings of: normally employed in service temperatures above 1100°F
Alloy Type UNS Number(s)
(593°C) where resistance to creep and rupture is required, and
Fe-Ni-Cr-Mo-N N08367 is annealed to develop optimum properties in this temperature
Low-carbon Cr-Ni-Fe-N R20033 range.
Low-carbon Ni-Cr-Mo N06035, N06058, N06059
Low-carbon Ni-Cr-Mo-Cu N06200
1.2 The values stated in inch-pound units are to be regarded
Low-carbon Ni-Cr-Mo-W N06686 as standard. The values given in parentheses are mathematical
Low-carbon Ni-Fe-Cr-Mo-Cu N08031 conversions to SI units that are provided for information only
Low-carbon Ni-Mo-Cr N10276, N06022, N10362
Low-carbon Ni-Mo-Cr-Ta N06210
and are not considered standard.
Ni N02200 1.3 This standard does not purport to address all of the
Ni-Co-Cr-Si N12160 safety concerns, if any, associated with its use. It is the
Ni-Cr-Co-Mo N06617
Ni-Cr-Fe N06600, N06603, N06690 responsibility of the user of this standard to become familiar
Ni-Cr-Fe-Al N06025 with all hazards including those identified in the appropriate
Ni-Cr-Fe-Si N06045 Material Safety Data Sheet (MSDS) for this product/material
Ni-Cr-Mo-Nb N06625
Ni-Cr-Mo-Si N06219 as provided by the manufacturer, to establish appropriate
Ni-Cr-Mo-W N06110 safety and health practices, and determine the applicability of
Ni-Cr-W-Mo N06230 regulatory limitations prior to use.
Ni-Cu N04400
Ni-Fe-Cr N08120, N08800, N08810, N08811
Ni-Fe-Cr-Mo-Cu N08825
2. Referenced Documents
Ni-Fe-Cr-W N06674 2.1 ASTM Standards:3
Ni-Mo N10665, N10675, N10629
Ni-Mo-Cr-Fe N10242, N10624 B880 Specification for General Requirements for Chemical
Check Analysis Limits for Nickel, Nickel Alloys and
1.1.1 The nickel-iron-chromium alloys are UNS N08120, Cobalt Alloys
UNS N08800, UNS N08810, and UNS N08811. Alloy UNS E8 Test Methods for Tension Testing of Metallic Materials
N08800 is normally employed in service temperatures up to E29 Practice for Using Significant Digits in Test Data to
and including 1100°F (593°C). Alloys UNS N08810, N08120, Determine Conformance with Specifications
and UNS N08811 are normally employed in service tempera- E76 Test Methods for Chemical Analysis of Nickel-Copper
tures above 1100°F (593°C) where resistance to creep and Alloys4
rupture is required, and are annealed to develop controlled E112 Test Methods for Determining Average Grain Size
grain size for optimum properties in this temperature range. E350 Test Methods for Chemical Analysis of Carbon Steel,
Low-Alloy Steel, Silicon Electrical Steel, Ingot Iron, and
Wrought Iron
1
This specification is under the jurisdiction of ASTM Committee B02 on E1473 Test Methods for Chemical Analysis of Nickel,
Nonferrous Metals and Alloys and is the direct responsibility of Subcommittee
B02.07 on Refined Nickel and Cobalt and Their Alloys.
Current edition approved Oct. 1, 2011. Published November 2011. Originally
3
approved in 1972. Last previous edition approved in 2010 as B564 – 10. DOI: For referenced ASTM standards, visit the ASTM website, www.astm.org, or
10.1520/B0564-11. contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
2
For ASME Boiler and Pressure Vessel Code applications see related Specifi- Standards volume information, refer to the standard’s Document Summary page on
cation SB-564 in Section II of that Code. the ASTM website.
4
* New designations established in accordance with ASTM E527 and SAE J1086, Withdrawn. The last approved version of this historical standard is referenced
Practice for Numbering Metals and Alloys (UNS). on www.astm.org.

*A Summary of Changes section appears at the end of this standard.


Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
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B564 – 11
Cobalt, and High-Temperature Alloys 8.2.1 Chemical Analysis—Representative samples shall be
2.2 Military Standards:5 taken during pouring or subsequent processing.
MIL-STD-129 Marking for Shipment and Storage 8.2.1.1 Product (check) analysis shall be wholly the respon-
MIL-STD-271 Nondestructive Testing Requirements for sibility of the purchaser.
Metals 8.2.2 Mechanical Properties and Grain Size—Samples of
the material to provide test specimens for mechanical proper-
3. Ordering Information ties and grain size shall be taken from such locations in each lot
3.1 It is the responsibility of the purchaser to specify all as to be representative of that lot.
requirements that are necessary for material ordered under this
specification. Examples of such requirements include, but are 9. Number of Tests
not limited to, the following: 9.1 Chemical Analysis—One test per lot.
3.1.1 Alloy (Table 1).
9.2 Mechanical Properties—One test per lot.
3.1.2 Condition (Table 2).
9.3 Grain Size—For alloys N08810, N08120, UNS N08811,
3.1.3 Quantity (mass or number of pieces).
and N06674, one test per lot.
3.1.4 Forging, sketch or drawing.
3.1.5 Certification—State if certification or a report of test
10. Specimen Preparation
results is required (14.1).
3.1.6 Samples for Product (Check) Analysis—Whether 10.1 The tension test specimen representing each lot shall
samples for product (check) analysis should be furnished (see be taken from a forging or from a test prolongation.
4.2). 10.2 The axis of the specimen shall be located at any point
3.1.7 Purchaser Inspection—If the purchaser wishes to midway between the center and the surface of solid forgings
witness tests or inspection of material at the place of manu- and at any point midway between the inner and outer surfaces
facture, the purchase order must so state indicating which tests of the wall of hollow forgings, and shall be parallel to the
or inspections are to be witnessed (12.1). direction of greatest metal flow.

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10.3 The specimens shall be the largest possible round type
4. Chemical Composition shown in Test Methods E8.
4.1 The material shall conform to the composition limits
specified in Table 1. 11. Test Methods
4.2 If a product (check) analysis is performed by the 11.1 The chemical composition, mechanical, and other
purchaser, the material shall conform to the product (check) properties of the material as enumerated in this specification
analysis variations in accordance with Specification B880. shall be determined, in case of disagreement, in accordance
with the following methods:
5. Mechanical Properties and Other Requirements
Test ASTM Designation
5.1 Mechanical Properties—The material shall conform to Chemical Analysis E76, E350, E1473
the mechanical properties specified in Table 2. Tension E8
Rounding Procedure E29
5.2 Grain Size—Annealed alloys UNS N08810, N08120, Grain Size E112
and UNS N08811 shall conform to an average grain size of
ASTM No. 5 or coarser. Annealed alloy UNS N06674 shall 11.2 The measurement of average grain size may be carried
conform to an average grain size of ASTM No. 7 or coarser. out by the planimetric method, the comparison method, or the
intercept method described in Test Methods E112. In case of
6. Dimensions and Permissible Variations dispute, the “referee” method for determining average grain
6.1 Dimensions and tolerances shall be as specified on the size shall be the planimetric method.
applicable forging sketch or drawing. 11.3 For purposes of determining compliance with the
specified limits for requirements of the properties listed in the
7. Workmanship, Finish and Appearance following table, an observed value, or a calculated value, shall
7.1 The material shall be uniform in quality and condition, be rounded as indicated as follows, in accordance with the
sound, and free of injurious imperfections. rounding method of Practice E29:
Rounded Unit for Observed or
8. Sampling Test Calculated Value
Chemical composition nearest unit in the last right-hand place
8.1 Lot Definition: of figures of the specified limit
8.1.1 A lot for chemical analysis shall consist of one heat. Tensile strength, yield strength nearest 1000 psi (6.9 MPa)
Elongation nearest 1 %
8.1.2 A lot for mechanical properties and grain size testing Grain size:
shall consist of all material from the same heat, size, finish, 0.0024 in. (0.060 mm) or larger nearest multiple of 0.0002 in. (0.005 mm)
condition, and processed at one time. less than 0.0024 in. (0.060 mm) nearest multiple of 0.0001 in. (0.002 mm)
8.2 Test Material Selection:
12. Inspection
5 12.1 Inspection of the material by the purchaser shall be
Available from Standardization Documents Order Desk, DODSSP, Bldg. 4,
Section D, 700 Robbins Ave., Philadelphia, PA 19111-5098, http:// made as agreed upon between the purchaser and the seller as
www.dodssp.daps.mil. part of the purchase contract.

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B564 – 11

TABLE 1 Chemical RequirementsA


Composition, %
Low- Low- Low- Low-
Nickel- Nickel-
Carbon Carbon Nickel- Carbon Carbon
Nickel- Chromium- Chromium-
Nickel Nickel- Nickel- Chromium- Nickel- Nickel-
Element Copper Iron- Molybdenum-
Alloy Molybdenum- Chromium- Iron-Silicon Chromium- Chromium-
Alloy Aluminum Tungsten
Chromium Molybdenum Alloy Molybdenum Molybdenum
Alloy Alloy
Alloy Alloy Alloy Alloy
UNS UNS UNS UNS UNS UNS UNS UNS UNS
N02200 N04400 N06022 N06025 N06035 N06045 N06058 N06059 N06110
Nickel 99.0B min 63.0B min balanceB balance balanceB 45 min balance balanceB 51.0B min
Copper 0.25 28.0–34.0 ... 0.10 0.30 0.3 0.50 0.50 0.50
Iron 0.40 2.5 2.0–6.0 8.0–11.0 2.00 21.0–25.0 1.5 1.5 1.0
Manganese 0.35 2.0 0.50 0.15 0.50 1.0 0.50 0.5 1.0
Carbon 0.15 0.3 0.015 0.15–0.25 0.050 0.05–0.12 0.010 0.010 0.15
Silicon 0.35 0.5 0.08 0.5 0.60 2.5–3.0 0.10 0.10 1.0
Sulfur 0.01 0.024 0.02 0.01 0.015 0.010 0.010 0.010 0.015
Chromium ... ... 20.0–22.5 24.0–26.0 32.25–34.25 26.0–29.0 20.0–23.0 22.0–24.0 28.0–33.0
Aluminum ... ... ... 1.8–2.4 0.40 ... 0.40 0.1–0.4 1.0

--`,``,,`,`,`,`,`,,`,,```,,```,-`-`,,`,,`,`,,`---
Titanium ... ... ... 0.1–0.2 ... ... ... ... 1.0
Columbium ... ... ... ... ... ... ... ... 1.0
(Nb) +
Tantalum
Molybdenum ... ... 12.5–14.5 ... 7.60–9.00 ... 19.0 - 21.0 15.0–16.5 9.0–12.0
Phosphorus ... ... 0.02 0.02 0.030 0.02 0.015 0.015 0.50
Tungsten ... ... 2.5–3.5 ... 0.60 ... 0.3 ... 1.0-4.0
Cobalt ... ... 2.5 ... 1.00 ... 0.3 0.3 ...
Vanadium ... ... 0.35 ... 0.20 ... ... ... ...
Nitrogen ... ... ... ... ... ... 0.02 - 0.15 ... ...
Boron ... ... ... ... ... ... ... ... ...
Lanthanum ... ... ... ... ... ... ... ... ...
Aluminum + ... ... ... ... ... ... ... ... ...
Titanium
Nickel + ... ... ... ... ... ... ... ... ...
Molybdenum
Columbium ... ... ... ... ... ... ... ... ...
(Nb)
Tantalum ... ... ... ... ... ... ... ... ...
Zirconium ... ... ... 0.01–0.10 ... ... ... ... ...
Cerium ... ... ... ... ... 0.03–0.09 ... ... ...
Yttrium ... ... ... 0.05–0.12 ... ... ... ... ...
A
Maximum unless range or minimum is given. Where ellipses (...) appear in this table there is no requirement and the element need neither be analyzed for nor reported.
B
Element shall be determined arithmetically by difference.

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B564 – 11

TABLE 1 Chemical RequirementsA (continued)


Composition, %
Low-
Low-Carbon
Carbon Nickel- Nickel Nickel- Nickel Nickel- Nickel-
Nickel- Nickel-
Nickel- Chromium- Chromium- Chromium- Chromium- Chromium- Iron-
Molybdenum- Chromium-
Element Chromium- Molybdenum- Tungsten- Iron- Cobalt- Molybdenum- Chromium-
Chromium- Iron
Molybdenum- Silicon Molybdenum Aluminum Molybdenum Columbium Tungsten
Tantalum Alloy
Copper Alloy Alloy Alloy Alloy Alloy Alloy
Alloy
Alloy
UNS UNS UNS UNS UNS UNS UNS UNS UNS
N06200 N06210 N06219 N06230 N06603 N06617 N06625 N06600 N06674
Nickel balanceB balanceB balanceB balanceB balanceB 44.5 min 58.0B min 72.0B min balanceB
Copper 1.3–1.9 ... 0.50 ... 0.5 0.5 ... 0.5 ...
Iron 3.0 1.0 2.0-4.0 3.0 8.0–11.0 3.0 5.0 6.0–10.0 20.0-27.0
Manganese 0.50 0.5 0.50 0.30–1.00 0.15 1.0 0.5 1.0 1.50
Carbon 0.010 0.015 0.05 0.05–0.15 0.20–0.40 0.05–0.15 0.10 0.15 0.10
Silicon 0.08 0.08 0.70-1.10 0.25–0.75 0.5 1.0 0.5 0.5 1.0
Sulfur 0.010 0.02 0.010 0.015 0.010 0.015 0.015 0.015 0.015
Chromium 22.0–24.0 18.0-20.0 18.0-22.0 20.0–24.0 24.0–26.0 20.0–24.0 20.0–23.0 14.0–17.0 21.5-24.5
Aluminum 0.50 ... 0.50 0.50 2.4–3.0 0.8–1.5 0.4 ... ...
Titanium ... ... 0.50 ... 0.01–0.25 0.6 0.4 ... 0.05-0.20
Columbium ... ... ... ... ... ... 3.15–4.15 ... ...

--`,``,,`,`,`,`,`,,`,,```,,```,-`-`,,`,,`,`,,`---
(Nb) +
Tantalum
Molybdenum 15.0–17.0 18.0-20.0 7.0-9.0 1.0–3.0 ... 8.0–10.0 8.0–10.0 ... ...
Phosphorus 0.025 0.02 0.020 0.030 0.02 ... 0.015 ... 0.030
Tungsten ... ... ... 13.0–15.0 ... ... ... ... 6.0-8.0
Cobalt 2.0 1.0 1.0 5.0 ... 10.0 min– ... ... ...
15.0
Vanadium ... 0.35 ... ... ... ... ... ... ...
Nitrogen ... ... ... ... ... ... ... ... 0.02
Boron ... ... ... 0.015 ... 0.006 ... ... 0.0005-
0.006
Lanthanum ... ... ... 0.005–0.050 ... ... ... ... ...
Aluminum + ... ... ... ...
Titanium
Nickel + ... ... ... ... ... ... ... ... ...
Molybdenum
Columbium ... ... ... ... ... ... ... ... 0.10-0.35
(Nb)
Tantalum ... 1.5-2.2 ... ... ... ... ... ... ...
Zirconium ... ... ... ... 0.01–0.10 ... ... ... ...
Cerium ... ... ... ... ... ... ... ... ...
Yttrium ... ... ... ... 0.01–0.15 ... ... ... ...
A
Maximum unless range or minimum is given. Where ellipses (...) appear in this table there is no requirement and the element need neither be analyzed for nor reported.
B
Element shall be determined arithmetically by difference.

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B564 – 11

TABLE 1 Chemical RequirementsA (continued)


Composition, %
Low-
Low-
Carbon Iron- Nickel-
Carbon
Nickel- Nickel- Nickel- Nickel- Nickel- Iron-
Nickel- Nickel-Iron- Nickel-Iron-
Chromium- Iron- Iron- Chromium- Iron- Chromium-
Element Chromium- Chromium Chromium
Iron Chromium- Chromium Molybdenum- Chromium Molybdenum-
Molybdenum- Alloy Alloy
Alloy Molybdenum- Alloy Nitrogen Alloy Copper
Tungsten
Copper Alloy Alloy
Alloy
Alloy
UNS UNS UNS UNS UNS UNS UNS UNS UNS
N06686 N06690 N08031 N08120 N08367 N08800 N08810 N08811 N08825
Nickel remainder 58.0B min 30.0–32.0 35.0–39.0 23.50–25.50 30.0–35.0 30.0–35.0 30.0–35.0 38.0–46.0
Copper ... 0.5 1.0–1.4 0.50 0.75 0.75 0.75 0.75 1.5–3.0
Iron 5.0 7.0–11.0 balanceB balance balanceB 39.5B min 39.5B min 39.5B min 22.0B min
Manganese 0.75 0.5 2.0 1.5 2.00 1.5 1.5 1.5 1.0
Carbon 0.010 0.05 0.015 0.02–0.10 0.030 0.10 0.05–0.10 0.06–0.10 0.05
Silicon 0.08 0.5 0.3 1.0 1.00 1.0 1.0 1.0 0.5
Sulfur 0.02 0.015 0.010 0.03 0.030 0.015 0.015 0.015 0.03
Chromium 19.0–23.0 27.0–31.0 26.0-28.0 23.0–27.0 20.0–22.0 19.0–23.0 19.0–23.0 19.0–23.0 19.5–23.5
Aluminum ... ... ... 0.40 ... 0.15–0.60 0.15–0.60 0.15–0.60 0.2
Titanium 0.02–0.25 ... ... 0.20 ... 0.15–0.60 0.15–0.60 0.15–0.60 0.6–1.2
Columbium ... ... ... 0.4–0.9 ... ... ... ... ...
(Nb) +
Tantalum
Molybdenum 15.0–17.0 ... 6.0-7.0 2.50 6.00–7.00 ... ... ... 2.5–3.5
Phosphorus 0.04 ... 0.020 0.040 0.040 ... ... ... ...
Tungsten 3.0–4.4 ... ... 2.50 ... ... ... ... ...
Cobalt ... ... ... 3.0 ... ... ... ... ...
Vanadium ... ... ... ... ... ... ... ... ...
Nitrogen ... ... 0.15-0.25 0.15–0.30 0.18–0.25 ... ... ... ...
Boron ... ... ... 0.010 ... ... ... ... ...
Lanthanum ... ... ... ... ... ... ... ... ...
Aluminum + ... ... ... ... ... ... 0.85–1.20 ...
Titanium
Nickel + ... ... ... ... ... ... ... ... ...
Molybdenum
Columbium ... ... ... ... ... ... ... ... ...
(Nb)
Tantalum ... ... ... ... ... ... ... ... ...
Zirconium ... ... ... ... ... ... ... ... ...
Cerium ... ... ... ... ... ... ... ... ...
Yttrium ... ... ... ... ... ... ... ... ...
A
Maximum unless range or minimum is given. Where ellipses (...) appear in this table there is no requirement and the element need neither be analyzed for nor reported.
B
Element shall be determined arithmetically by difference.
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B564 – 11

TABLE 1 Chemical RequirementsA (continued)


Composition, %
Low- Low-
Nickel- Nickel- Nickel-
Carbon Carbon Chromium-
Molybdenum- Molybdenum- Nickel- Nickel- Nickel- Cobalt-
Nickel- Nickel- Nickel-Iron-
Element Chromium- Chromium- Molybdenum Molybdenum Molybdenum Chromium-
Molybdenum- Molybdenum- Nitrogen
Iron Iron Alloy Alloy Alloy Silicon
Chromium Chromium Alloy
Alloy Alloy Alloy
Alloy Alloy
UNS UNS UNS UNS UNS UNS UNS UNS UNS
N10242 N10276 N10362 N10624 N10629 N10665 N10675 N12160 R200033
Nickel balanceB balanceB balanceB balanceB balance balanceB 65.0 min balanceB 30.0–33.0
Copper ... ... ... 0.5 0.5 ... 0.20 ... 0.30–1.20
Iron 2.0 4.0–7.0 1.25 5.0-8.0 1.0–6.0 2.0 1.0–3.0 3.5 balanceB
Manganese 0.80 1.0 0.60 1.0 1.5 1.0 3.0 1.5 2.0
Carbon 0.03 0.010 0.010 0.01 0.010 0.02 0.01 0.15 0.015
Silicon 0.80 0.08 0.08 0.10 0.05 0.10 0.10 2.4–3.0 0.50
Sulfur 0.015 0.03 0.010 0.01 0.01 0.03 0.010 0.015 0.01
Chromium 7.0-9.0 14.5–16.5 13.8-15.6 6.0-10.0 0.5–1.5 1.0 1.0–3.0 26.0–30.0 31.0–35.0
Aluminum 0.50 ... 0.50 0.5 0.1–0.5 ... 0.50 ... ...
Titanium ... ... ... ... ... ... 0.20 0.20–0.80 ...
Columbium ... ... ... ... ... ... ... ... ...
(Nb) +
Tantalum
Molybdenum 24.0-26.0 15.0–17.0 21.5-23.0 21.0-25.0 26.0–30.0 26.0–30.0 27.0–32.0 1.0 0.50–2.0
Phosphorus 0.030 0.04 0.025 0.025 0.04 0.04 0.030 0.030 0.02
Tungsten ... 3.0–4.5 ... ... ... ... 3.0 1.0 ...
Cobalt 1.00 2.5 ... 1.0 2.5 1.00 3.0† 27.0–33.0† ...
Vanadium ... 0.35 ... ... ... ... 0.20 ... ...
Nitrogen ... ... ... ... ... ... ... ... 0.35–0.60
Boron 0.006 ... ... ... ... ... ... ... ...
Lanthanum ... ... ... ... ... ... ... ... ...
Aluminum + ... ... ... ... ... ...
Titanium
Nickel + ... ... ... ... ... ... 94.0–98.0 ... ...
Molybdenum
Columbium ... ... ... ... ... ... 0.20 1.0 ...
(Nb)
Tantalum ... ... ... ... ... ... 0.20 ... ...
Zirconium ... ... ... ... ... ... 0.10 ... ...
Cerium ... ... ... ... ... ... ... ... ...
--`,``,,`,`,`,`,`,,`,,```,,```,-`-`,,`,,`,`,,`---

Yttrium ... ... ... ... ... ... ... ... ...
† Editorially corrected.
A
Maximum unless range or minimum is given. Where ellipses (...) appear in this table there is no requirement and the element need neither be analyzed for nor reported.
B
Element shall be determined arithmetically by difference.

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B564 – 11
TABLE 2 Mechanical Property RequirementsA

Yield Elongation
Maximum Section Strength, in
Tensile Strength,
Material and Condition Thickness, 0.2 % Offset, min, 2 in. or 50
min, ksi (MPa)
in. (mm) ksi (MPa) mm or 4D,
min, %
Iron-nickel-chromium-molybdenum-
nitrogen alloy UNS N08367, ... 95 (655) 45 (310) 30
solution annealed
Low-carbon chromium-nickel-iron-
nitrogen alloy UNS R20033, ... 109 (750) 55 (380) 40
solution annealed
Low-carbon nickel-chromium-
molybdenum
alloy UNS N06035, solution
... 85 (586) 35 (241) 30
annealed
alloy UNS N06058, solution
... 110 (760) 52 (3600 40
annealed
alloy UNS N06059, solution
... 100 (690) 45 (310) 45
annealed
Low-carbon nickel-chromium-
molybdenum-copper alloy ... 100 (690) 45 (310) 45
UNS N06200, solution annealed
Low-carbon nickel-chromium-
molybdenum-tungsten alloy ... 100 (690) 45 (310) 45
UNS N06686, solution annealed
Low-carbon nickel-iron-chromium-
molybdenum-copper-alloy ... 94 (650) 40 (276) 40
UNS N08031, solution annealed
Low-carbon nickel-chromium-
molybdenum alloy UNS N10276, ... 100 (690) 41 (283) 40
solution annealed
Low-carbon nickel-chromium-
molybdenum alloy UNS N06022, ... 100 (690) 45 (310) 45
solution annealed
Low-carbon nickel-molybdenum-
chromium UNS N10362, solution ... 105 (725) 45 (310) 40
annealed

--`,``,,`,`,`,`,`,,`,,```,,```,-`-`,,`,,`,`,,`---
Low-carbon nickel-molybdenum-
chromium-tantalum alloy UNS ... 100 (690) 45 (310) 45
N06210, solution annealed
Nickel alloy UNS N02200,
... 55 (380) 15 (105) 40
annealed
Nickel-cobalt-chromium-silicon alloy
... 90 (620) 35 (240) 40
UNS N12160, solution annealed
Nickel-chromium-cobalt-
molybdenum alloy UNS N06617, ... 95 (655) 35 (241) 35
annealed
Nickel-chromium-iron alloy
... 80 (552) 35 (241) 30
UNS N06600, annealed
Nickel-chromium-iron-aluminum
... 94 (650) 43 (300) 25
alloy UNS N06603, annealed
Nickel-chromium-iron alloy
... 85 (586) 35 (241) 30
UNS N06690, annealed
Nickel-chromium-iron-aluminum Up to 4 (102) 98 (680) 39 (270) 30
alloy UNS N06025, solution Over 4 (102) to 84 (580) 39 (270) 15
annealed 12 (305) incl
Nickel-chromium-iron-silicon alloy
... 90 (620) 35 (240) 35
UNS N06045, solution annealed
Nickel-chromium-molybdenum- Up to 4 (102), incl 120 (827) 60 (414) 30
columbium alloy UNS N06625, Over 4B (102) to 110 (758) 50 (345) 25
annealed 10 (254), incl
Nickel-chromium-molybdenum-
silicon alloy UNS N06219, solution ... 96 (660) 39 (270) 50
annealed
Nickel-chromium-molybdenum- Up to 4 (102), incl 95 (655) 45 (310) 60
tungsten alloy UNS N06110, Over 4 (102) to 90 (621) 40 (276) 50
annealed 10 (254), incl
Nickel-chromium-tungsten-
molybdenum alloy UNS N06230, ... 110 (758) 45 (310) 40
solution annealedC
Nickel-copper alloy UNS N04400,
... 70 (483) 25 (172) 35
annealed
Nickel-iron-chromium alloys:
UNS N08120, solution annealed ... 90 (621) 40 (276) 30
UNS N08800, annealed ... 75 (517) 30 (207) 30

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B564 – 11

TABLE 2 Continued
Yield Elongation
Maximum Section Strength, in
Tensile Strength,
Material and Condition Thickness, 0.2 % Offset, min, 2 in. or 50
min, ksi (MPa)
in. (mm) ksi (MPa) mm or 4D,
min, %
UNS N08810 and UNS N08811,
... 65 (448) 25 (172) 30
annealed
Nickel-iron-chromium-molybdenum-
copper alloy UNS N08825, ... 85 (586) 35 (241) 30
annealed
Nickel-iron-chromium-tungsten alloy
... 86 (590) 34 (235) 30
UNS N06674, solution annealedC
Nickel-molybdenum alloy UNS
... 110 (760) 51 (350) 40
N10665, solution annealed
Nickel-molybdenum alloy UNS
... 110 (760) 51 (350) 40
N10675, solution annealed
Nickel-molybdenum alloy UNS
... 110 (760) 51 (350) 40
N10629, solution annealed
Nickel-molybdenum-chromium-iron
... 105 (725) 45 (310) 40
alloy UNS N10242, annealed
Nickel-molybdenum-chromium-iron
... 104 (720) 46 (320) 40
alloy UNS N10624, annealed
A
Forging quality is furnished to chemical requirements and surface inspection only.
B
Over 4 to 10-in. (102 to 254-mm) diameter for parts machined from forged bar.
C
Solution annealed at a minimum temperature of 2150°F (1177°C) followed by a water quench or rapidly cooled by other means.

13. Rejection and Rehearing results on representative samples meet specification require-
13.1 Material, tested by the purchaser, that fails to conform ments. When specified in the purchase order or contract, a
to the requirements of this specification may be rejected. report of the test results shall be furnished.
Rejection should be reported to the producer or supplier
promptly and in writing. In case of dissatisfaction with the 15. Product Marking
results of the test, the producer or supplier may make claim for 15.1 The material shall be marked legibly with the name of
a rehearing. the material, this specification number, the heat number and
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14. Certification condition, and such other information as may be defined in the
contract or order.
14.1 When specified in the purchase order or contract, a
manufacturer’s certification shall be furnished to the purchaser
16. Keywords
stating that material has been manufactured, tested, and in-
spected in accordance with this specification, and that the test 16.1 nickel alloy forgings

SUPPLEMENTARY REQUIREMENTS

The following supplementary requirements shall apply only when specified by the purchaser in the
inquiry, contract, or order, for agencies of the U.S. Government.

S1. Referenced Documents MIL-STD-792 Copper-Base Alloy Mill Products


S1.1 The following documents of the issue in effect on date
of material purchase form a part of this specification to the S2. Chemical Composition
extent referenced herein. S2.1 UNS alloy N04400 shall conform to the composition
S1.1.1 Federal Standards: limits specified in Table 1 except as specified in Table S2.1
Fed. Std. No. 102 Preservation, Packaging and Packing
Levels S3 Mechanical Properties
Fed. Std. No. 123 Marking for Shipment (Civil Agencies) S3.1 Mechanical property requirements for UNS alloy
Fed. Std. No. 185 Identification Marking of Copper and N04400 forgings in the hot finished and hot finished/high
Copper-Base Alloy Mill Products tensile conditions shall be as specified in Table S3.1
S1.1.2 Military Standards:
MIL-STD-129 Marking for Shipment and Storage S4. Number of Tests
S1.1.3 Military Specification: S4.1 One tensile specimen is required for each forging
MIL-C-3993 Packaging of Copper greater than 250 pounds in as shipped weight.

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TABLE S2.1 Chemical Requirements decrease in the calibrated sensitivity and resolution, or both, or
Composition Limits, % any change in search unit, couplant, instrument settings, or
Element UNS 04400 scanning speed from that used for calibration shall require
Carbon 0.2 max recalibration. Recalibration shall be performed at least once per
Sulfur 0.015 max 8-h shift.
Aluminum 0.5 max
Lead 0.006 max
S5.2.3 Procedure—Paragraphs S 5.2.3.1 through S5.2.3.4
Tin 0.006 max describe the requirements for rod, bar, and simple forged
Zinc 0.02 max shapes.
Phosphorous 0.02 max
S5.2.3.1 Rod—Rod shall be testing using the longitudinal
wave technique. The scanning path shall be circumferential or
helical with the beam directed along a radius of the rod.
S5. Nondestructive Tests S5.2.3.2 Bar—Bar shall be tested using the longitudinal
S5.1 When specified by the purchaser, each piece of each lot wave technique through one side of each pair of parallel sides
shall be inspected. The purchaser shall specify if one or both (thickness and width only).
tests are required. S5.2.3.3 Ring and Hollow Round Products—Rings and other
S5.2 Ultrasonic Tests: hollow cylindrical products shall be tested using the shear
S5.2.1 General Requirements: wave method by the contact or immersion technique. The shear
S5.2.1.1 Ultrasonic testing shall be performed in accordance wave entrant angle shall be such to ensure reflection from the
with MIL-STD-271 as modified by the requirements specified notch or notches used in calibration. For contact testing, the
herein. Testing shall be done by a longitudinal wave or shear search unit shall be fitted with a wedge or shoe machined to fit
wave technique as specified herein. the curvature of the piece being inspected. The product also
S5.2.1.2 Acoustic compatibility between the production shall be inspected with a longitudinal wave test from the
material and the calibration standard material shall be within external circumferential and end surfaces.
75 %. If the acoustic compatibility is within 25 %, no gain S5.2.3.4 Disc or Pancake Forgings—Disc or pancake forg-
compensation is required for the examination. If acoustic ings shall be inspected with a longitudinal wave technique
compatibility difference is between 25 % and 75 %, a change from both parallel surfaces.
in the gain or dB controls shall be accomplished to compensate S5.2.4 Acceptance Criteria:
for the differences in acoustic compatibility. This method S5.2.4.1 Shear Wave—Any material that produces indica-
cannot be used if the ultrasonic noise level exceeds 50 % of the tions equal to or larger than the response from the reference
rejection value. notch or higher than the straight line joining the two peak
S5.2.2 Calibration: amplitudes shall be rejected.
S5.2.2.1 Shear Wave—The shear wave test shall be cali- S5.2.4.2 Longitudinal Wave—Any material that produces
brated on two notches, one notch cut into the inside and one indications equal to or larger than the response from the
into the outside surface. The notches shall be cut axially and reference hole, or that produces a complete loss of back
shall have a depth of 5 % of the material thickness of 1⁄4 in. (6.4 reflection shall be rejected. Material shall be tested using a
mm), whichever is less. Notch length shall not exceed 1 in. square, rectangular, or circular transducer having an effective
(25.4 mm). Notches shall be made either in the piece to be area of one square inch or less, but no dimension shall be
examined or in a separate defect-free specimen of the same size smaller than the diameter of the reference hole. In the event of
(within 61⁄8 in. (3.18 mm), shape, material, and condition, or disagreement on the degree of back reflection loss, it shall be
acoustically similar material. The position and amplitude of the determined by the contact method using a 1 to 1-1/8 in. (25.4
response from each notch shall be marked on the instrument to 28.6 mm) diameter transducer or one whose area falls within
screen or a transparent overly, and these marks shall be used as this range.
the evaluation reference. Indications that appear between these S5.2.4.3 Reference Notch Removal—If reference notches or
points shall be evaluated on the basis of a straight line joining flat-bottomed holes are made in the material to be tested, they
the two peak amplitudes. shall be so located than their subsequent removal will not
S5.2.2.2 Longitudinal Wave—The longitudinal wave test
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impair the suitability of the material for its intended use.


shall be calibrated on a flat-bottomed reference hole of a given
S5.3 Liquid Penetrant Inspection:
diameter in accordance with Table S5.1 for specified material
thickness drilled either into the piece to be tested or into a S5.3.1 Procedure—Liquid penetrant inspection shall be in
separate defect-free specimen of the same size (within 61⁄8 in accordance with MIL-STD-271.
(3.18 mm), shape, material, and condition, or acoustically S5.3.2 Surface Requirements—The surface produced by hot
similar material. Holes are to be drilled to midsection and the working is not suitable for liquid penetrant testing Therefore,
bottom of the hole shall be parallel to the entrant surface. The liquid penetrant testing will not be applicable to products
ultrasonic test instrument shall be adjusted so that the response ordered with a hot finished surface.
from the reference hole shall not be less than 25 % and not S5.3.3 Acceptance Criteria—Linear defects revealed by
more than 75 % of screen height. liquid penetrant inspection shall be explored by grinding or
S5.2.2.3 Recalibration—During quality conformance in- other suitable means. Depth of defects shall not exceed the
spection, any realignment of the search unit that will cause a dimensional tolerance of the material.

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B564 – 11
TABLE S3.1 Mechanical Properties of UNS N04400 Forgings
Condition and Diameter Between Parallel Tensile Strength, min, psi Yield Strength, min, psi (Mpa) Elongation in 2 in. or
Surfaces, in. (mm) (Mpa) (0.2% offset) 50 mm, or 4D, min, %
Hot Finished -to 12 (305) 80 000 (552) 40 000 (276) 30
Hot Finished -over 12 (305) 75 000 (517) 40 000 (276) 30
Hot Finished/High Tensile - Rounds 3 to 6 (76 to 95 000 (655) 70 000 (483) 20
152) inclusive
Hot Finished/High Tensile - Rounds over 6 to 12 85 000 (586) 60 000 (414) 25
(152 to 305) and hex, squares, and flats 3 to 12
(76 to 305)

TABLE S5.1 Ultrasonic Testing Reference Hole for Rod, Bar, specification number and the alloy number shall be used. In
Disc, Pancake Forgings, and Forgings addition, the method and location of marking shall be in
Material Thickness, in. (mm) Hole Diameter, in. (mm) accordance with MIL-STD-792. Forging stock shall be marked
Up to and including 6 (152) ⁄ 5(3.18)
18
with low stress die stamps or vibroetching.
Over 6 (152) and including 16 (406) 1⁄4 (6.4)

Over 16 (406) As agreed upon


S8. Preparation for Delivery

S6. Quality Assurance S8.1 Preservation, Packaging, and Packing:


S6.1 Responsibility for Inspection: S8.1.1 Military Agencies—The material shall be separated
S6.1.1 Unless otherwise specified in the contract or purchase by size, composition, grade, or class, and shall be preserved
order, the manufacturer is responsible for the performance of and packaged level A or C, and packed Level A, B, or C as
all inspections and test requirements specified. Except as specified in the contract or purchase order.
otherwise specified in the contract or purchase order, the S8.1.2 Civil Agencies—The requirements of Fed. Std. No.
manufacturer may use his own or any other suitable facilities 102 shall be referenced for definitions for the various levels of
for the performance of the inspection and test requirements packaging protection.
unless disapproved by the purchaser at the time the order is S8.2 Marking:
placed. The purchaser shall have the right to perform any of the
inspections or tests set forth when such inspections and tests S8.2.1 Military Agencies—In addition to any special mark-
are deemed necessary to ensure that the material conforms to ing required by the contract or purchase order, marking for
prescribed requirements. shipment shall be in accordance with MIL-STD-129.
S8.2.2 Civil Agencies—In addition to any special marking
S7. Identification Marking required by the contract or purchase order, marking for
S7.1 All material shall be properly marked for identification shipment shall be in accordance with Fed. Std. No. 123.
in accordance with Fed. Std. No. 185 except that the ASTM

SUMMARY OF CHANGES

Committee B02 has identified the location of selected changes to this standard since the last issue (B564 - 10)
that may impact the use of this standard. (Approved October 1, 2011.)

(1) Revised 1.1 to tabularize alloys. (3) Added new footnote A to Table 1 and revised Table 1 to
(2) Added a new material N06674 to 1.1, 1.1.2, 5.2.9.3, and address a new alloy with a columbium (Nb) range, rather than
Tables 1 and Table 2. just a max.

Committee B02 has identified the location of selected changes to this standard since the last issue (B564 - 06a)
that may impact the use of this standard. (Approved October 1, 2010.)

(1) Added a new material N10362 to Table 1 and Table 2.

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B564 – 11
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Designation: B564 – 11
Standard Specification for
Nickel Alloy Forgings1
This standard is issued under the fixed designation B5
Cobalt, and High-Temperature Alloys
2.2
Military Standards:5
MIL-STD-129 Marking for Shipment and Storage
MIL-STD-271 Nondest
TABLE 1 Chemical RequirementsA
Composition, %
Element
Nickel
Alloy
Nickel-
Copper
Alloy
Low-
Carbon
Nickel-
Molybdenum-
Chrom
TABLE 1 Chemical RequirementsA (continued)
Composition, %
Element
Low-
Carbon
Nickel-
Chromium-
Molybdenum-
Copper
Alloy
Low-
TABLE 1 Chemical RequirementsA (continued)
Composition, %
Element
Low-
Carbon
Nickel-
Chromium-
Molybdenum-
Tungsten
Alloy
Ni
TABLE 1 Chemical RequirementsA (continued)
Composition, %
Element
Nickel-
Molybdenum-
Chromium-
Iron
Alloy
Low-
Carbon
Nickel
TABLE 2 Mechanical Property RequirementsA
Material and Condition
Maximum Section
Thickness,
in. (mm)
Tensile Strength,
min, k
13. Rejection and Rehearing
13.1 Material, tested by the purchaser, that fails to conform
to the requirements of this specific
S5. Nondestructive Tests
S5.1 When specified by the purchaser, each piece of each lot
shall be inspected. The purchaser shall
S6. Quality Assurance
S6.1 Responsibility for Inspection:
S6.1.1 Unless otherwise specified in the contract or purchase
order,

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