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Manual DeltaOHM HD2305

This document provides operating instructions for a pH meter and thermometer model HD2305.0. It includes 3 key points: 1. The instrument allows for measurement of pH, redox potential (ORP) in mV, and temperature using Pt100 or Pt1000 probes. 2. The pH electrode can be calibrated on one, two, or three points and temperature probes are fitted with an automatic detection module. 3. Other functions include maximum, minimum, and average readings, relative measurement, and automatic shut-off.
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0% found this document useful (0 votes)
82 views30 pages

Manual DeltaOHM HD2305

This document provides operating instructions for a pH meter and thermometer model HD2305.0. It includes 3 key points: 1. The instrument allows for measurement of pH, redox potential (ORP) in mV, and temperature using Pt100 or Pt1000 probes. 2. The pH electrode can be calibrated on one, two, or three points and temperature probes are fitted with an automatic detection module. 3. Other functions include maximum, minimum, and average readings, relative measurement, and automatic shut-off.
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd
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English

Operating Manual
pH Meter / Thermometer
HD2305.0

Companies / Brands of GHM

www.deltaohm.com
Keep for future reference
SOMMARIO

GENERAL CHARACTERISTICS ................................................................................................................................. 3

DESCRIPTION OF THE FUNCTIONS ........................................................................................................................ 6

THE PROGRAMMING MENU ..................................................................................................................................... 9

PROBES AND MEASUREMENT ................................................................................................................................ 10

THE ELECTRODE FOR pH MEASUREMENT ........................................................................................................ 10


Automatic or manual pH compensation 11
How to manually change the temperature 11
pH ELECTRODE CALIBRATION ....................................................................................................................................... 12
Calibration procedure 12
Temperature characteristics of Delta OHM buffer solutions 14
4 WIRE Pt100 AND 2 WIRE Pt1000 TEMPERATURE PROBES ......................................................................................... 15
Temperature measurement 15
Connecting the TP47 module for the 4 wire Pt100 and 2 wire Pt1000 probes 15
Direct connection of 4 wire Pt100 sensors to a DIN45326 connector 17
WARNINGS .................................................................................................................................................................... 18

INSTRUMENT SIGNALS AND FAULTS .................................................................................................................. 19

INSTRUMENT STORAGE ........................................................................................................................................... 20


Notes on pH electrodes use 20
LOW BATTERY WARNING AND BATTERY REPLACEMENT ......................................................................... 21

WARNING ABOUT BATTERY USE ................................................................................................................................... 21


NOTES ABOUT WORKING AND OPERATIVE SAFETY ..................................................................................... 22

TECHNICAL CHARACTERISTICS .......................................................................................................................... 23

TECHNICAL INFORMATION ON THE pH METER – THERMOMETER .................................................................................. 23


INSTRUMENT PROBES AND MODULES TECHNICAL DATA ........................................................................... 24
PH ELECTRODES....................................................................................................................................................... 24
SONDE DI TEMPERATURA .............................................................................................................................................. 24
TEMPERATURE PROBES PT100 SENSOR USING SICRAM MODULE .................................................................................... 24
Pt100 4-WIRE AND Pt1000 2-WIRE PROBES COMPLETE WITH TP47 MODULE .................................................................. 24
ORDERING CODES...................................................................................................................................................... 25

HD2305.0 - 2 - V1.6
GENERAL CHARACTERISTICS

The pH meter - Thermometer Model HD2305.0 is a portable instrument that allows measurement of
pH and redox potential (ORP) in mV.
It also measures the temperature using Pt100 or Pt1000 immersion, penetration or contact probes.
The electrode calibration can be carried out on one, two or three points at 4.01pH, 6.86pH and
9.18pH.
The temperature probes are fitted with the SICRAM automatic detection module, with the factory
calibration settings already being memorized inside.

The units of measurement for the measurable quantities are:


 pH
 mV
 °C
 °F
Using the Max, Min and Avg function of this instrument respectively obtains the maximum, mini-
mum or average values.

Other available functions are:

 the relative measurement REL;


 the automatic turning off which can also be disabled.

HD2305.0 - 3 - V1.6
pH meter - Thermometer
HD2305.0

HD2305.0 - 4 - V1.6
HD2305.0

1. 8-pole DIN45326 connector, input for Pt100 temperature probes with Sicram module, 4 wire di-
rect Pt100 probes, 2 wire Pt1000 probes complete with TP47 module.
2. pH/mV input, female BNC
3. Battery symbol: displays the battery charge level.
4. Function indicators.
5. Secondary display line.
6. DATA/ENTER key: during normal operation displays the maximum (MAX), the minimum
(MIN) and the average (AVG) of current measurements. In the menu, confirms the current se-
lection. In calibration mode, acquires the nominal buffer value.
7. pH-mV/ESC key: during normal operation switches the display between pH and mV; in the
menu, resets the value set with the arrows. In calibration mode, allows you to exit calibration.
8.  key: in the menu, increases the current value. In calibration mode, increases the displayed
nominal buffer value.
9. °C/°F/MENU key: it allows selection of the unit of measurement; when pressed together with
the DATA key, it allows to open the menu.
10. CAL: starts the calibration procedure.
11. /REL-mV key: during normal operation enables the relative measurement (displays the dif-
ference between the current value and the logged value when the key is pressed); press the key
again to return to the normal measurement. It works only if you are displaying the mV. In the
menu, decreases the current value. In calibration mode, decreases the displayed nominal buffer
value.
12. ON-OFF/AUTO-OFF key: turns the instrument on and off; when pressed together with the
°C/°F/MENU key, disables the AutoPowerOff function.
13. MAX (maximum value), MIN (minimum value) and AVG (average value) symbols.
14. Main display line.
15. Line for symbols and comments.

HD2305.0 - 5 - V1.6
DESCRIPTION OF THE FUNCTIONS
The keyboard of the pH meter Model HD2305.0 is composed of double-function keys. The function
on the key is the "main function", while the one above the key is the "secondary function".
When the instrument is in standard measurement mode, the main function is active.
Once the Settings Menu has been opened, by pressing simultaneously the DATA+°C/°F keys, the
secondary function is enabled.
The pressing of a key is accompanied by a short confirmation "beep": a longer "beep" sounds if the
wrong key is pressed. Each key specific function is described in detail below.

ON-OFF and AUTO-OFF key

This key has two functions:


 ON/OFF: to turn the instrument on press ON, to turn it off press OFF.
The turning on enables all display segments for a few seconds, starts an Auto-test including the de-
tection of the probe connected to the input, and sets the instrument ready for normal measurement.
The following is displayed:

mm min 23
k µ cm s

>>>
MIN

 AUTO/OFF: the AutoPowerOff function can be disabled by simultaneously pressing this key
and the "°C/°F-MENU" key when turning the instrument on.

During turning on, should no probes be connected, the "NO_PRBE_SER_NUM" message is dis-
played in the line for symbols for a few seconds, while the "ERR" message is shown in the central
part of the display, and the last manually-set temperature appears in the secondary line. The unit of
measurement symbol (°C or °F) starts blinking, and a letter "m" meaning "manual" appears next to
the battery symbol.
When the probe fitted with SICRAM module is inserted into a functioning instrument, the
"NEW_PROB_DET" (New probe detected) message appears, while the "ERR" message is
shown in the central part of the display, and a sequence of "beeps" is simultaneously issued. As the
data are captured upon turning the instrument on, it is necessary to turn it off and on again.
Caution! Replace the probes when the instrument is off.

HD2305.0 - 6 - V1.6
Tasto pH-mV/ESC

The "pH-mV" key has three functions:


 pH-mV: pressing this key once switches the display between pH and mV;
 ESC: once the MENU has been opened with the DATA+°C/°F keys, the "pH-mV" key will al-
low to cancel the parameters set using the  and  arrows.
 In calibration mode, it allows to exit calibration.

TDATA/ENTER key

The "DATA" key is used for the following functions:


 DATA: during normal measurement, by pressing this key once the maximum (MAX) value of
the measurements captured by the probe connected to the instrument is displayed, updating it
with the acquisition of new samples;
- by pressing this key again the minimum (MIN) value is displayed;
- by pressing this key, a third time the average (AVG) value is displayed.
The acquisition frequency is once a second.
The MAX, MIN and AVG values remain in the memory until the instrument is on, even after
exiting the DATA display function. When the instrument is off, the previously memorized data
are cleared. Upon turning on, the instrument automatically starts memorizing the MAX, MIN
and AVG values.
To reset the previous values and start with a new measurement session:
 press DATA until the FUNC_CLRD message appears;
 use the  and  arrows to select YES;
 confirm by pressing ENTER.
 ENTER: once the MENU has been opened with the DATA+°C/°F keys, the DATA key will
perform the ENTER function and the MENU can be browsed and the displayed parameter con-
firmed. In calibration mode, acquires the nominal buffer value.

 key

Una volta entrati nel MENU, tramite i tasti DATA e °C/°F, il tasto  permetterà di incrementare il
valore del parametro selezionato nel MENU. In calibrazione permette di incrementare il valore del
buffer nominale.

°C/°F/MENU Key

Il tasto °C/°F viene utilizzato per le seguenti funzioni:


 °C/°F: when the temperature probe is connected, the key changes the unit of measurement from
degrees Celsius to Fahrenheit. If the probe is not present, the compensation temperature must be
entered manually: to manually change the value shown in the display lower line, press °C/°F
once. The temperature indicated starts blinking. While the display is blinking, it is possible to

HD2305.0 - 7 - V1.6
change the compensation temperature using the arrows ( and ). Confirm using DA-
TA/ENTER. The display stops blinking, and the temperature displayed is used for compensa-
tion. If the temperature probe is not present, to change the unit of measurement between °C and
°F, it is necessary to press twice the °C/°F key.

 MENU: to access to the menu press simultaneously DATA+°C/°F: the Probe Type will be
displayed.
 use the  and  arrows (respectively located above the HOLD and REL keys) to modify
the displayed value;
 press DATA/ENTER to confirm the modification and go onto the next item;
 press CLR/ESC to cancel the modification;
 to exit the menu, press the °C/°F key again.

For more info, please see following chapter.

CAL key

Press this key to start the calibration procedure (vd. par. pH).

/ REL-Mv key

The "/ REL-mV" key is used for the following functions:


 REL-mV: it displays the difference between the current value and that measured on pressing
the key. The "REL" message is displayed on the left. To return to the normal measurement,
press the key again. It only works with mV, so to enable the REL function select the "mV" unit
of measurement using the "pH-mV" key.

 : Once the MENU has been opened with the °C/°F/MENU key, the  key will allow to de-
crease the value of the selected parameter. During electrode calibration, it allows to decrease the
nominal buffer value

HD2305.0 - 8 - V1.6
THE PROGRAMMING MENU
To access to the menu press simultaneously the following keys:

The item to be set is:


Probe type: the "PRBE_TYPE_RTD_" message is displayed in the comment line. The main line
in the center of the display shows the type of probe connected to the instrument. The following
probes can be connected to the input:
 temperature probes Pt100 complete with SICRAM module
 4 wire Pt100 probes through module TP47
 2 wire Pt1000 probes through module TP47
The probes fitted with SICRAM module, and Delta Ohm Pt1000 probes, are automatically detected
by the instrument upon turning on: the Probe Type menu item is configured by the instrument and
cannot be modified by the user.
The temperature probes direct 4 wire Pt100, and the Pt1000 probes that are not manufactured by
Delta OHM, when turned on display the message "NO_PRBE_SER_NUM". In this case the probe
type must be entered manually.

Access to the menu by selecting Probe type using the DATA and °C/°F keys at the same time:
- use the  and  arrows to modify the displayed value;
- press DATA/ENTER to confirm the modification and go onto the next item;
- press pH-mV/ESC to cancel the modification;
- to exit the menu, press the °C/°F key again.

HD2305.0 - 9 - V1.6
PROBES AND MEASUREMENT
The instrument works with the following probes:
 electrodes for pH measurement;
 electrodes for redox potential ORP measurement (REDOX);
 specific ion electrodes.

Caution! The pH measurement is influenced by the temperature measurement.

The temperature is used for the automatic compensation of the Nernst coefficient with the pH
electrode.
The measurement can be performed using probes with the following sensor:
 4 wire Pt100;
 2 wire Pt1000;
Some probes are fitted with SICRAM module that acts as an interface between the sensor on the
probe and the instrument. There is a microprocessor circuit with a permanent memory inside the
module that enables the instrument to recognize the type of probe connected and to read its calibra-
tion information.
The Delta Ohm Pt1000 probes are automatically detected while the direct 4 wire Pt100 temperature
probe is not automatically detected by the instrument and must be set up in the Probe type menu
item (please see the menu description on chapter 3).
The pH or mV indication is displayed in the main line; the secondary line shows the temperature.
The probes are detected during turn on, and this cannot be performed when the instrument is
already on, therefore if a probe is connected and the instrument is on, it is necessary to turn it
off and on.

The probes fitted with SICRAM module are calibrated in the factory; no calibration is required by
the user.

THE ELECTRODE FOR pH MEASUREMENT

The electrode for pH measurement, generally in glass, generates an electrical signal proportional to
the pH according to Nernst law. Of this signal the following aspects are considered:
 Zero point: The pH where the electrode generates a potential of 0 mV. In most electrodes, this
value is found at about 7 pH.
 Offset or Asymmetry Potential: represents the potential (in mV) generated by an electrode when
immersed in a buffer solution at 7 pH. Generally oscillates between ± 20 mV.
 Slope: response of the electrode expressed in mV per pH units. The theoretical electrode slope at
25°C is 59.16 mV/pH. When the electrode is new the slope is close to the theoretical value.
 Sensitivity: it is the electrode's slope expression in relative terms. It is obtained by dividing the
actual value of the slope by the theoretical value, and is expressed as a %. The asymmetry po-
tential and the slope vary in time with the use of the electrode, which necessitates regular cali-
bration.

HD2305.0 - 10 - V1.6
The pH electrodes must be calibrated using the buffer solutions (see paragraph pH electrode calibra-
tion).
The ORP and specific ion electrodes do not need calibration as their absolute voltage is measured.
The ORP (REDOX) buffer solutions are only used to check the quality of an ORP (REDOX) elec-
trode.
User calibration of the temperature sensor is not required: the sensor is calibrated in the fac-
tory and the Callendar Van Dusen parameters are recorded in the SICRAM module.

Automatic or manual pH compensation


In a correct measurement of pH, the results need to be expressed together with the temperature val-
ue at which the reading is performed.
The electrode slope varies according to the temperature in a known mode according to Nernst law:
e.g., a 1pH variation, that at 25°C means 59.16mV, at 100°C means 74.04mV.

mV
74.04mV T=100°C, 74.04mV/pH

59.16mV T=25°C, 59.16mV/pH


54.20mV

T=0°C, 54.20mV/pH

pH
0mV

6pH 7pH 8pH

-54.20mV

-59.16mV
-74.04mV

When a temperature probe is present, the instrument automatically applies the ATC function: au-
tomatic temperature compensation. To disable it, the temperature probe must be disconnected.
If the temperature probe is not present, and the correct value is not entered manually, the extent of
the error committed in pH measurement is proportional to temperature and pH value itself.
In absence of the temperature probe, the lower part of the display shows the manually set compen-
sation temperature. By default, it is equal to 25°C (see par. 4.1.2 how to manually change the tem-
perature).
To point this condition out, the °C or °F symbol blinks intermittently near the temperature value.
Moreover, in the main line an "m" (that is, manual) is turned on near the battery symbol.

How to manually change the temperature


In absence of the temperature probe, it is possible to manually set the temperature. Proceed as fol-
lows:
 press the °C/°F key once: the indicated temperature value starts blinking;
 select the solution temperature value by using the arrows;
 confirm by pressing DATA: the display stops blinking, and the temperature displayed is used
for compensation.

HD2305.0 - 11 - V1.6
 During manual compensation, to change the unit of measurement between °C and °F, it is nec-
essary to press twice the °C/°F key.

pH ELECTRODE CALIBRATION

The electrode calibration is used to compensate the zero potential and slope departures to which the
electrode is subject with time.
The calibration frequency depends on the accuracy desired by the user and by the effects that the
measured sample have on the electrode.
Generally, we recommend daily calibration, but it is the user's responsibility from personal experi-
ence, to establish the most appropriate frequency.

The calibration may be carried out using 1, 2 or 3 points.


 when using 1 point, the electrode offset is corrected;
 with 2 points the offset and the gain is corrected;
 finally, in case a three points calibration is carried out two offsets and two slopes are calculated,
the second point is the one in which the zero is performed.

The instrument has a memory of 3 buffers with relevant temperature compensation tables (ATC),
one for the acid, one for the neutral, and one for the alkaline band:
@25°C

BUFR_1 (NEUTRI) 6.860


BUFR_2 (ACIDI) 4.010
BUFR_3 (ALCALINI) 9.180

If electrode calibration was not carried out on the instrument, or the batteries have been
changed or the last calibration failed, the display blinks the CAL message.

Calibration procedure

1) Insert the temperature probe and the electrode in the solution of a calibration buffer. If no tem-
perature probe is available, use another thermometer and enter the value manually as indicated in
the paragraph ‘Automatic or Manual pH Compensation’.
2) The electrode calibration is started by pressing CAL.
3) Among the three prepared buffers, the instrument automatically detects the closest to the pH val-
ue being read and flags it up on the lower part of the display.
If the buffer is not detected the first buffer BUFR_1 is proposed.
4) At this point the CAL symbol is not blinking on the display and the following is shown from the
upper side downward:
a) the chosen buffer nominal value at 25°C (scrolling indication)
b) the pH measurement value with the current calibration
c) the temperature compensated buffer value
The detected and temperature compensated buffer value, shown in the lower line, can be modi-
fied using the arrows.

HD2305.0 - 12 - V1.6
5) Press DATA/ENTER to proceed with the calibration. The electrode offset mV value (OFFS) is
shown on the display for few seconds.
After a few seconds the instrument shows the measurement again, corrected according to the
new calibration, but remains in calibration mode.
Pressed repeatedly the DATA/ENTER key allows the calibration on the point to be repeated, for
example, in order to obtain a more stable value.
6) To end the electrode calibration press pH/mV (ESC), or continue the calibration for the second
point.
7) Extract the electrode from the buffer, clean it carefully, and insert it in the following buffer.
8) Press one time the °C/°F key (MENU).
9) The instrument displays the value detected on the new buffer: continue by repeating the steps
from point 3.
NOTES:
 After calibration, the instrument displays an electrode quality indication:
- no signal: electrode functioning.
- a small square blinking on the lower right: electrode almost exhausted.
- two small squares blinking on the lower right: electrode exhausted to be replaced.
 The 3-point calibration must always be carried out according to the fixed sequence: NEU-
TRAL>>ACID>>BASIC. The basic buffer must be the last in the sequence.
 Without having pressed DATA/ENTER at all, the calibration is interrupted by pressing
pH/mV (ESC); the previous values will continue to be used.
 The buffers are always presented in the sequence set in the menu with the parameters:
- BUFR_1,
- BUFR_2,
- BUFR_3.
 The 2 point calibration is possible using the sequence BUFR_1 - BUFR_2 or BUFR_2 -
BUFR_3 or even BUFR_1 - BUFR_3.
The 3-point calibration is only possible using the exact sequence BUFR_1 - BUFR_2 -
BUFR_3.

Allowed calibration sequences

1 BUFR_1 BUFR_2 BUFR_3


calibration
Number of

points

2 BUFR_1 - BUFR_2 BUFR_2 - BUFR_3 BUFR_1 - BUFR_3

3 BUFR_1 - BUFR_2 - BUFR_3

 In any case where no operation is performed, the “calibration” mode automatically stops
after 60 seconds.
 If the calibration is rejected by the instrument because it is considered to be excessively corrupt-
ed, the CAL ERR message will appear, followed by a long beep. The instrument remains in cal-
ibration mode and maintains the previous calibration values: at this point, if the calibration is in-
terrupted using pH-mV/ESC, the instrument signals the anomaly through the CAL message
blinking.

HD2305.0 - 13 - V1.6
Temperature characteristics of Delta OHM buffer solutions
The 3 standard buffers are memorized in the instruments with relevant variations according to tem-
perature: the characteristics of the three Delta Ohm standard buffers at 6.86pH, 4.01pH and 9.18pH
(@25°C) are reported below.

6.86 pH @ 25°C 4.01 pH @ 25°C


°C pH °C pH °C pH °C pH
0 6.98 50 6.83 0 4.01 50 4.06
5 6.95 55 6.83 5 4.00 55 4.07
10 6.92 60 6.84 10 4.00 60 4.09
15 6.90 65 6.85 15 4.00 65 4.10
20 6.88 70 6.85 20 4.00 70 4.13
25 6.86 75 6.86 25 4.01 75 4.14
30 6.85 80 6.86 30 4.01 80 4.16
35 6.84 85 6.87 35 4.02 85 4.18
40 6.84 90 6.88 40 4.03 90 4.20
45 6.83 95 6.89 45 4.05 95 4.23

9.18 pH @ 25°C
°C pH °C pH
0 9.46 50 9.01
5 9.39 55 8.99
10 9.33 60 8.97
15 9.28 65 8.94
20 9.22 70 8.92
25 9.18 75 8.90
30 9.14 80 8.88
35 9.10 85 8.86
40 9.07 90 8.85
45 9.04 95 8.83

HD2305.0 - 14 - V1.6
4 WIRE Pt100 AND 2 WIRE Pt1000 TEMPERATURE PROBES

The instrument accepts the input of Platinum temperature probes with resistances of 100Ω (Pt100)
and 1000Ω (Pt1000).
The Pt100 are connected to 4 wires, the Pt1000 to 2 wires; the excitation current was chosen in or-
der to minimize the sensor self-heating effects.
All probes with SICRAM module are calibrated in the factory; the 2 or 4 wire probes with direct in-
put are checked for conformity with class A tolerance according to norm IEC751 - BS1904 -
DIN43760.
For the temperature probes without SICRAM module (Pt100 4 wires, and Pt1000) the model con-
figuration is required (please see the description of the Probe Type menu).

Temperature measurement
The response time for the measurement of the temperature in air is greatly reduced if the air is mov-
ing. If the air is still, stir the probe. Please remember that the response times in any case are longer
than those for liquid measurements.
The temperature measurement by immersion is carried out by inserting the probe in the liquid for at
least 60 mm; the sensor is housed in the end part of the probe.
In the temperature measurement by penetration the probe tip must be inserted to a depth of at least
60 mm, the sensor is housed in the end part of the probe.
NOTE: when measuring the temperature on frozen blocks it is convenient to use a mechanical tool
to bore a cavity in which to insert the tip probe.
In order to perform a correct contact measurement, the measurement surface must be even and
smooth, and the probe must be perpendicular to the measurement plane.
So as to obtain the correct measurement, the insertion of a drop of oil or heat-conductive
paste between the surface and the probe is useful (do not use water or solvents). This method
also improves the response time.

Connecting the TP47 module for the 4 wire Pt100 and 2 wire Pt1000 probes
All probes produced by Delta OHM are provided with a TP47 module.
The HD2305.0 instrument also work with direct 4 wire Pt100, and 2 wire Pt1000 probes manufac-
tured by other producers: for the instrument connection is prescribed the TP47 connector to which
the probe's wires should be welded.

The instructions to connect the Platinum probe to the TP47 module are provided below. The TP47
module is supplied complete with fairlead and gasket for 5 mm maximum diameter cables. Do the
following to open the module and connect a probe:
1. unscrew the fairlead;
2. extract the gasket;
3. remove the label using a cutter;
4. unscrew the ring on the opposite side as illustrated in the figure:

HD2305.0 - 15 - V1.6
5. open the two module shells: the printed circuit to which the probe must be connected is
housed inside. On the left there are the 1…4 points on which the sensor wires must be weld-
ed. The JP1…JP4 jumpers are in the center of the board. These must be closed with a tin
bead for some type of sensors:

4 N
otUs
ed
3 N
i
1 0
00
2 P
t
1 0
00
1 P
t
1 0
03f
il
i

Caution! Before welding, pass the probe cable through the fairlead and gasket.

6. Weld the wires as shown in the table:

Sensor TP47 board connection Jumper to close

4 JP4
Pt100 3 JP3
Pt100 4 wires 4 wires 2 JP2 None
1 JP1

4 JP4
Pt1000 3 JP3
Pt1000 2 wires 2 wires 2 JP2
JP2
1 JP1

Ensure the welds are clean and perfect.

7. Once the welding operation is complete, close the two shells;


8. insert the gasket in the module;
9. screw the fairlead. At the other end of the module, enter the ring with the O-Ring as indicat-
ed in the picture.

HD2305.0 - 16 - V1.6
Direct connection of 4 wire Pt100 sensors to a DIN45326 connector

Sensor Direct soldering to the connector 4 wire Pt100 sensors can be soldered di-
rectly to the pins of the flying female
connector DIN45326 without making use
of the TP47 board. The 4 wires of the
Pt100 sensors have to be soldered as in-
dicated in the figure on the left. In order
Pt100 4 to use this type of probe it is necessary to
wires set up the menu item “Probe Type” as
described at page 8. The P100 probe is
recognized upon turning on the instru-
View of the soldering side ment: connect the probe when the in-
of the flying female connector strument is switched off and then turn it
on. This connector does not guarantee the
IP67 protection degree.

HD2305.0 - 17 - V1.6
WARNINGS
1. Do not expose the probes to gases or liquids that could corrode the material of the sensor or the
probe itself. Clean the probe carefully after each measurement.
2. Do not bend the probe connectors or force them upward or downward.
3. Do not bend or force the contacts when inserting the probe connector into the instrument.
4. Do not bend, deform or drop the probes, as this could cause irreparable damage.
5. Always select the most suitable probe for your application.
6. Do not use the temperature probes in presence of corrosive gases or liquids. The sensor contain-
er is made of AISI 316 stainless steel, while the contact probe container is made from AISI 316
stainless steel plus silver. Avoid contact between the probe surface and any sticky surface or
product that could corrode or damage it.
7. Above 400°C and below –40°C, avoid violent blows or thermal shocks to Platinum temperature
probes as this could cause irreparable damage.
8. To obtain reliable measurements, temperature variations that are too rapid must be avoided.
9. Temperature probes for surface measurements (contact probes) must be held perpendicular
against the surface. Apply oil or heat-conductive paste between the surface and the probe in or-
der to improve contact and reduce reading time. Whatever you do, do not use water or solvent
for this purpose. A contact measurement is always very hard to perform. It has high levels of
uncertainty and depends on the ability of the operator.
10. Temperature measurements on non-metal surfaces usually require a great deal of time due to the
low heat conductivity of non-metal materials.
11. Probes are not insulated from their external casing; be very careful not to come into contact with
live parts (above 48V). This could be extremely dangerous for the instrument as well as
for the operator, who could be electrocuted.
12. Avoid taking measurements in presence of high frequency sources, microwave ovens or large
magnetic fields; results may not be very reliable.
13. Clean the probe carefully after use.
14. The instrument is water resistant and IP67, but should not be immersed in water. The probe
connectors must be fitted with sealing gaskets. Should the instrument fall into the water, check
for any water infiltration. Gently handle the instrument in such a way as to prevent any water in-
filtration from the connectors' side.

HD2305.0 - 18 - V1.6
INSTRUMENT SIGNALS AND FAULTS
The following table lists all error indications and information displayed by the instrument and sup-
plied to the user in different operating situations:

Display indications Explenation


>>>_PRBE_TYPE type of probe connected
BATT TOO LOW - CHNG NOW battery discharged - replace it immediately
BAUDRATE >>> baud rate value
BUFR_1 first buffer value
BUFR_2 second buffer value
BUFR_3 third buffer value
CAL Program error: it appears after turning on for a few seconds. Contact the instru-
LOST ment's supplier.

CAL
Calibration not completed correctly.
blinking
CAL ERR calibration error
This message appears if the pH measurement exceeds the -2.000pH…19.999pH
limits, if the mV measurement exceeds the 2.4V limits, if the temperature
ERR
probe, already detected by the instrument, is disconnected. At the same time an
intermittent beep is issued.
FUNC CLRD max, min and average values cleared
NEW_PROB_DET new probe detected
OFFS offset
Measurement overflow: this appears when the probe measures a value exceed-
OVER ing the measurement range or the mV measurement is included in the
+2.0…+2.4V range.
PLS_EXIT >>> FUNC please exit using ESC >>> function reserved to factory calibration
RES_FOR_FACT ONLY
PRBE_SER #### #### serial number #### #### of the connected probe
PROB A probe with SICRAM module has been inserted when not admissible for that
ERR specific instrument.

This appears if the probe, has already been detected by the instrument, but is
PROB COMM LOST
disconnected. At the same time an intermittent beep is issued.
SLPE% gain %
SYS
Instrument management program error. Contact the instrument's supplier and
ERR
communicate the numeric code # reported by the display.
#
Measurement overflow: this appears when the mV measurement is included in
UNDR
the -2.4…-2.0V range.

HD2305.0 - 19 - V1.6
INSTRUMENT STORAGE
Instrument storage conditions:
 Temperature: -25…+65°C.
 Humidity: less than 90%RH without condensation.
 Do not store the instrument in places where:
 humidity is high;
 the instrument may be exposed to direct sunlight;
 the instrument may be exposed to a source of high temperature;
 the instrument may be exposed to strong vibrations;
 the instrument may be exposed to steam, salt or any corrosive gas.

The instrument case is made of ABS plastic: do not use any incompatible solvent for cleaning.

Notes on pH electrodes use

The average life of a pH electrode is about one year according to the use and maintenance per-
formed.
The electrodes used at high temperatures or in highly alkaline environments have a shorter life.
The new electrodes must be conditioned for half a day by immersing them into a buffer at 6.86pH
or 4pH.
Calibrate the electrode with solutions closer to the values being measured. A new electrode must
always be calibrated at neutral pH (6.86pH) first point and at least a second point.
Some of the most frequent problems and their possible solutions are reported below.
Wrong pH measurement. Carry out the following checks:
Check that the diaphragm is not obstructed and possibly clean it using the HD62PT solution.
Check that the reference system is not contaminated and, in case of a filling type electrode, replace
the electrolyte with the KCL3M solution.
Check that no air bubbles are present in the electrode tip and that it is sufficiently immersed.
Even dirt residuals deposited on the membrane can alter the measurement: use the HD62PP solu-
tion for protein cleaning.
Slow response or wrong measurements. Possible causes are aging or erosion of the membrane or
a connector short circuiting.

Storage. Keep the electrode immersed in the HD62SC solution.

HD2305.0 - 20 - V1.6
LOW BATTERY WARNING AND BATTERY REPLACEMENT
The battery symbol
on the display constantly shows the battery charge status. To the extent that batteries have dis-
charged, the symbol "empties". When the charge decreases still further it starts blinking.

In this case, batteries should be replaced as soon as possible.


If you continue to use it, the instrument can no longer ensure correct measurement. The memory da-
ta are maintained.
If the battery charge level is insufficient, the following message appears when you turn the in-
strument on:
BATT TOO LOW
CHNG NOW
The instrument issues a long beep and turns off. In this case, replace the batteries in order to
turn the instrument back on.
To replace the batteries, proceed as follows:
1. switch the instrument off;
2. unscrew the battery cover counter clockwise;
3. replace the batteries (3 1.5V alkaline batteries - type AA);
4. screw the cover on clockwise.

Malfunctioning upon turning on after battery replacement


After replacing the batteries, the instrument may not restart correctly; in this case, repeat the opera-
tion.
After disconnecting the batteries, wait a few minutes in order to allow circuit condensers to dis-
charge completely; then reinsert the batteries.

WARNING ABOUT BATTERY USE

 Batteries should be removed when the instrument is not used for an extended time.
 Flat batteries must be replaced immediately.
 Avoid batteries leaking.
 Always use good quality leakproof alkaline batteries. Sometimes on the market, it is possi-
ble to find new batteries with an insufficient charge capacity.

HD2305.0 - 21 - V1.6
NOTES ABOUT WORKING AND OPERATIVE SAFETY

Authorized use

The technical specifications as given in chapter TECHNICAL CHARACTERISTICS must be ob-


served. Only the operation and running of the measuring instrument according to the instructions
given in this operating manual is authorized. Any other use is considered unauthorized.

General safety instructions

This measuring system is constructed and tested in compliance with the EN 61010-1 safety regula-
tions for electronic measuring instruments. It left the factory in a safe and secure technical condi-
tion.
The smooth functioning and operational safety of the measuring system can only be guaranteed if
the generally applicable safety measures and the specific safety instructions in this operating manu-
al are followed during operation.
The smooth functioning and operational safety of the instrument can only be guaranteed under the
environmental and electrical operating conditions that are in specified in chapter TECHNICAL
CHARACTERISTICS.

Do not use or store the product in places such as listed below:


 Rapid changes in ambient temperature which may cause condensation.
 Corrosive or inflammable gases.
 Direct vibration or shock to the instrument.
 Excessive induction noise, static electricity, magnetic fields or noise.

If the measuring system was transported from a cold environment to a warm environment, the for-
mation of condensate can impair the functioning of the measuring system. In this event, wait until
the temperature of the measuring system reaches room temperature before putting the measuring
system back into operation.

Obligations of the purchaser

The purchaser of this measuring system must ensure that the following laws and guidelines are ob-
served when using dangerous substances:
 EEC directives for protective labour legislation
 National protective labour legislation
 Safety regulations

HD2305.0 - 22 - V1.6
TECHNICAL CHARACTERISTICS
TECHNICAL INFORMATION ON THE pH METER – THERMOMETER
Instrument
Dimensions (Length x Width x Height) 140x88x38mm
Weight 160g (complete with batteries)
Material ABS
Display 2x4½ digits plus symbols
Visible area: 52x42mm
Operating conditions
Operating temperature -5…50°C
Warehouse temperature -25…65°C
Working relative humidity 0…90%RH without condensation
Protection degree IP67
Power
Batteries 3 x 1.5V type AA batteries
Autonomy 200 h with 1800mAh alkaline batteries
Power absorbed with instrument off < 20A
Connections
Input module for the temperature probes 8-pole male DIN45326 connector
pH/mV input Female BNC
Unit of Measurement pH – mV - °C - °F;
Measurement of pH by Instrument
Measurement range -2.00…+19.999pH
Resolution 0.01
Accuracy 0.01pH 1digit
Input impedance >1012
Calibration error @25°C |Offset| > 20mV
Slope < 50mV/pH or Slope > 63mV/pH
Sensitivity < 85% or Sensitivity > 106.5%
Automatic/manual temperature compensation -50…+150°C
Measurement of mV by Instrument
Measurement range -1999.9…+1999.9mV
Resolution 0.1mV
Accuracy 0.1mV 1digit
Drift after 1 year 0.5mV/year
Measurement of temperature by Instrument
Pt100 measurement range -200…+650°C
Pt1000 measurement range -200…+650°C
Resolution 0.1°C
Accuracy 0.1°C 1digit
Drift after 1 year 0.1°C/year

HD2305.0 - 23 - V1.6
INSTRUMENT PROBES AND MODULES TECHNICAL DATA
pH ELECTRODES

ORDERING
MEASURING RANGE AND USE DIMENSIONS
CODES

0…14pH / 0…80°C / 3bar


Corpo in Epoxy - GEL
1 diaframma ceramico
Cavo L=1m con BNC
KP30
Acqua di scarico, Acqua potabile,
Emulsioni acquose, Galvaniche, Colo-
ri, Vernici, Sospensioni acquose, Suc-
chi di frutta, Titolazione.

SONDE DI TEMPERATURA

TEMPERATURE PROBES PT100 SENSOR USING SICRAM MODULE

Model Type Application Range Accuracy


TP472I Immersion -196°C…+500°C
TP472I.O Immersion -50°C…+300°C
TP473P.I Penetration -50°C…+400°C
TP473P.O Penetration -50°C…+300°C
TP474C.O Contact -50°C…+300°C ±0.1°C (@ 0 °C)
±0.2°C (-50 °C ≤ t ≤
TP475A.O Air -50°C…+250°C
250 °C)
TP472I.5 Penetration -50°C…+400°C ±0.3°C (t < -50 °C; t >
250 °C)
TP472I.10 Penetration -50°C…+400°C
TP49A.I Immersion -70°C…+250°C
TP49AC.I Contact -70°C…+250°C
TP49AP.I Penetration -70°C…+250°C
TP87.O Immersion -50°C…+200°C
Temperature drift @20°C 0.003%/°C
Pt100 4-WIRE AND Pt1000 2-WIRE PROBES COMPLETE WITH TP47 MODULE

Model Type Application Range Accuracy


TP47.100.O Pt100 4 wires -50…+250°C Classe A
TP47.1000.O Pt1000 2 wires -50…+250°C Classe A
TP87.100.O Pt100 4 wires -50…+200°C Classe A
TP87.1000.O Pt1000 2 wires -50…+200°C Classe A
Temperature drift @20°C 0.005%/°C

TP47 Modulo per il collegamento agli strumenti della serie HD23… di sonde Pt100 a 4 fili e
Pt1000 a 2 fili senza elettronica di ampificazione e linearizzazione.

HD2305.0 - 24 - V1.6
ORDERING CODES
HD2305.0 The kit is composed of: instrument HD2305.0, 3 1.5V alkaline batteries, operating
manual and case.
HD22.2 Laboratory electrode holder composed of basis plate with incorporated magnetic
stirrer, staff and replaceable electrode holder. Height max. 380mm. For 12mm
electrodes.
HD22.3 Laboratory electrode holder with metal basis plate. Flexible electrode holder for
free positioning. For Ø 12mm probes.
pH/mV electrodes, temperature probes, standard reference solutions for different
measurement types, connection cables have to be ordered separately.
pH ELECTRODES

KP30 Combined pH electrode for common use, GEL filled, cable 1m with BNC, Epoxy
body
CP Extension cable 1.5m with BNC connectors on one side and S7 on the other side
for electrode with S7 connector.
BNC Female BNC for electrode extension.

pH STANDARD SOLUTIONS

HD8600C ACCREDIA ISO 17025 certified buffer solutions kit: pH 4.01+ pH 7.00 + pH
10.01. Two 50 ml bottles for each type (6 bottles in total).
HD8642 Standard solution 4.01pH - 200cc.
HD8672 Standard solution d 6.86pH - 200cc.
HD8692 Standard solution d 9.18pH - 200cc.

REDOX STANDARD SOLUTIONS

HDR220 Redox standard solution 220mV 0,5 l.


HDR468 Redox standard solution 468mV 0,5 l.

ELECTROLYTE SOLUTIONS

KCL 3M 100ml ready for use solution for refilling of the electrodes

CLEANING AND MAINTENANCE

HD62PT Diaphragm cleaning (tiourea in HCl) – 500ml.


HD62PP Protein cleaning (pepsina in HCl) – 500ml.
HD62RF Regeneration (acido fluoridrico) – 100ml.
HD62SC Solution for electrode preservation – 200ml.

HD2305.0 - 25 - V1.6
TEMPERATURE PROBES COMPLETE WITH SICRAM MODULE
TP472I Immersion probe, sensor Pt100. Stem Ø 3 mm, length 300 mm. Cable length 2
metres.
TP472I.O Immersion probe, sensor Pt100. Stem Ø 3 mm, length 230 mm. Cable length 2
metres.
TP473P.I Penetration probe, sensor Pt100. Stem Ø 4mm, length 150 mm. Cable length 2
metres.
TP473P.O Penetration probe, sensor Pt100. Stem Ø 4mm, length 150 mm. Cable length 2
metres.
TP474C.O Contact probe, sensor Pt100. Stem Ø 4 mm, length 230 mm, contact surface Ø
5 mm. Cable length 2 metres.
TP475A.O Contact probe, sensor Pt100. Stem Ø 4 mm, length 230 mm, contact surface Ø
5 mm. Cable length 2 metres.
TP472I.5 Immersion probe, sensor Pt100. Stem Ø 6 mm, length 500 mm. Cable length 2
metres.
TP472I.10 Immersion probe, sensor Pt100. Stem Ø 6 mm, length 1000 mm. Cable length 2
metres
TP49A.I Immersion probe, sensor Pt100. Stem Ø 2.7 mm, length 150 mm. Cable length 2
metres. Aluminium handle.
TP49AC.I Contact probe, sensor Pt100. Stem Ø 4 mm, length 150 mm. Cable length 2
metres. Aluminium handle.
TP49AP.I Penetration probe, sensor Pt100. Stem Ø 2.7 mm, length 150 mm. Cable length 2
metres. Aluminium handle.
TP87.O Immersion probe, sensor Pt100. Stem Ø 3 mm, length 70 mm. Cable length 2
metres.

TEMPERATURE PROBES WITHOUT SICRAM MODULE

TP47.100.O Immersion probe, sensor Pt100 direct 4 wires. Probe's stem Ø 3mm, length
230mm. 4-wire connection cable with connector, length 2 metres.
TP47.1000.O Immersion probe, sensor Pt1000. Probe's stem Ø 3mm, length 230mm. 2-wire
connection cable with connector, length 2 metres.
TP87.100.O Immersion probe, sensor Pt100 direct 4 wires. Probe's stem Ø 3mm, length 70mm.
4-wire connection cable with connector, length 1 metre.
TP87.1000.O Immersion probe, sensor Pt1000. Probe's stem Ø 3mm, length 70mm. 2-wire
connection cable with connector, length 1 metre.
TP47 Only connector for probe connection: Pt100 direct 4 wires, Pt1000 and Ni1000 2
wires.

HD2305.0 - 26 - V1.6
GUARANTEE

TERMS OF GUARANTEE
All DELTA OHM instruments are subject to accurate testing, and are guaranteed for 24 months from the
date of purchase. DELTA OHM will repair or replace free of charge the parts that, within the warranty
period, shall be deemed non efficient according to its own judgement. Complete replacement is excluded
and no damage claims are accepted. The DELTA OHM guarantee only covers instrument repair. The
guarantee is void in case of incidental breakage during transport, negligence, misuse, connection to a
different voltage than that required for the appliance by the operator. Finally, a product repaired or
tampered by unauthorized third parties is excluded from the guarantee. The instrument shall be returned
FREE OF SHIPMENT CHARGES to your dealer. The jurisdiction of Padua applies in any dispute.

The electrical and electronic equipment marked with this symbol cannot be disposed of in public
landfills. According to the Directive 2011/65/EU, the european users of electrical and electronic
equipment can return it to the dealer or manufacturer upon purchase of a new one. The illegal
disposal of electrical and electronic equipment is punished with an administrative fine.

This guarantee must be sent together with the instrument to our service centre.
IMPORTANT: Guarantee is valid only if coupon has been correctly filled in all details.

Instrument Code:  HD2305.0

Serial Number

RENEWALS

Date Date
Inspector Inspector

Date Date
Inspector Inspector

Date Date
Inspector Inspector
GHM GROUP – Delta OHM | Delta Ohm S.r.l. a socio unico
Via Marconi 5 | 35030 Caselle di Selvazzano | Padova | ITALY
Phone +39 049 8977150 | Fax +39 049 635596
www.deltaohm.com | [email protected]

The quality level of our instruments is the result of the constant development of the product. This may
produce some differences between the information written in this manual and the instrument you have
purchased. We cannot completely exclude the possibility of errors in the manual, for which we apologize.
The data, images and descriptions included in this manual cannot be legally asserted. We reserve the
right to make changes and corrections with no prior notice.
GHM GROUP – Delta OHM | Delta Ohm S.r.l. a socio unico
Via Marconi 5 | 35030 Caselle di Selvazzano | Padova | ITALY
Phone +39 049 8977150 | Fax +39 049 635596
www.deltaohm.com | [email protected]

V1.6
01/09/2020

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