Distilasi Kondisi 2 REV FIX
Distilasi Kondisi 2 REV FIX
℃ T( ) Flowrate (L/h)
No t (menit)
F D B F D
1 0 35.6 34.2 47.6 75 50
2 10 36.3 31 50.1 75 50
3 20 38.2 37.6 58.3 75 50
4 30 30.5 40.7 60.8 75 50
5 50 35.5 45.2 63.1 75 50
6 65 38.6 38.4 74.7 75 50
7 80 36.6 34.2 62.8 75 50
8 95 36.4 44 70 65 50
9 110 38.6 46 84.8 65 50
10 125 40 35.7 76 65 50
11 140 35.7 40.4 70 65 50
KONDISI 1
a. Perhitungan Pada Feed
No T feed (C) F Feed (L/h) %etanol(v/v) ρ etanol(kg/L) ρ air(kg/L) %etanol (m/m)
1 85 75 15% 0.7299 0.968585 0.11737466059
2 85.3 75 21% 0.7296 0.9683903 0.16685754959
3 87 75 15% 0.7278 0.967287 0.11721518747
4 82.4 75 12% 0.7326 0.9702724 0.09334944538
5 85.3 75 17% 0.7296 0.9683903 0.13368456732
6 86.7 75 17% 0.7282 0.9674817 0.13357087933
7 89.3 75 16% 0.7254 0.9657943 0.12515916481
rata-rata 85.86 75 16% 0.7290142857143 0.9680287 0.1267444935
Perhitungan Distilasi
No T Distilat ( C) F Distilat (L/h) %etanol(v/v) ρ etanol(kg/L) ρ air(kg/L) %etanol (m/m)
1 80.9 50 47% 0.7342 0.9712459 0.40132614989
2 82 50 50% 0.733 0.970532 0.43028249543
3 84.6 50 52% 0.7304 0.9688446 0.44955491261
4 83.3 50 51% 0.7317 0.9696883 0.43989240134
5 81.9 50 50% 0.7332 0.9705969 0.43033298159
6 82.3 50 50% 0.7323 0.9703373 0.4300974729
7 79.6 50 51% 0.7355 0.9720692 0.44056456402
rata-rata 82.09 50.00 50% 0.73290 0.97047 0.43172
Perhitungan Bottom
No T bottom ( C ) F bottom ( L/h) %etanol(v/v) ρ etanol(kg/L) ρ air(kg/L) %etanol (m/m)
1 79 25 3% 0.7361 0.972428 0.02287592153
2 63.2 25 0% 0.7513 0.9815024 0
3 58 25 0% 0.7561 0.984206 0
4 57 25 0% 0.757 0.984689 0
5 72 25 5% 0.743 0.976614 0.03850007042
6 60.7 25 3% 0.7537 0.9828599 0.02316736181
7 58.2 25 8% 0.7559 0.9841094 0.0626099645
rata-rata 64.01 25.00 3% 0.75 0.98 0.02
Data Fraksi
xF 0.1267444934987
xD 0.43172
xW 0.02
100 0 0
98.1 0.02 0.192
95.2 0.05 0.377
100
91.8 0.1 0.527f(x) = 153.044 x⁶ − 514.466 x⁵ + 757.069 x⁴ − 642.576 x³ + 335.768 x² − 110.597 x + 100.056
87.3 0.2 0.656R² = 0.99995694188497
84.7 0.3 95
0.713
83.2 0.4 0.746
82 0.5 0.771
90
81 0.6 0.794
y
80
90
y
85
79.1 0.8 0.858
78.3 0.9 0.912
80
78.2 0.94 0.942 Tb,F 90.306778 C
78.1 0.96 0.959
75
Taverage 88.08196 C
78.2 0.98 0.978 0 0.1 0.2 pengecekan
0.3 0.4 0.5 Point
T boiling 0.6 0.7 0.8 0.9 1
78.3 1 1 x xy
0.1267444934987 0
cp( kJ/kg.C) 0.1267444934987 88.08196
etanol 3.29
air 4.21
cp campur 4.0933950659812 entalpy mixture (Kj/kg)
xF HL Hv
0.1 285.9 1870
0.1267444934987 278.54526 1782.81295119
0.2 258.4 1544
lamda 1504.2677 kj/kg mixture
q 1.0121083
slope 83.588027
𝑞=1+(𝑐𝑝 𝑐𝑎𝑚𝑝𝑢𝑟𝑎𝑛
(𝑇𝐵−𝑇𝐹))/𝜆𝑐𝑎𝑚𝑝𝑢𝑟𝑎𝑛 garis xF
garis xD
garis xW
garis q
1
f(x) = − 47.78752 x⁶ + 165.19 x⁵ − 223.28 x⁴ + 150.0191 x³ − 52.55603 x² + 9.406291 x
0.9 R² = 0.999748713204906
0.8
0.7
0.6
Axis Title
mencari stage
x y Nteoritis 1.8564146263184
0.43172 0.43172 Nactual 12
0.066186 0.4317578796836 E0 15.470121885987 %
0.066186 0.1173557224042
0.01345 0.117362442329
0.01345 0.0048841370853
wrate (L/h) %etanol (v/v) Reflux Ratio
B F D B L D
25 15% 47% 3% 30 20
25 21% 50% 0% 30 20
25 15% 52% 0% 30 20
25 12% 51% 0% 30 20
25 17% 50% 5% 30 20
25 17% 50% 3% 30 20
25 16% 51% 8% 30 20
25 19% 58% 0% 30 20
25 19% 60% 0% 30 20
25 25% 60% 0% 30 20
25 23% 65% 3% 30 20
68 x² − 110.597 x + 100.056
7 0.8 0.9 1
x y
0.126744 0
0.126744 0.1267444935
0.43172 0
0.43172 0.43172
0.02 0
0.02 0.02
0.126744 0.1267444935 slope
0.132529 0.6103383327 83.59996
Mencari λ campuran
Enthalpy Etanol Tb 78,3 °C Enthalpy air pada Tb 100 °C
Hv 1064 Hv 2676.1
HL 207 HL 419.04
λ 857 λ 2257.06
𝜆 𝑐𝑎𝑚𝑝𝑢𝑟𝑎𝑛= 𝑥_𝑒𝑡𝑎𝑛𝑜𝑙×𝜆_𝑒𝑡𝑎𝑛𝑜𝑙+𝑥_𝑎𝑖𝑟×𝜆_𝑎𝑖𝑟
λ Campuran = 2010.57917182
Mencari q
𝑞=1+(𝐶_𝑝 𝑐𝑎𝑚𝑝𝑢𝑟𝑎𝑛(𝑇_𝐵−𝑇_𝐹))/("λ" 𝑐𝑎𝑚𝑝𝑢𝑟𝑎𝑛)
q 1.0165524978
yn+1 = q XF R = L/D =
x -
q-1 q-1 XD
yn+1 =
yn+1 = 1.0165524978 0.17605018941
x -
0.0165524978 0.0165524978
yn+1 =
yn+1 = 61.4138428023 x - 10.6358684682
Enriching
yn+1 = 0.6 xn + 0.21850090206
XD Y
0.546252255 0.54625225514
0.3 0.39850090206
0.2 0.33850090206
0.178485175 0.32559200701
q line
yn+1 = 61.4138428023 x - 10.6358684682
XF Y
0.176050189 0.17605018941
0.178485175 0.32559200701
0.188 0.90993397865
XW y
0.005754655 0.0057546553
0.178485175 0.32559200701
Steam Consumption
X
Polynomial (X)
Y
Logarithmic (Y)
Polynomial (Y)
boiling point
boiling point 2
x, y
boiling point
x y
0 88.08753345866
0.17605018941 88.08753345866
1.5
0.47835891369
R XD
xn +
R+1 R+1
1.5 0.54625225514
xn +
2.5 2.5
0.6 xn + 0.21850090206
0.6
0.21850090206
1
f(x) = − 42.5916391481901 x⁶ + 148.067657094717 x⁵ − 201.548185563782 x⁴ + 136.757525728078 x³ − 48.61432474061
R² = 0.998540909123525
0.8
0.7
0.6
0.4
0.2
0.1
0
0 0.1 0.2 0.3 0.4 0.5
Jumlah plate
x y Tray teoritis
0.54625225514 0.546252255 Tray actual
ran 0.10239713192 0.546220329 Efisiensi tray
0.10239713192 0.184708769
ran 0.02100443612 0.184706475
0.02100443612 0.033993914
ran 0.00186746115 0.034359412
0.00186746115 -0.00144202
Menghitung steam consumption
𝑚𝑠=(𝑉𝑏𝑎𝑟 × ƛ)/ƛ𝑠
𝑉 𝑏𝑎𝑟=𝑉−(1−𝑞)𝐹
𝑉=(𝑅+1)𝐷
R 1.5
q 1.016552497799
D 43.26444403063 kg/h
F 61.97587147589 kg/h
ƛ 2044.039172804 kJ/kg
ƛs 2257.06 kJ/kg
Mencari V
V= 108.1611100766
Mencari V bar
V bar = 109.1869655527
Menghitung ms
ms = 109.1869655527 × 2044.039173
2257.06
ms = 98.88192371908 kg/h
tung water cosumption
ƛ)/((𝑇2−𝑇1)𝐶𝑝)
)𝐷
1.5
43.2644440306 kg/h
108.161110077
108.161110077 × 1515.06850921
8.14 × 4.182
4813.87682903 kg/h
%Etanol m/m
Feed Distilate Bottom
ρ air ρ etanol F ρ air ρ etanol D ρ air ρ etanol B
0.9937592 0.775828 0.1210882 0.9942394 0.777046 0.4093573 0.9890732 0.765388 0.0233739
0.9935191 0.775219 0.1717844 0.995337 0.77983 0.4392995 0.9880217 0.76321 0
0.9928674 0.773566 0.1208732 0.9930732 0.774088 0.4578314 0.9840611 0.75583 0
0.9955085 0.780265 0.0965596 0.9919574 0.771391 0.4473263 0.9828056 0.753548 0
0.9937935 0.775915 0.1378678 0.9900764 0.767476 0.4366732 0.9815567 0.751386 0.0387293
0.9927302 0.773218 0.1375814 0.9927988 0.773392 0.437887 0.9749994 0.740294 0.022944
0.9934162 0.774958 0.1293668 0.9942394 0.777046 0.4485643 0.9817196 0.751668 0.0624234
0.9934848 0.775132 0.1547011 0.990578 0.76852 0.517231 0.97781 0.7449 0
0.9927302 0.773218 0.1544773 0.989742 0.76678 0.5374847 0.9687148 0.73006 0
0.99225 0.772 0.2059353 0.9937249 0.775741 0.5393742 0.974222 0.73902 0
0.9937249 0.775741 0.1890871 0.9920828 0.771652 0.5909191 0.97781 0.7449 0.0230186
Equilibrium
Polynomial (Equilibriu
x=y
Linear (x=y)
XF
XD
XW
q line
Linear (q line)
Enriching
Linear (Enriching)
Stripping
Linear (Stripping)
Trays
2.7968752
12
23.307%
Plate actual 12
Feed plate 4
Waktu sampling 10 menit
Laju alir steam 100 L/jam
Interpolasi densitas
T (°C) ρ air ρ ethanol
30 0.99568 0.7807
40 0.99225 0.772
50 0.98807 0.7633
60 0.98324 0.7543
70 0.97781 0.7449
80 0.97183 0.7351
90 0.96534 0.7246
1000
1000000
Equilibrium
Polynomial (Equilibrium)
x=y
Linear (x=y)
XF
XD
XW
q line
Linear (q line)
Enriching
Linear (Enriching)
Stripping
Linear (Stripping)
Trays
No T (menit) T hot (⁰C) T cold (⁰C)
in out in
1 0 79 30.6 26.8
2 10 63.2 35.3 27.7
3 20 58 30.9 27.8
4 30 57 31.2 28.8
5 40 72 32.8 29.5
6 50 60.7 31.6 30
7 65 58.2 38.4 30.3
8 80 62.9 33.4 29.8
9 95 58.9 33.4 30.8
10 110 65 34 30.6
11 125 67.5 33.5 29.6
12 140 74.4 30 30
KONDISI 2 65.74 32.86 30.16
Fluida dingin
T in 30.16 °C
T out 32.68 °C
∆T 2.52 °C
Tav 31.42 °C
Flowrate 600 L/h
Densitas air
T densitas
30 996.68 kg/m3
31.42 996.05094 kg/m3
0.99605094 kg/L
40 992.25 kg/m3
Cp air
T Cp
30 4.181 kJ
31.42 4.181
40 4.181
q m ∙ Cp ∙ ∆T
6321.672
T cold (⁰C) Flowrate (L/h)
out hot cold
29 25 600
34.2 25 600
30.1 25 600
34.2 25 600
31.8 25 600
32 25 600
32 25 600
31.8 25 600
32.4 25 600
32.7 25 600
34.8 25 600
31.7 25 600
32.68 25 600
Fluida panas
T in 65.74
T out 32.86
∆T 32.88
Tav 49.3
% v/v bottom 1%
XW 0.015499
NO t (menit) T hot (⁰C) T cold (⁰C) Flowrate (L/h)
in out in out hot cold
1 0 120.1 93 54 88.2 100 22
2 10 121.1 95 56 90 100 22
3 20 120.4 92 58 88.2 100 22
4 30 122 95 56.7 90.4 100 22
5 40 120.6 92 59 89.9 100 22
6 50 119.6 94 66.8 90.3 110 22
7 65 119.1 92 84 88.6 95 22
8 80 119.5 95 85.5 89.6 98 22
9 95 128.8 94 86.9 90.8 110 22
10 110 118.7 95 88.6 91.2 130 20
11 125 118.7 92 56.5 91.3 100 20
12 140 118.1 92 83.3 87.1 100 22
NO t (menit) T Hot (⁰C) T Cold (⁰C) Flowrate (L/h)
in out in out hot cold
1 0 80.9 51.3 25.2 33.4 25.2 2
2 10 82 56.6 26.6 37.6 25.2 2
3 20 84.6 47.9 26.4 36.1 25.2 2
4 30 83.3 55.4 29.6 37.7 25.2 2
5 40 81.9 46.1 28.3 36.1 25.2 2
6 50 82.3 52.7 28.7 38.8 25.2 2
7 65 79.6 42.2 29.3 35.3 25.2 2
8 80 78.5 44.3 29.5 35.6 25.2 2
9 95 80.5 53.2 29.1 39.2 25.2 2
10 110 82.4 53.2 29.5 41 25.2 2
11 125 77.8 48 29.6 36.6 25.2 2
12 140 70.4 48 29.7 35.7 25.2 2
1 0
2 10
3 20
4 30
5 40
6 50
7 65
8 80
9 95
10 110
11 125
12 140
Average
Fluida Panas
T in 100 ˚C Densitas Etanol
T out 71.95 ˚C 159.05 19.413
ΔT 28.05 ˚C 359.125 11.83104
T average 85.975 ˚C 513.92 5.965
flowrate fluida panas 1.164 L/h
fraksi volume feed etanol 0.1614286 Cp air
fraksi massa feed etanol 0.1267445 80 4.199
11.831044 kmol/m3 85.975 4.204378
densitas etanol pada T avg
0.544228 kg/L 90 4.208
densitas air pada T avg 0.9679522 kg/L
densitas campuran 0.899551 kg/L q Fluida dingin
0.8 cal/g ˚C q fluida panas
cp etanol pada T avg
3.34944 kJ/kg K q average
cp air pada T avg 4.2043775 kJ/kg K
cp campuran 4.0960189 kJ/kg K
m fluida dingin 1.0470774 kg/h ΔT1
λ 2230.0608 kJ/kg ΔT2
ΔTLMTD
A
U
T hot (⁰C) T cold (⁰C) Flowrate (L/h)
hot hot
In out in out cold
(mL/s) (L/s)
100 72.6 46.2 85 23.6 75 1.416
100 77.3 43.5 85.3 12.4 75 0.744
100 71.7 50.9 87 24 75 1.44
100 53 36.6 82.4 19.8 75 1.188
100 76 45 85.3 23 75 1.38
100 78 37.3 86.7 20.2 75 1.212
100 68 37.1 89.3 16 75 0.96
100 79 39.9 89.1 16.2 75 0.972
100 76 44.8 77.1 25.8 65 1.548
100 80 38.5 86.2 27.8 65 1.668
100 77 42.5 72.5 22 65 1.32
100 68.8 48.8 74.4 10 65 0.6
100 71.95 42.0625 86.2625 19.4 75 1.164
100 75.45 43.65 77.55 21.4 65 1.284
Fluida Panas
Densitas air T in 100
80 0.97183 T out 75.45
85.975 0.96795223 ΔT 24.55
90 0.96534 T average 87.725
flowrate fluida panas 1.284
fraksi volume feed etanol 0.161429
fraksi massa feed etanol 0.126744
11.76473
densitas etanol pada T avg
0.541177
densitas air pada T avg 0.966816
165781 kJ/h densitas campuran 0.898106
2455.348 kJ/h 0.8
cp etanol pada T avg
84118.35 kJ/h 3.34944
cp air pada T avg 4.205953
cp campuran 4.097394
286.8875 K m fluida dingin 1.153168
303.0375 K λ 2230.061
294.8888 K
0.5 m2
570.509 kJ/h.m2.K
ate 65 L/h)
˚C Densitas Etanol Densitas air
˚C 159.05 19.413 60 0.9832
˚C 333.75 12.79264 60.6 0.983062
˚C 513.92 5.965 70 0.9809
L/h
Cp air
60 4.187
kmol/m3 60.6 4.1873
kg/L 70 4.192
kg/L
kg/L
cal/g ˚C
kJ/kg K
kJ/kg K
kJ/kg K
kg/h
kJ/kg
as
˚C Densitas Etanol Densitas air
˚C 159.05 19.413 80 0.97183
˚C 360.875 11.76473 87.725 0.966816475
˚C 513.92 5.965 90 0.96534
L/h
Cp air
80 4.199
kmol/m3 87.725 4.205953
kg/L 90 4.208
kg/L
kg/L q Fluida dingin 141451 kJ/h
cal/g ˚C q fluida panas 2687.634 kJ/h
kJ/kg K q average 72069.11 kJ/h
kJ/kg K
kJ/kg K
kg/h ΔT1 295.6 K
kJ/kg ΔT2 304.95 K
ΔTLMTD 300.2507 K
A 0.5 m2
U 480.0595 kJ/h.m2.K