b65 4360 (Rev. C 2002.11) en - Adhesive or Non Adhesive Cellular Materials For Sealing, Packing and Acoustic Insulation
b65 4360 (Rev. C 2002.11) en - Adhesive or Non Adhesive Cellular Materials For Sealing, Packing and Acoustic Insulation
B65 4360
NORMES VEHICULES
Page 1/20
NO USE RESTRICTION
This is a translation, the French original shall be used in all cases of litigation Date of translation : 28/04/2004
CONTENTS
2. SYMBOLS
The symbol for the designation of the material consists of a group of figures and letters in the following order :
1 2 3 4 5 6 7 8 9 10 11
Certain characteristics for specific use are not allocated a specific symbol. They carry the letter ”Z” placed at
the end of the complete designation. This letter cross refers to a “Note Z” on the drawing.
Self-adhesive
cellular material P U R 0 2 I2 S2 0 1 1 1 2 1 4 1 Norme B65 4360
4. EXPRESSION ON DOCUMENTS
Indicate that this concerns a self-adhesive cellular material to be followed by the complete designation of the
material and the reference number of this norme.
If the complete designation includes letter “Z”, do not omit the note specifying the type of test, the reference
number of the test method and the requirement.
Furthermore, state, if applicable, the reference numbers of the required specific documents.
5. GENERAL REQUIREMENTS
These requirements are those of normes B14 0100, B20 0110 and B74 0100. Deliveries, in particular, must conform
to the drawings and technical specifications and for characteristics not specified in these documents, to samples
which have been approved.
The supplied self-adhesive cellular materials must be free from any defect, visible or not, which may be detrimental
to the function or appearance. No technical modification even minor must not be made by the supplier without the
agreement of the relevant company of the Group.
6. REQUIRED CHARACTERISTICS
The requirements are specified in the following tables according to the symbol set on the drawing for each of
the characteristics taken into account.
Designation Symbols
Polyurethane foam (polyether or polyester) PUR (PEUR or PAUR)
Impregnated polyurethane foam PURI
Polyvinyl chloride foam PVC
Polyethylene foam PE
Polypropylene foam PP
Ethylene propylene diene terpolymer foam EPDM
Chloroprene foam CR
Natural rubber foam NR
Silicone foam SI
Note : In the case of specific requirements for this characteristic, these are indicated in the designation by
the letters “XX” with a corresponding detailed note on the drawing.
Density (MV)
Documents 3 Symbols
(kg/m )
D45 1045 10 ≤ MV < 20 01
D45 1045 20 ≤ MV < 30 02
D45 1045 30 ≤ MV < 40 03
D45 1045 40 ≤ MV < 60 04
D45 1045 60 ≤ MV < 80 06
D45 1045 80 ≤ MV < 100 08
D45 1045 100 ≤ MV < 140 10
D45 1045 MV ≥140 14
Note : In the case of specific requirements for this characteristic, these are indicated in the designation by
the letters “XX” with a corresponding detailed note on the drawing.
Note : In the case of specific requirements for this characteristic, these are indicated in the designation by
the letter “X” followed by the suffix “Y”, with a corresponding detailed note on the drawing.
(*) Including the plenum collector.
Note : In the case of specific requirements for this characteristic, these are indicated in the designation by
the letter “X” followed by the suffix “Y”, with a corresponding detailed note on the drawing.
The water absorption rate under vacuum shall be tested in accordance with test method D45 1520.
A material showing an open cell percentage ≤ 50, determination in accordance with test method D45 1355
with a water absorption rate ≤ 26% shall be considered to be CELLULAR otherwise it shall be considered to
be SPONGY.
6.5. COMPRESSIBILITY
Compressibility = compression strength
The compressibility (Pn) shall be measured to 50% according to test method D41 1541 :
• at the 1st compression cycle for cellular materials,
• at the 5th compression cycle for spongy materials.
Compressibility
Documents Symbols
(daN/dm²)
D41 1541 1 ≤ Pn < 10 00
D41 1541 10 ≤ Pn < 20 01
D41 1541 20 ≤ Pn < 40 02
D41 1541 40 ≤ Pn < 80 04
D41 1541 80 ≤ Pn < 160 08
D41 1541 160 ≤ Pn < 300 16
D41 1541 300 ≤ Pn < 1000 30
Note : When the part does not allow the compressibility Pn to be defined, the two figures for the
compressibility index number are replaced by “XX” and the requirement replacing it (test and result)
must be shown on the drawing or in the documents.
Materials from different categories comply also with limit characteristics such as residual deformation
(DR), tear strength (Rd), compressibility variation, etc.
These characteristics are shown in specific documents according to Appendix 3.
This symbol shows the maximum compression rate of the part in its use on the vehicle. It must in terms of the
compressibility in relation to the surface of the compressed part.
Remark : If a part is not compressed uniformly, the maximum compression rate shall be retained for the
choice of symbol.
6.7. COMBUSTIBILITY
Note : In the case of specific requirements for these characteristics, these are indicated in the designation by
the letter “X” with a corresponding detailed note on the drawing.
A dash (-) means that there is no requirement.
Symbols and
Documents Characteristics Expression
requirements
of results 0 1 2 3
Colour fastness using the equipment CI 3000
D47 1431 (interior parts)
• After 200 hours
(if exposure behind tinted glass and/or Index - ≥4 - -
reflecting glass)
• After 240 hours Index - - ≥4 -
(if exposure behind clear glass)
Colour fastness to WEATHER OMETER
D27 1389
(exterior parts) No. 2 range – 3 cycles
Index - - - ≥4
Note : In the case of specific requirements for these characteristics, these are indicated in the designation by
the letter “X” with a corresponding detailed note on the drawing.
A dash (-) means that there is no requirement.
Note : In the case of specific requirements for these characteristics, these are indicated in the designation by
the letter “X” with a corresponding detailed note on the drawing.
A dash (-) means that there is no requirement.
The acoustic absorption coefficient is measured with the test specimen at the bottom of the tube, from 100 Hz to
6300 Hz.
The various acoustic efficiency classes are defined in Appendix 1.
The corresponding values are specified in the table of Appendix 1.
The curve analysis field ranges between 250 Hz and 6300 Hz.
3 points outside the class are tolerated (over the 15 points measured).
No point showing a variation of more than 5% lower than the referenced value of the class must be accepted.
In this case, the lower class must be considered as being the class for the absorbent.
Each measurement curve must be shown with values.
Note : If different results are obtained from the same sample between the two measuring equipment Kundt
tube according to test method D45 5014 and Impedance tube according to test method D45 5430,
only the results from the Impedance tube shall be used.
According to the function and efficiency required from the sound proofing material, an acoustic class
shall or shall not be specified (from 1 to 4). A dash (-) means that there is no requirement.
In the case of specific requirements for these characteristics, these are indicated in the designation by
the letter “X” with a corresponding detailed note on the drawing.
IN LABORATORY
Receiver supports
• Type Type (*)
• Preliminary cleaning (**)
• Temperature °C 23 ± 2
Alignment
• Pressure MPa 0,02
• Duration of application s 10
Conditioning of test specimens
• Temperature °C 23 ± 2
• Relative humidity % 50 ± 5
• Duration h 24
Appendix 1
ABSORPTION
MEASUREMENT WITH IMPEDANCE TUBE
Appendix 2 (1/3)
NUMERICAL CROSS REFERENCES
(2) The receiver substrate must be suitable for bonding, which means :
• clean
• unpolluted
• without condensation.
To achieve this, the work station for the carrier substrate must also be clean (free from dust, grease,
anti-adhesive product…).
Under no circumstances should the temperature of the receiver substrate be lower than that of the
workshop (condensation created by introducing a cold part into a warmer location is totally
incompatible with proper bonding). If it is lower than 15°C, the receiver substrate should be heated up.
In the case of a contaminated surface (dust, traces of grease…), cleaning with a lint free absorbent
paper soaked in alcohol (denatured alcohol or isopropanol) shall be necessary before bonding.
(3) • Parts bonded in Production Centres : Parts shall be transported and stored away from humidity
and external pollution. No detachment of the protective film or damage to parts are tolerated during
transport and storage.
The storage temperature shall be between – 10°C and 50°C; the exposure of parts to any significant
heat sources is to be avoided.
The protective film must be removed from the part without damage or tear, or loss of adhesive
property even after 6 months storage in the conditions stated above.
(4) The fitting of these parts shall be carried out manually. The temperature of the receiver substrate,
during bonding, shall be between 15°C and 40°C. A slight warm up at 35°C, 40°C shall reactivate the
glue and improve the adhesion immediately (in particular for parts which are not bonded on flat
substrates).
The protective film must not be removed beforehand. Any part retrieved from storage with a section of
the protective film removed, shall be scrapped.
All contact of the adhesive with a contaminated surface is to be avoided at all cost, in particular with
hands.
During application of pressure, care must be taken as not to damage or tear the part.
Note : For parts bonded onto several faces, care must be taken as not to elongate the part during
application or bond it under stress.
The part must be correctly positioned before applying the pressure so as to avoid any removing/re-
bonding which would damage the adhesive.
Appendix 2 (2/3)
NUMERICAL CROSS REFERENCES (continued)
(5) Self-adhesive cellular materials with a protective film with one anti-adhesive face minimum.
(7) After ageing, a maximum variation of plus or minus 20% is tolerated. During these tests, no tear of the
protective film or damage to the adhesive is tolerated.
Note : No detachment of the protective film during transport, storage and handling of parts is tolerated.
Trace symmetrical reference marks along the length L and the width L’ according to the above
diagram by means of a paring knife.
24 hours after bonding, subject the test specimen to the conditions shown in this norme (the maximum
operating temperature is specified in the § 6.2., according to the material designation).
After the test, condition the test specimen for 1 hour at 23°C ± 2°C and 50% ± 5% relative humidity.
Measure the dimensional variations by means of a suitable device capable of measuring 1/20 mm.
Express the results in mm (absolute values over L and L’).
(9) To check the adhesion, the peeling at right angle test shall be carried out in accordance with
test method D51 1485 or a tensile shear test in accordance with MES D41 1108 according to the
thickness, density and hardness of the material. However, the peeling at right angle test is preferred.
Appendix 2 (3/3)
NUMERICAL CROSS REFERENCES (continued)
(10) Definition of fluids and test conditions : select the fluids according to the stresses encountered on the
vehicles.
Method of
Designation Composition Drying time
exposure
Alcohol Denatured Ethanol Immersion 1 min 24 hours
Cleaning product Sodium lauryl sulphate diluted to Immersion 24 hours 24 hours
10 g/l in softened water
Temporary protection Conforming to 24 hours
D47 1279
product (*) norme B14 6855
Protection removal Conforming to Min. 2 hours
D47 1279
product (*) norme B74 6210 Max. 4 hours
50% 2-2-4 Trimethyl-pentane Immersion
AFNOR C 24 hours
50% Toluene 1 min
85% AFNOR C Immersion
CARBUROL 24 hours
15% Methanol 1 min
Conforming to STL 24 h at 23°C ± 2°C
Grease (**) 24 hours
S71 3106 then 10 cycles
D47 1309 AF
Appendix 3 (1/3)
SPA SAMPLE
Appendix 3 (2/3)
Appendix 3 (3/3)
8.1. RECORDS
8.1.1. CREATION
• OR : 01/12/1995 – CREATION OF THE NORME.
8.2.1.2 Others
8.3. EQUIVALENT TO :
8.4. CONFORMS TO :
8.5. KEY-WORDS