Tunable Diode Laser Spectrometer: Tdls Gpro 500
Tunable Diode Laser Spectrometer: Tdls Gpro 500
TABLE OF CONTENT
1 Introduction............................................................................................................................5
1.1 Safety information............................................................................................................5
Laser Spectrometer GPro 500
1.2 Symbols.........................................................................................................................5
1.3 Purpose..........................................................................................................................5
1.4 Qualified personnel..........................................................................................................5
1.4.1 Transport, storage and handling..............................................................................5
1.5 Additional documentation.................................................................................................6
1.6 General...........................................................................................................................6
1.7 Proper use of the product..................................................................................................7
1.7.1 Measuring principle...............................................................................................7
1.7.2 Instrument description............................................................................................8
1.7.3 Software...............................................................................................................8
1.7.4 System overview...................................................................................................8
4 Operation..............................................................................................................................22
4.1 Instrument start-up.........................................................................................................22
4.2 Instrument shut-down....................................................................................................22
4.3 Fault indication..............................................................................................................22
5 Maintenance.........................................................................................................................24
5.1 Routine maintenance...................................................................................................... 24
2
Contents Next Page Previous Page Print Close
7 Troubleshooting....................................................................................................................33
8.1 SIL Parameters..............................................................................................................33
8.1.1 Covered types of GPro 500...................................................................................33
8.1.2 SIL parameters....................................................................................................33
8.2 Compliance and Standards Information............................................................................33
8.3 Labels..........................................................................................................................34
8.3.1 Type labels.........................................................................................................34
8.3.2 Additional labels..................................................................................................35
3
Contents Next Page Previous Page Print Close
FIGURES
Figure 1. General setup GPro 500.......................................................................................................9
Figure 8. Menu for configuring the pressure and temperature compensation using external sensors........ 19
Disclaimer of Liability
To ensure consistency with the hardware and software described the contents of this publication have been
reviewed carefully. However, since variance cannot be excluded entirely we cannot guarantee full consistency.
GPro is a registered trademark of the METTLER TOLEDO group in Switzerland, USA, Germany and France.
4
Contents Next Page Previous Page Print Close
1 Introduction
1.1 Safety information
Read this manual and ensure that you fully understand its content before you attempt to install, operate
or maintain the GPro 500® used in a safety integrated (SIL) environment.
1.2 Symbols
Pay particular attention to all special information and warnings. This type of information is marked with
the corresponding pictograms. To observe these notices will ensure your personal safety and prevent
damage of property:
WARNING
Warnings highlight specific hazards which, if not taken
into account, may result in personal injury or death.
CAUTION
Cautions highlight hazards which, if not taken into account,
can result in damage to the TDL or to other equipment or property.
This manual incorporates also “be aware” information, which is used as follows:
hhThis highlights information which is useful for you to pay attention, for example specific opera-
tion conditions.
1.3 Purpose
This document contains information and safety instructions required to use the GPro 500 with direct
analog output option (GPro 500 XXXXXXXXXXXXXXXX _ _ / _A in SIL environments.
The manual is intended for personnel responsible for planning, installation, commissioning, service and
maintenance.
5
Contents Next Page Previous Page Print Close
hhPlease study the entire documentation carefully before installing or using the GPro 500. It is a
sophisticated instrument utilizing state-of-the-art electronic and laser technology. Installation,
operation and maintenance of the instrument require care and preparation and should only be
attempted by competent /qualified personnel. Failure to do so may damage the instrument and
void the warranty.
CAUTION
METTLER TOLEDO strongly recommends having the final installation and commissioning
executed under the full supervision of a METTLER TOLEDO representative.
Do not power up the system before the wiring has been fully checked by trained personal.
It is strongly recommended to have the wiring approved by
a METTLER TOLEDO Service representative.
Wrong wiring can lead to damage of the sensor head and /or the M400 transmitter.
1.6 General
The GPro 500 designed for continuous in situ monitoring of gases in stacks, pipes, ducts, extractive
measurement cells etc. and it is based on tunable diode laser technology. The GPro 500 utilizes a single
side installation (probe-type TDL) without the need for alignment to measure the average gas concentra-
tion along the line-of-sight path in the probe.
The GPro 500 can be considered to be a Type B element acc. to IEC 61508:2010.
The gas concentration is provided to the DCS as linear analog signal (4 – 20 mA, NAMUR). 4 mA indicate
low level, 20 mA indicate high level. The analog values for instrument errors can be parameterized within
the NAMUR settings.
6
Contents Next Page Previous Page Print Close
Component Process gas temperature (°C) Process gas pressure (mbar abs. ⁄⁄ psia)
O2 0 … 600 0.3 … 8 // 4.35 … 116.03
O2 & spectral temperature 0 … 150 0.8 … 5 // 11.63 … 72.52
CO (ppm) 0.8 … 2 // 11.63 … 29.00
CO (%) 0.8 … 1.5 // 11.63 … 21.75
CO2 (%) 0.8 … 2 // 11.63 … 29.00
CO2 & CO 0.8 … 2 // 11.63 … 29.00
H2O 0 … 600 0.8 … 2 // 11.63 … 29.00
HCl 0.8 … 3 // 11.63 … 43.50
H2S 0.8 … 2 // 11.63 … 29.00
CH4 0.8 … 3 // 11.63 … 43.50
NH3 0.8 … 3 // 11.63 … 43.50
WARNING
The GPro 500 may only be used for applications described
in the catalogue and approved by METTLER TOLEDO.
CAUTION
The approval might contain limitations which differ from the conditions
provided in the table above. These limitations have to be followed.
7
Contents Next Page Previous Page Print Close
• junction box
• optional M400 transmitter (user interface; see remark below).
CAUTION
When the analog outputs of the M400 are used and /or when the GPro 500
is configured or operated via the M400 the SIL compliance is no longer valid.
External pressure and temperature measurements must be available; depending on the application, am-
bient conditions and process adaption additional purge gas (in general N2, 99.7) might be necessary.
1.7.3 Software
The software of the GPro 500 consists of 2 programs:
• The firmware of the GPro 500 (not visible to the user) which is integrated in the CPU electronics. It
performs all necessary calculations and self-monitoring tasks.
• The MT-TDL Suite which is a Windows based program. It runs on a standard PC connected to the
GPro 500 through the Ethernet connection. It enables communication and parameterization of the
GPro 500 during installation, normal operation, calibration and service. For a detailed description
please refer to chapter 6 of the Operating Instructions TDLS GPro 500.
8
Contents Next Page Previous Page Print Close
P
5
T
4
6 1 2 3
WARNING
When connecting the external power supply to the junction box,
do not exceed the 24 VDC, max. 60 W limit!
WARNING
When connecting the external analog inputs for pressure and temperature
compensation make sure that the complete system is switched off!
9
Contents Next Page Previous Page Print Close
hhFurther details and valuable information are provided in the GPro 500 Series Pre-Installation
Laser Spectrometer GPro 500
Requirements
hhNote: For complete information regarding the installation please refer to GPro 500 Series Pre-
Installation Requirements, the GPro 500 Quick Setup Guide, and to Operating Instructions
TDLS GPro 500.
WARNING
Ensure that neither the GPro 500 nor the external pressure and temperature
sensors are energized when connecting them to the junction box.
Do not open the junction box in an explosive
atmosphere when the GPro 500 is energized.
hhIf the analog outputs of the external sensors are set properly with respect to out-of-range and
failure signals the GPro 500 is able to detect both.
• External analog signals between 3.6 … 3.8 mA and 20.0 … 20.5 mA are considered as out of range
of the external sensors
• External analog signal is considered as failure signal when it is either below 3.8 mA or above 20.5 mA
• In case of failure signal the GPro 500 will also change to the failure state and the reading is set by the
software to 110 %
• Please note: the GPro 500 is not able to detect measurement errors of the external sensors by us-
ing higher diagnosis function. As long as the external analog signal is between 4 and 20 mA the
GPro 500 will assume well working external sensors
2.2 Preparations
• You will find a detailed information in chapters 2.1 to 2.4 of the Operating Instructions TDLS GPro 500
WARNING
Do not forget to ground the GPro 500
10
Contents Next Page Previous Page Print Close
hhFor efficient installation you must make sure that the pre-installation requirements are met prior
to the visit of the METTLER TOLEDO technician.
hhIf the process is running it is recommended for purged probes to connect and turn on the purging
at maximum flow before inserting the probe into the process. This is to avoid instant contamina-
tion of the optics.
WARNING
Do not use FORCE when you assemble the spectrometer and the process
adaption. The head will slot into the process adaption at the right angle.
The mechanical tolerance of the parts is very small, using force will damage
the interface resulting in alignmen issues and loss in transmission!
Also ensure that the gasket is in place.
11
Contents Next Page Previous Page Print Close
2.3.3 Purging
Depending on the configuration supplied there may be requirement for either one or two optical purges
(instrument and process purge).
Standard purged probe SP Blow-back probe with filter BB
Laser Spectrometer GPro 500
Instrument purge
The GPro 500 TDL head attaches to the process adaption via a precision mechanical interface. Between
the optical window of the TDL and the process window of the process adaption is a cavity. This cavity
is part of the optical path of the analyzer and therefore it is important that there are no traces of the gas
to be measured, i.e. O2 or H2O or other, in this space. Otherwise it will add to the measurement signal
leading to a wrong reading. The instrument purge is to flush this space.
For O2 measurement this is normally nitrogen is used and for other measurements instrument grade air is
recommended.
Typical purge gas flow for instrument purge is < 1 L /min.
hhProcess purge is critical for the protection of the wetted optical components and for correct
operation of the analyzer. Therefore, it must be running all the times! A no-flow alarm switch is
recommended to this purpose.
For oxygen applications nitrogen purge is required or alternatively another clean, non-explosive, non-
corrosive, dry and O2 free gas. For other measurements, instrument grade air is normally recommended.
The GPro 500 SP and W process adaption are designed to consume as little purge gas as possible while
keeping the optical surfaces protected and clean.
Alternatively, gas cylinders may be used to ensure proper purging of the probes.
12
Contents Next Page Previous Page Print Close
WARNING
The process purge gas inlet must have a check valve to avoid
contamination of the purging system from process gas.
Always start process purging at maximum before inserting
the probe or before starting the process.
Process purge gas must always run in order to avoid contamination
of the optical surfaces and ensure protection of the optical surfaces.
Do not remove and / or disassemble the process purge gas
inlet otherwise the PED pressure certificate is void.
Do not connect the instrument and process purge in series, otherwise
when disassembling the sensor head the process purging will stop.
For further details, please refer to chapter 3 of the Operating Instructions TDLS GPro 500.
CAUTION
If the process flow rate remains constant this will be a good purge flow but the effective
path length will always be a function of the process flow rate so be observant on this.
2
Inecreased reading
1 4
On the x-axis there is purge flow and on the y-axis there is the instrument concentration reading.
1 Concentration reading with high purge flow. The path length is now shorter than the effective
path length since the purge tubes is completely filled with purging gas and some of the purging
gas is flowing into the measurement path.
2 Concentration reading with optimized purge flow. The path length is now equal to the effective
path length since the purge tubes are completely filled with purge gas. See the illustration below.
3 Concentration reading with no purge flow. The path length is now equal to the nominal path
length since the probe is completely filled with process gas.
4 The optimized purge flow.
13
Contents Next Page Previous Page Print Close
14
Contents Next Page Previous Page Print Close
Transmission and
NSL for signal
optimization
15
Contents Next Page Previous Page Print Close
to pin 13 … 16 of the junction box with a common available Ethernet cable. Depending on the type of
Ethernet cable (T568A or T568B) the wiring is as below:
• T568A Ethernet cable
-- White /green goes to 13
-- Green solid goes to 14
-- White /orange goes to 15
-- Orange solid goes to 16
• T568B Ethernet cable
-- White /orange goes to 13
-- Orange solid goes to 14
-- White /green goes to 15
-- Green solid goes to 16
After start of the MT-TDL Suite the connection between the GPro 500 and the PC is established automati-
cally.
16
Contents Next Page Previous Page Print Close
1
11 10
2 3
4
5
6
18
12
13
14
15
16
17
20 21 19
17
Contents Next Page Previous Page Print Close
18
Contents Next Page Previous Page Print Close
Figure 8. Menu for configuring the pressure and temperature compensation using external sensors
1 Switch to the “external in” tab
2 Enter the start and end value of the pressure / temperature sensor in the respective field
3 Transmit the settings using the “Flash Settings” button
hhIf the settings are correct and the wiring between the analog outputs of the sensors and the junc-
tion box is correct the actual readings for pressure and sensor are shown in 17 and 18
hhThe trend of the external readings is shown in the graph in the “external in” tab
19
Contents Next Page Previous Page Print Close
hhThe accuracy of the temperature measurement also influences the reading of the GPro 500.
hhAs a rule of thumb an error or 1 °C in the temperature signal will lead to an error of 0.25 % of
reading
hhIn case of failure and /or disconnection of the pressure and /or temperature sensor, the analog
output of the GPro 500 will switch into the alarm / failure state.
hhPlease note the GPro 500 is not able to detect measurement errors of the external sensors by
using higher diagnosis function. As long as the external analog signal is between 4 and 20 mA
the GPro 500 will assume well working external sensors.
The best readings are achieved when the correct process pressure and temperature is provided via
correct working external sensors. However, for processes which run on stable or nearly stable pressure
and /or temperature using fixed pressure and /or temperature may be the better choice. Whether the
measurement will work without pressure and /or temperature sensor has to be discussed during the
evaluation of your application.
hhThe optical path length influences directly the reading of the GPro 500. The setting of the ad-
equate OPL has a direct impact on the accuracy of the measurement value.
21
Contents Next Page Previous Page Print Close
4 Operation
4.1 Instrument start-up
Assumed that the TDL is connected correctly via the junction box to the power supply it will power up
Laser Spectrometer GPro 500
automatically when the power is switched on. The start-up time is approximately 1 min.
WARNING
To not interrupt the process purge as long as the process
is running and the probe is in the process!
hhIt is important that the receiving device (in general the DCS) is able to detect and interpret the
fault situation to comply with the safety function.
Fault messages are also indicated at the simulation window (upper half) of the MT-TDL suite.
22
Contents Next Page Previous Page Print Close
hhMonitoring the transmission of the GPro 500 via the 2 ndanalog output gives always complete
information about the cleanliness of the optical surfaces of the GPro 500. Furthermore, if the
transmission starts to drop a maintenance /service intervention can be planned.
For troubleshooting of all fault situations please refer to chapter 9 of the Operating Instructions TDLS
GPro 500.
23
Contents Next Page Previous Page Print Close
5 Maintenance
The GPro 500 is designed to reduce maintenance to a minimum. Experience has shown that mainte-
nance intervals of more than 12 months are acceptable for most applications. The maintenance opera-
tions described below will secure continuous and safe operation of the instrument.
Laser Spectrometer GPro 500
24
Contents Next Page Previous Page Print Close
hhIf your GPro 500 measures CO ppm level please contact your supplier about the correct configu-
ration of the calibration tube.
hhDepending on site regulations and for your personal safety it is recommended to use your per-
sonal protective equipment (PPE)
6.2 Calibration
Depending on the configuration of the GPro 500 (for example with in situ probe installed, with in situ
probe installed in a by-pass, with a blow-back probe or extractive probe) the verification process may
differ slightly
25
Contents Next Page Previous Page Print Close
If you are only performing a simple calibration, observe the values of the reading and record it for docu-
mentation and certification purposes.
For documentation in MT-TDL Suite you can also follow the calibration procedure described in section 6.3
Laser Spectrometer GPro 500
but activate “calibrate” instead of “adjust”. The calibration factor is stored in the calibration history but not
used for measurement.
If the reading shows more than 2 % error or when an adjustment is requested follow the calibration
procedure described below.
WARNING
Do not interrupt the process purge as long as the process is
running and the process adaption is in the process!
26
Contents Next Page Previous Page Print Close
WARNING
Do not interrupt the process purge as long as the process is
running and the process adaption is in the process!
Blow-back filter process adaptions are especially good at coping with process gases that contain par-
ticularly high levels of dust or liquids. It is also possible to fill the protected inner volume of the filter with
a calibration gas:
• Connect the calibration gas bottle via a pressure reducer and a flow regulator to the blow-back inlet of
the process adaption.
• Adjust the pressure to be slightly above the process gas pressure
• Adjust the flow regulator to a flow between 1 and 10 l/h
• If you are using corrosive or toxic gases for the calibration process carry out a leak test following your
site regulations
• Connect your computer/laptop to the junction box and start MT-TDL Suite
• Open the calibration gas bottle and flush the filter with calibration gas.
• Observe the reading of the TDL (ppm-trend tab) and wait until the signal is stable
• If the signal does not stabilize enhance the pressure of the calibration gas.
WARNING
During the calibration/adjustment using the blow-back inlet the calibration
gas flows freely into the process and mixes with the process gas.
If this is not possible choose another suited
calibration method as described above.
If you are only performing a simple calibration, observe the values of the reading and record it for docu-
mentation and certification purposes.
We highly recommend a flow monitoring alarm switch at the process purge inlet to detect blocking of
the filter by dust.
27
Contents Next Page Previous Page Print Close
For documentation in MT-TDL Suite you can also follow the calibration procedure described in section
6.3 but activate “calibrate” instead of “adjust”. The calibration factor is stored in the calibration history
but not used for measurement.
If the reading shows more than 2 % error or when an adjustment is requested follow the adjustment
Laser Spectrometer GPro 500
hhThe quality of the calibration depends on the quality of the setting for the new opl!
If you are only performing a simple verification, observe the values of the reading and record it for docu-
mentation and certification purposes.
For documentation in MT-TDL Suite you can also follow the calibration procedure described in section
6.3 but activate “calibrate” instead of “adjust”. The calibration factor is stored in the calibration history
but not used for measurement.
If the reading shows more than 2 % error or when an adjustment is requested follow the adjustment
procedure described in section 6.3.
WARNING
Before you open the sample gas path of the extractive system check
whether there can be back pressure from the exhaust line.
If this is the case the connection between the exhaust line and the sample
gas outlet of the extractive cell need to be closed by a suited valve
28
Contents Next Page Previous Page Print Close
If you are only performing a simple verification, observe the values of the reading and record it for docu-
mentation and certification purposes.
For documentation in MT-TDL Suite you can also follow the calibration procedure described in section
6.3 but activate “calibrate” instead of “adjust”. The calibration factor is stored in the calibration history
but not used for measurement.
If the reading shows more than 2 % error or when an adjustment is requested follow the adjustment
procedure described in section 6.3.
Calibration modes
One-point-calibration: Calibration with a certified calibration gas
Process calibration: Process gas is used as calibration gas. For this calibration method it is nec-
essary to obtain the concentration of the measurement gas by a 2nd analyzer.
Please note that the quality of the calibration depends strongly on the quality
of the concentration value.
Both are slope calibrations.
“cal type” allows to switch between both modes
29
Contents Next Page Previous Page Print Close
30
Contents Next Page Previous Page Print Close
hhIf the calibration fails please contact your supplier or the METTLER TOLEDO support.
hhRegardless whether the GPro 500 is validated or calibrated we strongly recommend to measure
the analog value of the analyzer by use of a suited multimeter and check whether the expected
value in shown in the DCS.
31
Contents Next Page Previous Page Print Close
32
Contents Next Page Previous Page Print Close
7 Troubleshooting
All information about the maintenance and error messages are given in chapter 9 of the Operating In-
structions TDLS GPro 500. There you find also some recommendations about the actions to be taken.
33
Contents Next Page Previous Page Print Close
8.3 Labels
8.3.1 Type labels
The spectrometer of the GPro 500 is marked with a product identification label:
Laser Spectrometer GPro 500
1 4
5
11
6
10
7
9
8
4
1
5
11 6
10
7
9
8
34
Contents Next Page Previous Page Print Close
Note labels
1/2" NPT
GAS GRP A: SEAL
REQUIRED AT
ENCLOSURE ENTRANCE
WARNING –
WAIT 2 MIN. BEFORE
OPENING AFTER
DE-ENERGIZING
Figure 17. Note label
Grounding labels
M6x12
M4x6
35
Competence Center
The Latest News on Applications and Products
Visit us online to discover white papers, application notes, how-to videos and
our list of upcoming webinars.
www.mt.com/o2-gas
www.mt.com
For more information