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b65 4360 (Rev. C 2002.11) en - Adhesive or Non Adhesive Cellular Materials For Sealing, Packing and Acoustic Insulation

This document provides standards for adhesive and non-adhesive cellular materials used for sealing, packing, and acoustic insulation in vehicles. It defines symbols to designate material characteristics, including type of material, density, vehicle zone, structure, compressibility, combustion, water absorption, adhesiveness, and acoustics. The document establishes requirements for these materials and provides examples of how to express material specifications on documents.

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Diego Camargo
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0% found this document useful (0 votes)
730 views20 pages

b65 4360 (Rev. C 2002.11) en - Adhesive or Non Adhesive Cellular Materials For Sealing, Packing and Acoustic Insulation

This document provides standards for adhesive and non-adhesive cellular materials used for sealing, packing, and acoustic insulation in vehicles. It defines symbols to designate material characteristics, including type of material, density, vehicle zone, structure, compressibility, combustion, water absorption, adhesiveness, and acoustics. The document establishes requirements for these materials and provides examples of how to express material specifications on documents.

Uploaded by

Diego Camargo
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd
You are on page 1/ 20

PSA PEUGEOT – CITROËN

B65 4360
NORMES VEHICULES

ADHESIVE or NON ADHESIVE CELLULAR MATERIALS


FOR SEALING,
PACKING AND ACOUSTIC INSULATION

Page 1/20
NO USE RESTRICTION

This is a translation, the French original shall be used in all cases of litigation Date of translation : 28/04/2004

CONTENTS

1. OBJECT AND FIELD OF APPLICATION 2


2. SYMBOLS 2
3. EXAMPLE OF MATERIAL DESIGNATION 3
4. EXPRESSION ON DOCUMENTS 3
5. GENERAL REQUIREMENTS 3
6. TECHNICAL CHARACTERISTICS 3
6.1. TYPE OF MATERIAL 3
6.2. DENSITY 4
6.3. VEHICLE ZONE 4
6.4. MATERIAL STRUCTURE 4
6.5. COMPRESSIBILITY 5
6.6. COMPRESSION RATE 5
6.7. COMBUSTIBILITY 6
6.8. COLOUR FASTNESS 6
6.9. WATER ABSORPTION 6
6.10. ADHESIVE CHARACTERISTICS 6
6.11. MEASUREMENT OF THE ACOUSTIC ABSORPTION COEFFICIENT IN TERMS OF
FREQUENCY 10
7. CONDITIONS FOR IMPLEMENTATION (PROCESS) 11
APPENDIX 1 – ABSORPTION – MEASUREMENT WITH IMPEDANCE TUBE 12
APPENDIX 2 – NUMERICAL REFERENCES 13
APPENDIX 3 – SPA SAMPLE 16
8. RECORDS AND REFERENCE DOCUMENTS 19
8.1. RECORDS 19
8.2. REFERENCE DOCUMENTS 19
8.3. EQUIVALENT TO : 20
8.4. CONFORMS TO : 20
8.5. KEY-WORDS 20

OR : 01/12/1995 C: 20/11/2002 General use


PSA PEUGEOT - CITROËN

ADHESIVE or NON ADHESIVE CELLULAR MATERIALS- INSULATION B65 4360 2/20

1. OBJECT AND FIELD OF APPLICATION


The object of this standard is to :
• define the symbols to be used for the characteristics of parts in cellular materials.
• specify the characteristics of categories and classes defined hereafter.
It applies to self-adhesive or non adhesive “spongy” or “honey-combed” cellular materials.
Furthermore, it applies to sheets, strips, moulded or cut out parts, etc., used to provide sealing (to water, air, dust) or
packing, or for acoustic insulation (anti-vibratory, anti-squeaking,…).
For the majority of parts in self adhesive cellular material, it defines the details to be carried on the drawing in order to
obtain the properties for use. Certain parts may be the subject of a specific document which will define the additional
required properties according to norme B20 0150 which cannot be expressed by the designations of this norme.
It must include the following standards B14 0100, B20 0110, B62 0020 and B74 0100 giving the general
requirements for consultation by Suppliers.

2. SYMBOLS
The symbol for the designation of the material consists of a group of figures and letters in the following order :

1 2 3 4 5 6 7 8 9 10 11

1 Symbol for the type of material : 4 letters (according to § 6.1.).


2 Symbol for density : 2 figures (according to § 6.2.).
3 Symbol for the vehicle zone : this symbol consists of one capital letter followed by a
number. The letter refers to the specific characteristic,
the number refers to the degree to which the material
possesses this characteristics (according to § 6.3.).
4 Symbol for the material structure : this symbol consists of a capital letter followed by a
number. The letter refers to the class of material, the
number refers to the method used to manufacture the
part (according to § 6.4.).
5 Symbol for compressibility : 2 figures (according to § 6.5.).
6 Symbol for the compression rate : 1 figure (according to § 6.6.).
7 Symbol for combustibility : 1 figure (according to § 6.7.).
8 Symbol for colour fastness : 1 figure (according to § 6.8.).
9 Symbol for water absorption : 1 figure (according to § 6.9.).
10 Symbol for adhesive characteristics : 1 figure (according to § 6.10.).
11 Symbol for acoustics : 1 figure (according to § 6.11.).

Certain characteristics for specific use are not allocated a specific symbol. They carry the letter ”Z” placed at
the end of the complete designation. This letter cross refers to a “Note Z” on the drawing.

OR : 01/12/1995 C : 20/11/1002 General use


PSA PEUGEOT - CITROËN

ADHESIVE or NON ADHESIVE CELLULAR MATERIALS- INSULATION B65 4360 3/20

3. EXAMPLE OF MATERIAL DESIGNATION


A material with the following characteristics is designated as follows :

1 Type of material : polyurethane


3
2 Density : 25 kg/m
3 Vehicle zone : body interior 85°C
4 Material structure : spongy cut out
5 Compressibility : 10 daN/dm² to 20 daN/dm²
6 Compression rate : 10%
7 Combustibility : ≤ 100 mm/min
8 Colour fastness : 240 h
9 Water absorption : ≤ 10%
10 Adhesive characteristics : passenger compartment interior : normal strength
11 Acoustic characteristics : applicable

Self-adhesive
cellular material P U R 0 2 I2 S2 0 1 1 1 2 1 4 1 Norme B65 4360

4. EXPRESSION ON DOCUMENTS
Indicate that this concerns a self-adhesive cellular material to be followed by the complete designation of the
material and the reference number of this norme.
If the complete designation includes letter “Z”, do not omit the note specifying the type of test, the reference
number of the test method and the requirement.
Furthermore, state, if applicable, the reference numbers of the required specific documents.

5. GENERAL REQUIREMENTS
These requirements are those of normes B14 0100, B20 0110 and B74 0100. Deliveries, in particular, must conform
to the drawings and technical specifications and for characteristics not specified in these documents, to samples
which have been approved.
The supplied self-adhesive cellular materials must be free from any defect, visible or not, which may be detrimental
to the function or appearance. No technical modification even minor must not be made by the supplier without the
agreement of the relevant company of the Group.

6. REQUIRED CHARACTERISTICS
The requirements are specified in the following tables according to the symbol set on the drawing for each of
the characteristics taken into account.

6.1. TYPE OF MATERIAL

Designation Symbols
Polyurethane foam (polyether or polyester) PUR (PEUR or PAUR)
Impregnated polyurethane foam PURI
Polyvinyl chloride foam PVC
Polyethylene foam PE
Polypropylene foam PP
Ethylene propylene diene terpolymer foam EPDM
Chloroprene foam CR
Natural rubber foam NR
Silicone foam SI

Note : In the case of specific requirements for this characteristic, these are indicated in the designation by
the letters “XX” with a corresponding detailed note on the drawing.

OR : 01/12/1995 C : 20/11/1002 General use


PSA PEUGEOT - CITROËN

ADHESIVE or NON ADHESIVE CELLULAR MATERIALS- INSULATION B65 4360 4/20

6.2 DENSITY (VOLUME MASS)

Density (MV)
Documents 3 Symbols
(kg/m )
D45 1045 10 ≤ MV < 20 01
D45 1045 20 ≤ MV < 30 02
D45 1045 30 ≤ MV < 40 03
D45 1045 40 ≤ MV < 60 04
D45 1045 60 ≤ MV < 80 06
D45 1045 80 ≤ MV < 100 08
D45 1045 100 ≤ MV < 140 10
D45 1045 MV ≥140 14

Note : In the case of specific requirements for this characteristic, these are indicated in the designation by
the letters “XX” with a corresponding detailed note on the drawing.

6.3 VEHICLE ZONE

Vehicle zone Operating temperature Symbols


Min. Max.
- 30°C 60°C I1
Body interior - 30°C 85°C I2
- 30°C 100°C I3
- 30°C 60°C E1
Body exterior - 30°C 85°C E2
- 30°C 100°C E3
- 30°C 60°C M1
Engine compartment (*) - 30°C 85°C M2
- 30°C 120°C M3

Note : In the case of specific requirements for this characteristic, these are indicated in the designation by
the letter “X” followed by the suffix “Y”, with a corresponding detailed note on the drawing.
(*) Including the plenum collector.

6.4. MATERIAL STRUCTURE

Class Method used Symbols


Moulded in situ C1
Cellular Cut out (continuous block) C2
Cut out and moulded C3
Moulded in situ S1
Spongy Cut out (continuous block) S2
Cut out and moulded S3

Note : In the case of specific requirements for this characteristic, these are indicated in the designation by
the letter “X” followed by the suffix “Y”, with a corresponding detailed note on the drawing.

The water absorption rate under vacuum shall be tested in accordance with test method D45 1520.
A material showing an open cell percentage ≤ 50, determination in accordance with test method D45 1355
with a water absorption rate ≤ 26% shall be considered to be CELLULAR otherwise it shall be considered to
be SPONGY.

OR : 01/12/1995 C : 20/11/1002 General use


PSA PEUGEOT - CITROËN

ADHESIVE or NON ADHESIVE CELLULAR MATERIALS- INSULATION B65 4360 5/20

6.5. COMPRESSIBILITY
Compressibility = compression strength
The compressibility (Pn) shall be measured to 50% according to test method D41 1541 :
• at the 1st compression cycle for cellular materials,
• at the 5th compression cycle for spongy materials.

Compressibility
Documents Symbols
(daN/dm²)
D41 1541 1 ≤ Pn < 10 00
D41 1541 10 ≤ Pn < 20 01
D41 1541 20 ≤ Pn < 40 02
D41 1541 40 ≤ Pn < 80 04
D41 1541 80 ≤ Pn < 160 08
D41 1541 160 ≤ Pn < 300 16
D41 1541 300 ≤ Pn < 1000 30

Note : When the part does not allow the compressibility Pn to be defined, the two figures for the
compressibility index number are replaced by “XX” and the requirement replacing it (test and result)
must be shown on the drawing or in the documents.
Materials from different categories comply also with limit characteristics such as residual deformation
(DR), tear strength (Rd), compressibility variation, etc.
These characteristics are shown in specific documents according to Appendix 3.

6.6. COMPRESSION RATE

This symbol shows the maximum compression rate of the part in its use on the vehicle. It must in terms of the
compressibility in relation to the surface of the compressed part.

Deformation (D) in % Symbols


0 ≤ D < 10 0
10 ≤ D < 20 1
20 ≤ D < 30 2
30 ≤ D < 40 3
40 ≤ D < 50 4
50 ≤ D < 60 5
60 ≤ D < 70 6
70 ≤ D < 80 7
80 ≤ D < 90 8
90 ≤ D < 99 9

Remark : If a part is not compressed uniformly, the maximum compression rate shall be retained for the
choice of symbol.

OR : 01/12/1995 C : 20/11/1002 General use


PSA PEUGEOT - CITROËN

ADHESIVE or NON ADHESIVE CELLULAR MATERIALS- INSULATION B65 4360 6/20

6.7. COMBUSTIBILITY

Symbols and requirements


Documents Characteristics Expression
of results 0 1
D45 1333 Combustibility mm/min - ≤ 100

Note : In the case of specific requirements for these characteristics, these are indicated in the designation by
the letter “X” with a corresponding detailed note on the drawing.
A dash (-) means that there is no requirement.

6.8 COLOUR FASTNESS

Symbols and
Documents Characteristics Expression
requirements
of results 0 1 2 3
Colour fastness using the equipment CI 3000
D47 1431 (interior parts)
• After 200 hours
(if exposure behind tinted glass and/or Index - ≥4 - -
reflecting glass)
• After 240 hours Index - - ≥4 -
(if exposure behind clear glass)
Colour fastness to WEATHER OMETER
D27 1389
(exterior parts) No. 2 range – 3 cycles
Index - - - ≥4

Note : In the case of specific requirements for these characteristics, these are indicated in the designation by
the letter “X” with a corresponding detailed note on the drawing.
A dash (-) means that there is no requirement.

6.9. WATER ABSORPTION

Symbols and requirements


Documents Characteristics Expression
of results 0 1 2 3
D45 1429 Water absorption % - ≤ 10 ≤ 50 > 50

Note : In the case of specific requirements for these characteristics, these are indicated in the designation by
the letter “X” with a corresponding detailed note on the drawing.
A dash (-) means that there is no requirement.

6.10. ADHESIVE CHARACTERISTICS


ADHESIVE SYMBOLS AND CHARACTERISTICS
0 - No requirement : -
1 - Passenger compartment interior : wiring harness protections
2 - Engine compartment : wiring harness protections
3 - All vehicle zones : provisional strength
4 - Passenger compartment interior : normal strength
5 - Passenger compartment exterior : normal strength
6 - Engine compartment : normal strength
7 - Passenger compartment interior : reinforced strength
8 - Passenger compartment exterior : reinforced strength
9 - Engine compartment : reinforced strength

OR : 01/12/1995 C : 20/11/1002 General use


PSA PEUGEOT - CITROËN

ADHESIVE or NON ADHESIVE CELLULAR MATERIALS- INSULATION B65 4360 7/20

6.10. ADHESIVE CHARACTERISTICS (continued)

Documents Characteristics Expression Symbols and requirements


of results 0 1 2

NF EN 12035 FLAG TEST


• At 23°C ± 2°C, after 24 hours at 23°C ± 2°C Note - (6) (6)
D47 1309 • After 10 AF cycles Note - (6) (6)
• After exposure to fluids (10) Note - - (6)

D11 1157 RESISTANCE TO PEELING OF THE PROTECTIVE


FILM AT A FLAT ANGLE
• In the new condition N/cm - ≤ 0,15 ≤ 0,15
D47 1309 • After 1 AF cycle - (7) (7)

DIMENSIONAL VARIATIONS (8)


D45 1234
• After 24 hours at the max. operating temperature mm - ≤1 ≤1

ADHESION TO CLEAN GLASS (9)


Resistance to peeling at right angle
• Before ageing
D51 1485 • After 10 minutes at 23°C ± 2°C N/cm - - -
• After 24 hours at 23°C ± 2°C N/cm - - -
• After ageing
• After 1 AF cycle N/cm - - -
• After 5 AF cycles N/cm - - -
D47 1309 • After 10 AF cycles, loss between 5 and 10 cycles % - - -
• After exposure to fluids at 23°C ± 2°C (10) N/cm - - -
D47 1165 • After 3 days in humid cataplasm (H -3) N/cm - - -
Tensile strength - shearing
• Before ageing
D41 1108 • After 10 minutes at 23°C ± 2°c MPa - - -
• After 24 hours at 23°C ± 2°C MPa - - -
• After ageing
• After 1 AF cycle MPa - - -
• After 5 AF cycles MPa - - -
D47 1309 • After 10 AF cycles, loss between 5 and 10 cycles % - - -
• After exposure to fluids at 23°C ± 2°C (10) MPa - - -
D47 1165 • After 3 days in humid cataplasm (H -3) MPa - - -

Note : A dash (-) means that there is no requirement.


(a) If there is a specific shear stress of the part, the values shall be defined on the drawing of the part,
according to the geometry of the support,…
Numerical references ( )are detailed in Appendix 2.

OR : 01/12/1995 C : 20/11/1002 General use


PSA PEUGEOT - CITROËN

ADHESIVE or NON ADHESIVE CELLULAR MATERIALS- INSULATION B65 4360 8/20

6.10. ADHESIVE CHARACTERISTICS (continued)

Documents Characteristics Expression Symbols and requirements


of results 3 4 5 6

NF EN 12035 FLAG TEST


• At 23°C ± 2°C, after 24 hours at 23°C ± 2°C Note - - - -
D47 1309 • After 10 AF cycles Note - - - -
• After exposure to fluids (10) Note - - - -

RESISTANCE TO PEELING OF THE PROTECTIVE


D11 1157 FILM AT A FLAT ANGLE
• In the new condition N/cm ≤ 0,15 ≤ 0,15 ≤ 0,15 ≤ 0,15
D47 1309 • After 1 AF cycle (7) (7) (7) (7)

DIMENSIONAL VARIATIONS (8)


D45 1234
• After 24 hours at the max. operating temperature mm ≤1 ≤1 ≥1 ≤1

ADHESION TO CLEAN GLASS (9)


Resistance to peeling at right angle
• Before ageing
D51 1485 • After 10 minutes at 23°C ± 2°C N/cm ≥ 1,5 ≥ 1,5 ≥4 ≥4
• After 24 hours at 23°C ± 2°C N/cm ≥2 ≥2 ≥5 ≥5
• After ageing
• After 1 AF cycle N/cm - ≥2 ≥5 ≥5
• After 5 AF cycles N/cm - ≥ 2,8 ≥5 ≥5
D47 1309 • After 10 AF cycles, loss between 5 and 10 cycles % - ≤ 10 ≤ 10 ≤ 10
• After exposure to fluids at 23°C ± 2°C (10) N/cm - - - ≥4
D47 1165 • After 3 days in humid cataplasm (H -3) N/cm - - - -
Tensile strength - shearing
• Before ageing
D41 1108 • After 10 minutes at 23°C ± 2°c MPa
• After 24 hours at 23°C ± 2°C MPa
• After ageing (a) (a) (a) (a)
• After 1 AF cycle MPa
• After 5 AF cycles MPa
D47 1309 • After 10 AF cycles, loss between 5 and 10 cycles %
• After exposure to fluids at 23°C ± 2°C (10) MPa
D47 1165 • After 3 days in humid cataplasm (H -3) MPa

Note : A dash (-) means that there is no requirement.


(a) If there is a specific shear stress of the part, the values shall be defined on the drawing of the part,
according to the geometry of the support,....
Numerical references ( )are detailed in Appendix 2.

OR : 01/12/1995 C : 20/11/1002 General use


PSA PEUGEOT - CITROËN

ADHESIVE or NON ADHESIVE CELLULAR MATERIALS- INSULATION B65 4360 9/20

6.10. ADHESIVE CHARACTERISTICS (continued)

Documents Characteristics Expression Symbols and requirements


of results 7 8 9

NF EN 12035 FLAG TEST


• At 23°C ± 2°C, after 24 hours at 23°C ± 2°C Note - - -
D47 1309 • After 10 AF cycles Note - - -
• After exposure to fluids (10) Note - - -

RESISTANCE TO PEELING OF THE PROTECTIVE


D11 1157 FILM AT A FLAT ANGLE
• In the new condition N/cm ≤ 0,15 ≤ 0,15 ≤ 0,15
D47 1309 • After 1 AF cycle (7) (7) (7)

DIMENSIONAL VARIATIONS (8)


D45 1234
• After 24 hours at the max. operating temperature mm ≤1 ≥1 ≤1

ADHESION TO CLEAN GLASS (9)


Resistance to peeling at right angle
• Before ageing
D51 1485
• After 10 minutes at 23°C ± 2°C N/cm ≥ 1,5 ≥4 ≥4
• After 24 hours at 23°C ± 2°C N/cm ≥2 ≥5 ≥5
• After ageing
• After 1 BF cycle N/cm ≥2 ≥5 ≥5
D47 1309 • After 5 BF cycles N/cm ≥ 2,8 ≥5 ≥5
• After 10 BF cycles, loss between 5 and 10 cycles % ≤ 10 ≤ 10 ≤ 10
• After exposure to fluids at 23°C ± 2°C (10) N/cm - - ≥4
D47 1165 • After 3 days in humid cataplasm (H -3) N/cm - - ≥4
Tensile strength - shearing
• Before ageing
D41 1108
• After 10 minutes at 23°C ± 2°C MPa
• After 24 hours at 23°C ± 2°C MPa
• After ageing
• After 1 BF cycle MPa
(a) (a) (a)
• After 5 BF cycles MPa
D47 1309
• After 10 BF cycles, loss between 5 and 10 cycles %
• After exposure to fluids at 23°C ± 2°C (10) MPa
D47 1165 • After 3 days in humid cataplasm (H3) MPa

Note : A dash (-) means that there is no requirement.


(a) If there is a specific shear stress of the part, the values shall be defined on the drawing of the part,
according to the geometry of the support,…
Numerical references ( )are detailed in Appendix 2.

OR : 01/12/1995 C : 20/11/1002 General use


PSA PEUGEOT - CITROËN

ADHESIVE or NON ADHESIVE CELLULAR MATERIALS- INSULATION B65 4360 10/20

6.11. MEASUREMENT OF THE ACOUSTIC ABSORPTION COEFFICIENT IN RELATION TO FREQUENCY

The acoustic absorption coefficient is measured with the test specimen at the bottom of the tube, from 100 Hz to
6300 Hz.
The various acoustic efficiency classes are defined in Appendix 1.
The corresponding values are specified in the table of Appendix 1.
The curve analysis field ranges between 250 Hz and 6300 Hz.
3 points outside the class are tolerated (over the 15 points measured).
No point showing a variation of more than 5% lower than the referenced value of the class must be accepted.
In this case, the lower class must be considered as being the class for the absorbent.
Each measurement curve must be shown with values.

Documents Acoustic absorption coefficient Symbols


- - 0
D45 5014 Class 1 1
D45 5014 Class 2 2
D45 5014 Class 3 3
D45 5014 Class 4 4
D45 5014 - XX

Note : If different results are obtained from the same sample between the two measuring equipment Kundt
tube according to test method D45 5014 and Impedance tube according to test method D45 5430,
only the results from the Impedance tube shall be used.
According to the function and efficiency required from the sound proofing material, an acoustic class
shall or shall not be specified (from 1 to 4). A dash (-) means that there is no requirement.
In the case of specific requirements for these characteristics, these are indicated in the designation by
the letter “X” with a corresponding detailed note on the drawing.

OR : 01/12/1995 C : 20/11/1002 General use


PSA PEUGEOT - CITROËN

ADHESIVE or NON ADHESIVE CELLULAR MATERIALS- INSULATION B65 4360 11/20

7. CONDITIONS FOR IMPLEMENTATION (PROCESS)

Characteristics Expression of Self-adhesive cellular


results materials
IN MANUFACTURE
Receiver substrates
• Type Type (1)
• Preparation before bonding (2)
Carrier substrates
• Type Type (5)
• Temperature °C ≥ 18
• Storage (3)
• Method of application

IN LABORATORY
Receiver supports
• Type Type (*)
• Preliminary cleaning (**)
• Temperature °C 23 ± 2
Alignment
• Pressure MPa 0,02
• Duration of application s 10
Conditioning of test specimens
• Temperature °C 23 ± 2
• Relative humidity % 50 ± 5
• Duration h 24

Note : (*) Toughened glass plate, 3 to 4 mm thick.


(**) Cleaning products, if required, according to whether or not the surface is greasy or polluted.
Numerical references ( )are detailed in Appendix 2
Use an approved solvent selected from the following list :
• Cyclohexane,
• Ethyl acetate,
• Methyl ethyl ketone,
• Propan – 2 – ol,
• Denatured alcohol.

OR : 01/12/1995 C : 20/11/1002 General use


PSA PEUGEOT - CITROËN

ADHESIVE or NON ADHESIVE CELLULAR MATERIALS- INSULATION B65 4360 12/20

Appendix 1

ABSORPTION
MEASUREMENT WITH IMPEDANCE TUBE

ACCORDING TO TEST METHOD D45 5430

Frequencies (Hz) Class 1 Class 2 Class 3 Class 4


100 0,5 0,5 0,5 0,5
125 0,7 0,7 0,7 0,7
160 1,2 1,2 1,2 1,2
200 1,2 1,2 2 2,5
250 2 2 2,5 3
315 2,3 2,4 3,5 4,5
400 2,8 3 6 7,3
500 3,8 5 8,3 11,3
630 4,5 7,1 11,7 16,7
800 5,6 10 16,4 23,5
1000 7,3 13,3 21,2 31,7
1250 9,0 18,5 29 40,7
1600 12,0 24,8 39,2 53,7
2000 16,5 34 51,2 67,3
2500 22,8 45 65,1 80
3150 31,5 60,8 77,8 89
4000 42 72,5 86,4 93,8
5000 56 80,2 90,7 96,3
6300 66,4 84 92,3 97

OR : 01/12/1995 C : 20/11/1002 General use


PSA PEUGEOT - CITROËN

ADHESIVE or NON ADHESIVE CELLULAR MATERIALS- INSULATION B65 4360 13/20

Appendix 2 (1/3)
NUMERICAL CROSS REFERENCES

(1) All types of production substrates.

(2) The receiver substrate must be suitable for bonding, which means :
• clean
• unpolluted
• without condensation.
To achieve this, the work station for the carrier substrate must also be clean (free from dust, grease,
anti-adhesive product…).
Under no circumstances should the temperature of the receiver substrate be lower than that of the
workshop (condensation created by introducing a cold part into a warmer location is totally
incompatible with proper bonding). If it is lower than 15°C, the receiver substrate should be heated up.
In the case of a contaminated surface (dust, traces of grease…), cleaning with a lint free absorbent
paper soaked in alcohol (denatured alcohol or isopropanol) shall be necessary before bonding.

(3) • Parts bonded in Production Centres : Parts shall be transported and stored away from humidity
and external pollution. No detachment of the protective film or damage to parts are tolerated during
transport and storage.
The storage temperature shall be between – 10°C and 50°C; the exposure of parts to any significant
heat sources is to be avoided.
The protective film must be removed from the part without damage or tear, or loss of adhesive
property even after 6 months storage in the conditions stated above.

• Parts delivered to Production Centres already fitted or bonded : No damage or tear, or


detachment are tolerated during transport and storage within a temperature range of – 20°C to 50°C
before fitting to body.

(4) The fitting of these parts shall be carried out manually. The temperature of the receiver substrate,
during bonding, shall be between 15°C and 40°C. A slight warm up at 35°C, 40°C shall reactivate the
glue and improve the adhesion immediately (in particular for parts which are not bonded on flat
substrates).
The protective film must not be removed beforehand. Any part retrieved from storage with a section of
the protective film removed, shall be scrapped.

All contact of the adhesive with a contaminated surface is to be avoided at all cost, in particular with
hands.

Pressure must mandatorily be applied to each part to guarantee proper bonding.

The pressure application may be carried out :


• with a rubber roller,
• by smoothing out manually,
• by inflatable bag, etc.

During application of pressure, care must be taken as not to damage or tear the part.

Note : For parts bonded onto several faces, care must be taken as not to elongate the part during
application or bond it under stress.

The part must be correctly positioned before applying the pressure so as to avoid any removing/re-
bonding which would damage the adhesive.

OR : 01/12/1995 C : 20/11/1002 General use


PSA PEUGEOT - CITROËN

ADHESIVE or NON ADHESIVE CELLULAR MATERIALS- INSULATION B65 4360 14/20

Appendix 2 (2/3)
NUMERICAL CROSS REFERENCES (continued)

(5) Self-adhesive cellular materials with a protective film with one anti-adhesive face minimum.

(6) Without detachment or separation of the adhesive/cellular material.

(7) After ageing, a maximum variation of plus or minus 20% is tolerated. During these tests, no tear of the
protective film or damage to the adhesive is tolerated.

Note : No detachment of the protective film during transport, storage and handling of parts is tolerated.

(8) Dimensional variation


Check the dimensional variations on a test specimen consisting of a toughened glass plate and the
part bonded together according to the diagram below :

Reference marks (length)


Glass plate

Reference marks (width) Inspected element

Trace symmetrical reference marks along the length L and the width L’ according to the above
diagram by means of a paring knife.
24 hours after bonding, subject the test specimen to the conditions shown in this norme (the maximum
operating temperature is specified in the § 6.2., according to the material designation).
After the test, condition the test specimen for 1 hour at 23°C ± 2°C and 50% ± 5% relative humidity.
Measure the dimensional variations by means of a suitable device capable of measuring 1/20 mm.
Express the results in mm (absolute values over L and L’).

(9) To check the adhesion, the peeling at right angle test shall be carried out in accordance with
test method D51 1485 or a tensile shear test in accordance with MES D41 1108 according to the
thickness, density and hardness of the material. However, the peeling at right angle test is preferred.

OR : 01/12/1995 C : 20/11/1002 General use


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Appendix 2 (3/3)
NUMERICAL CROSS REFERENCES (continued)

(10) Definition of fluids and test conditions : select the fluids according to the stresses encountered on the
vehicles.

Method of
Designation Composition Drying time
exposure
Alcohol Denatured Ethanol Immersion 1 min 24 hours
Cleaning product Sodium lauryl sulphate diluted to Immersion 24 hours 24 hours
10 g/l in softened water
Temporary protection Conforming to 24 hours
D47 1279
product (*) norme B14 6855
Protection removal Conforming to Min. 2 hours
D47 1279
product (*) norme B74 6210 Max. 4 hours
50% 2-2-4 Trimethyl-pentane Immersion
AFNOR C 24 hours
50% Toluene 1 min
85% AFNOR C Immersion
CARBUROL 24 hours
15% Methanol 1 min
Conforming to STL 24 h at 23°C ± 2°C
Grease (**) 24 hours
S71 3106 then 10 cycles
D47 1309 AF

(*) According to the conditions shown in the production application range.


Temporary protection product : product generally applied to all new stored or transported vehicles .
Protection removal product : product used to eliminate the temporary protection product.

(**) Grease : Deposit a layer 2 mm thick by means of a template.


After exposure, no separation between the cellular material and adhesive and no detachment between
the adhesive and its substrate shall be noticed.

OR : 01/12/1995 C : 20/11/1002 General use


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Appendix 3 (1/3)

SPA SAMPLE

OR : 01/12/1995 C : 20/11/1002 General use


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Appendix 3 (2/3)

OR : 01/12/1995 C : 20/11/1002 General use


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Appendix 3 (3/3)

OR : 01/12/1995 C : 20/11/1002 General use


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8. RECORDS AND REFERENCE DOCUMENTS

8.1. RECORDS

8.1.1. CREATION
• OR : 01/12/1995 – CREATION OF THE NORME.

8.1.2. SUBJECT OF THE MODIFICATION


• C : 20/11/2002 – ACOUSTIC REQUIREMENTS INTEGRATED in § 6.11. and CURVES IN
Appendix 1
• B : 10/11/1999 – MODIFICATION TO THE TITLE AND CORRECTIONS MADE TO 6.5, 6.7, 6.8
and 6.10.

8.2 REFERENCE DOCUMENTS

8.2.1. PSA DOCUMENTS


8.2.1.1 Normes
B14 0100 FUNCTIONS OF BONDING, SEALING, ANTI-CHIPPING, DAMPING, ANTI-CORROSION AND
PROTECTION – GENERAL
B14 6855 TEMPORARY PROTECTION FUNCTIONS ON FINISHING PAINT IN EXTERIOR
SURROUNDINGS TO WEATHERING USING A WASHABLE DISPOSABLE FILM
B20 0150 PRODUCTS WHICH ARE THE SUBJECT OF A PRODUCT APPROVAL SPECIFICATION –
GENERAL REQUIREMENTS
B20 0110 SUPPLIES OF PRODUCTS OR ASSEMBLIES – GENERAL REQUIREMENTS
B62 0020 THERMOPLASTIC AND THERMOSETTING MATERIALS – CONVENTIONAL DESIGNATIONS
B74 0100 PRODUCT SUPPLIES – BONDING, SEALING, ANTI-CHIPPING, DAMPING, ANTI-
CORROSION, PROTECTION – GENERAL REQUIREMENTS
B74 6210 PROTECTION REMOVAL PRODUCTS USED COLD FOR VEHICLE EXTERIORS
D11 1157 ADHESIVES AND TRIM MATERIALS – PEELING AT A FLAT ANGLE
D27 1389 PAINT COATINGS – RUBBERS AND PLASTICS – ARTIFICIAL AGEING BY WEATHER-
OMETER
D41 1108 ADHESIVES – TENSILE-SHEAR STRENGTH (SHIM METHOD)
D41 1541 FLEXIBLE AND SEMI-FLEXIBLE CELLULAR MATERIALS – COMPRESSION STRENGTH
D45 1045 CELLULAR MATERIALS – APPARENT DENSITY
D45 1234 PARTS CONTAINING PLASTIC ELEMENTS – REACTION TO HEAT IN A NON RADIANT DRY
OVEN
D45 1333 MATERIALS INTERIOR TO PASSENGER COMPARTMENT – HORIZONTAL
COMBUSTIBILITY
D45 1355 CELLULAR PLASTICS AND RUBBERS – COMMUNICATING CELLS – VOLUME
PERCENTAGE
D45 1429 CELLULAR MATERIALS – WATER ABSORPTION
D45 1520 CELLULAR MATERIALS – WATER ABSORPTION UNDER VACUUM
D45 5014 POLYURETHANE FOAM, PADDING, FELT – ACOUSTIC ABSORPTION COEFFICIENT
(STANDING WAVE METHOD)
D45 5430 POLYURETHANE FOAM, PADDING, FELT – ACOUSTIC ABSORPTION COEFFICIENT –
IMPEDANCE TUBE MEASUREMENT
D47 1165 PRODUCTS APPLIED TO BODY IN WHITE OR PAINT COATED OR PLASTICS –
ACCELERATED AGEING
D47 1279 PLASTIC COMPONENTS – BEHAVIOUR IN CONTACT WITH PROTECTION AND
PROTECTION REMOVAL PRODUCTS
D47 1309 AUTOMOTIVE MATERIALS AND EQUIPMENT – AGEING ACCORDING TO A GIVEN
CLIMATIC CYCLE
D47 1431 MATERIALS AND PARTS FOR PASSENGER COMPARTMENT – COLOUR FASTNESS TO
ARTIFICIAL LIGHT AT HIGH AND MEAN TEMPERATURES
D51 1485 ADHESIVES – PEELING AT A RIGHT ANGLE
S71 3106 GREASE FOR BODY ACCESSORIES – GLASS LIFTS, HINGES, DOOR CHECKS

OR : 01/12/1995 C : 20/11/1002 General use


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8.2.1.2 Others

8.2.2. EXTERNAL DOCUMENTS


NF EN 12035 SELF-ADHESIVES TAPES – FLAG TEST OF ADHESIVE TAPES

8.3. EQUIVALENT TO :

8.4. CONFORMS TO :

8.5. KEY-WORDS

OR : 01/12/1995 C : 20/11/1002 General use

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