©,Metrohm METROHM Ltd. CH-9101 Herisau (Switzerland)
712 Conductometer
5.712.0012 program
Mains connection:
Mains voltage U_ = 100... 120 V, 220 ... 240 V (+ 10%)
Mains frequency f = 50... 60 Hz
Power consumption S$ = 13VA
8.712.1003 Instructions for Use
07.10.1994 / dé QMetrohn I
Table of contents
Page
1. Introduction ......... 0... eee eens 1
2. Parts and controls ................ 6... eeeeeeee ence eens 2
3. Installation Bee eee eee eee eee 4
3.1. Setting up the instrument 4
3.2 Mounting the accessory for holding the sensors .. 4
3.3 Mains connection and switching on the instrument . 5
3.3.1. Setting the instrument supply voltage 5
3.3.2 Fuse ; teeeeee 5
3.3.3 Mains cable and mains connection 5
3.3.4 On/off switching of the instrument 5
3.4 Attachment of sensors .. 6
3.5 Attachment of devices to the analogue output 8
3.5.1 Details of the analogue outputs 8
3.5.2 Attachment of a recorder 8
3.5.3. Attachment to 536 Potentiograph 9
3.5.4 Attachment to Titrinos 9
3.6 Attachment of devices to the RS232 interface 10
3.6.1 Attachment of a computer 10
3.6.2 Attachment of a printer . 10
3.7 Attachment of devices to the remote interface 13
3.7.1 Details of the remote interface 13
3.7.2 Attachment of a sample changer 13
4. Manual operation ee ee 14
4.1 Introduction to operation by means of examples 14
41.1 Basi istrument mode, main and auxiliary display ..... 14
4.1.2 Data entry beeen ee 15
4.1.3 Conductivity measurement 18
4.1.4 Temperature measurement 22
4.2 Fundamentals of operation 23
4.2.1. Main display wee eeeeeee bon
4.2.2. Overview of the key functions . . 23
4.2.3 Non-volatile main memory 25
4.2.4 Instrument dialogue 25
4.2.5 Text entry 25
4.3. Configuration,
key 27
8.712.103 Instructions for use
Table of contents 4.4 Conductivity measurement ........
44.1 General information on measuring the conductivity . 31
4.42 Parameters for conductivity measurement,
key 32
4.4.3 Calibration of the cell constant, ‘key .
4.4.4 Calibration of the temperature coefficient, key . 42
4.5 Temperature measurement 49
4.5.1 Selection of the main measurement mode, key 49
4.5.2 Parameters for temperature measurement,
key 50
4.6 Auto zero and compensation 54
46.1 General 54
46.2 key 55
46.3 key 56
46.4 key 57
4.6.5 key 58
4.7 Data output ... 60
4.7.1. Display of instrument data, key 60
47.2. Report output, key . 62
47.3. Measured value output and curve plot, Key... 65
5. Operation via RS232 interface Beene ee ere reer rer)
5.1 General rules .. 70
5.2 Call up of objects nm
5.3 Triggers 72
5.4 Status and errormessages .......... 02.0.0. 7B
5.4.1. Global status conditions 73
5.4.2 Delailed status conditions ............. peererS
5.4.3 Error messages ... 74
5.5 Remote control commands 76
5.6 Characteristics of the RS232 interface ...... ceceeeeeee 82
5.6.1 Data transfor protocol 82
5.6.2 Handshake . 83
5.6.3 Pin assignment .........6. 0.0. 0e cee ee eee e eee 87
5.7 What can you do if the data transfer does not work? ........... 89
6. Remote interface perce eee ereee ec oO)
6.1 Functions 90
6.2 Assignment of the programmable input lines ......... sees 90
6.3 Control inputs and outputs 93
Table of contents 8.712. 1003 Instructions for use QMetrohm m
Page
7. Safety, errors, maintenance, GLP, diagnostic test 95
71 Electrical safety Feed eee ee eee e eee 2 95
7.2. Error messages beet ete eteteeteeee es 95
7.3 Platinisation of conductivity cells 97
7.4 Standard operating procedure in the context
of GLP/SO 9001 guidelines .......... 00.0... ec ee 98
7.4.1 Accessories required ..... we . 98
7.4.2 Test of the 712 Conductometer with resistors. 98
7.43. Test of the 712 Conductometer with conductivity standard 99
7.5 Diagnostic test 2600... eee eee eee ee 101
7.6 Initialisation of the EEPROM memory ..............-..5- 109
8. Technical data ....... Se 8 |)
9. Standard equipment, options, warranty 114
9.1. Standard equipment of the 712 Conductometer 114
9.2 Optional accessories 115
9.2.1 Stirrers we w. 115
922 Conductivity cells and temperature sensors... 118
9.2.3 Measuring vessels ...............22205 .. 116
9.2.4 Conductivity standard 116
9.2.5 Connecting cables ........... seve . 116
9.2.6 VESUV 116
9.3 Warranty . .. WT
10. Index Se ee Seer eee eeeceee seve 118
8.712, 1003 Instructions for use Table of contents Iv .Metrohm
List of figures
Page
Front and rear of the 712 Conductometer ; 2
Attachment of sensors to the 712 Conductometer - 6
Conductivity measurement ranges as a function of the cell constant ..... 7
Analogue output circuitry of the 712 Conductometer .. 8
Attachment of recorders to the 712 Conductometer ........... 8
Attachment of the 712 Conductometer to the 536 Potentiograph 9
Attachment of the 712 Conductometer to Titrinos 9
Attachment of external devices to the RS232 interface ........ 10
Attachment of external devices to the remote interface 13
Attachment of the 712 Conductometer to the 664 Control Unit ......... 13
‘Schematic representation of rolling inquiries 26
Table of contents 8.712.1003 Instructions for use 1
Meth 1
Introduction
The 712 Conductometer is a modern conductivity measuring instrument with a
dynamic measurement range of 0 :S/cm... 2000 mS/cm, an autozero and a com-
pensation function. The measured conductivity is automatically converted to a
freely selectable reference value (usually 20°C or 25°C) using the specified or
experimentally determined temperature coefficient. Both the cell constant and the
temperature coefficient can be calibrated automatically. With the TDS (Total Dis-
solved Solids) function, the total conductivity can be expressed in terms of the
salt content (mg/L NaCl). In addition to the conductivity, measurement of the
temperature using a Pt100 or Pt1000 sensor is possible in the range -170
+500 °C.
Both the conductivity and the temperature have a freely configurable analogue
output available. Communication with a printer, a PC or other devices is possible
via remote control '/O lines and an RS232 interface.
These Instructions for Use provide a comprehensive overview of the parts and
controls, installation, operation, error rectification and technical data of the instru-
ment. The contents of the green pages are of interest to you only if you wish to
remote control your 712 Conductometer using the built-in RS232 or remote inter-
face. To find any particular information regarding the instrument, please consult
the Contents table or the Index at the back
For a rapid overview of the key functions and parameters, you have available
Shortform Instructions for Use affixed to the instrument and the 8.712.1023 Short
Operating Guide.
You will find additional information on measurement of the conductivity and the
measuring cells required in the following Metrohm documents:
© Application Bulletin No. 102 «Conductometry»
© Application Bulletin No. 64 «Platinisation of platinum
electrodes and conductivity measuring cells»
* Instruction sheet enclosed with all conductivity cells supplied
Brochure «Metrosensor electrodes»
Electrode catalogue
{8.712.109 Instructions for use Chap. 1 — Introduction 2. Parts and controls
sv bo-1209
ey 8y
ao
Fig. 1: Front and rear of the 712 Conductometer
Chap. 2 - Parts and controls 8.712.103 Instructions for uso &QMetrohm
In
le
la
lo
N
lo 1
ls
Main display (gas discharge display)
with measured value, unit and status display
Dialogue display (LCD)
comprising 2 lines, each of 24 characters
Keypad
with operating and numeric keys
Short-form Instructions for Use
6.2001.030 Stand Support
For fastening stand rod 6,
can be mounted on the ieft or the right (see section 3.2)
6.2016.050 Stand Rod
for holding 6.2013.010 Clamping Ring and 6.2021.020 Electrode Holder
Connection for conductivity cell (black sockets)
Connection for Pt100 or Pt1000 temperature sensor (red sockets)
Connection for platinisation of conductivity cells (green sockets)
Analogue output for conductivity
red socket: live
black socket: common
Analogue output for temperature
red socket: live
black socket: common
Mains voltage selector
115V: 100...120 V + 10%
230V: 220...240 V + 10%
Earthing socket
Earthing, see section 3.3.3
Mains switch
Switch for switching instrument on and off:
ON 0=OFF
The operational readiness is shown by displays 1 and 2 lighting up.
Mains connection plug
Cold appliance plug, type CEE(22), VI; mains connection, see section 3.3.3
Model plate with serial and manufacturing number
Remote interface
Remote 1/0 lines for the remote control of a sample changer or other
external devices
RS232 interface
RS232C interface for the attachment of a printer or a PC
8.712.103 Instructions for use Chap. 2 — Parts and controls QeMetrohm
Installation
This section describes the installation of the 712 Conductometer. Safe operation
of this instrument is assured only if you follow the instructions specified here ex-
actly. Bold, underlined numbers in the text (e.g. 15) refer to the parts and con-
trols numbered in the illustrations in section 2.
Set
g up the instrument
The 712 Conductometer is supplied together with the separately packed acces-
sories in an extremely well protected special package. This contains two shock-
absorbing foam linings. The instrument itself is packed in a dustproof, evacuated
polyethylene bag. It is advisable to keep this special packing since if for any rea-
son the instrument has to be returned only such packing guarantees indemnified
transport.
Immediately after receipt, a check must be made to ensure completeness of the
shipment and the absence of any damage (compare with delivery note and ac-
cessories list in Section 9). In the case of transport damage, see instructions in
Section 10, "Warranty".
The 712 Conductometer should be set up in the laboratory at a location free from
vibrations and suitable for the intended operation. It must be protected against
corrosive atmospheres and contamination by chemicals.
Mounting the accessory for holding the sensors
The accessory enclosed with the 712 Conductometer for holding the conductivity
cells and/or temperature sensors is mounted as follows:
1» Fasten stand rod 6 using the enclosed hex screw to stand
‘support 5.
2 Screw stand support 5 to the two screws on the underside of the
712 Conductometer using the enclosed washers and knurled
nuts. The stand support can be mounted so that the stand rod is
on the loft or the right of the instrument.
3> Fasten the 6.2013.010 Clamping Ring to stand rod 6 so that it
limits the lowest position of the electrode holder.
4» Fasten the 6.2021.020 Electrode Holder to stand rod 6. Press
the red lock button to shift it to any position you wish.
If you wish to stir the analysis solution, you can use the 728 Magnetic Swing-out
Stirrer (see section 9.2) available from Metrohm as an option. This stirrer can be
mounted directly on stand rod 6.
Chap. 3 Installation {8.712.1003 Instructions for use @.Metrohm 5
3.3
Mains connection and s\ hing on the instrument
3.3.1
Note: If the 712 Conductometer is connected to the power supply, the 712
Conductometer may be opened or parts removed as there is a dan-
ger of contact with live components. Before the 712 Conductometer
is opened to change components or for maintenance or repair work,
the mains cable must thus always be disconnected from the mains
connection plug 15 of the 712 Conductometer.
Setting the instrument supply voltage
3.3.2
Before switching on the 693 VA Processor for the first time, check that the mains
voltage set on the instrument (visible in mains voltage selector 12) matches the
local power supply voltage. If this is not the case, you must change the voltage
set on the instrument by moving the mains voltage selector 12 with a screwdriver.
Positions of mains [z30v] .
voltage selector 12: 230V: 220... 240 V + 10%
115V: 100... 120V + 10%
Fuse
3.3.3
The mains transformer of the 712 Conductometer is protected by a non-rever-
sible fusible cutout. If this blows, please inform Metrohm service.
Mains cable and mains connection
3.3.4
One of three mains cables is supplied with the instrument:
© 6.212.020 with plug SEV 12 (Switzerland ...
© 6.212.040 with plug CEE(7), Vil (Germany ...)
© 6.2122.070 with plug NEMA 5-15 (USA ...)
The cable is three-cored and fitted with a plug with an earthing pin. If a different
plug has to be attached, the yellow/green lead (IEC standard) must be connected
to the protective earth (instrument protection class 1).
Note: Each break in the earthing inside or outside
the instrument can make it a hazard.
Plug the mains cable into mains connection plug 15 of the 712 Conductometer
(see Fig. 1).
On/off switching of the instrument
The 712 Conductometer is switched on and off with mains switch 14.
When the instrument is switched on, all segments of displays 1 and 2 light up for
a few seconds and the instrument is then ready for measurement.
8.712.103 Instructions for use Chap. 3 Installation 3.4 Attachment of sensors
Conductivity cells and Pt100 or Pt1000 resistance thermometers can be attached
to the 712 Conductometer. The 6.0908.110 Conductivity Cell will be found particu-
larly practical as it has a built-in Pt100 temperature sensor.
The black banana plugs of the conductivity cells are connected to the black con-
nection sockets 7, the red banana plugs of the temperature sensors to the red
connection sockets 8 (see also Fig. 1).
Conductivity
cell
‘Temperature sensor
Fig. 2: Attachment of sensors to the 712 Conductometer
The following Table shows a selection of the most important conductivity cells
and temperature sensors available from Metrohm. In addition to the immersion
cells listed here, Metrohm also offers pipette, titration and Jones measuring cells.
You will find detailed information in the brochure ”Metrosensor Electrodes” and
in the Electrode Catalogue.
‘Min. immersion
Order No. | Description Cell constant
6.0908.110 | immersion coll wit integrated Pt100 os 40 mm
temperature sensor
6.0907.110 | immersion cel 08 40 mm
6.0910.120 | immersion cell for sample changer 09 20 mm
6.0901.040 | immersion cel on 50 mm
6.0901.110 | immersion cet! os 50 mm
6.103.000 | P1100 resistance thermometer;
application range -50 ... 100°C.
6.103.040 | Pt100 resistance thermometer for sample
‘changer, application range 50 ... 100°C
6.110.100 | Pt1000 resistance thermometer;
application range —50 ... 180°C;
also requires 6.2104.080 Cable (1 m) or
6.2104.110 Cable (2 m)
Chap. 3 - Installation 8.712.1008 Instructions for use Metrohm 7
The choice of conductivity cell depends on the expected conductivity of the ana-
lysis solution. The most important parameter here is the cell constant. The con-
ductivity measurement ranges for various cell constants are shown in Fig. 3. The
following rules of thumb apply:
© = 0.1 cm: for poorly conducting solutions such as distilled water, fully
oF partially demineralised water, etc.
c= 1 for moderately conducting solutions such as drinking water,
‘surface water, wastewater, etc.
c= 10 for solutions with good conductivity such as sea water, rin-
sing water, physiological solutions, ete.
¢ = 100 cmr': for solutions with very good conductivity such as electropla-
ting baths, brine, etc:
om 4 Cell constant
100
10
04
t+
0.1 4 10 100 1000 Siem Conductivity
1 10 100 1000 10°000 mS/cm
Fig. 3: Conductivity measurement ranges as a function of the cell constant
Notes on handling conductivity cells
‘© Degrease conductivity cells which have been stored dry by placing in acetone
for 1...2 h before use. Then rinse well with dist. water and place in dist. water
for 1...2 h.
© Conductivity cells in frequent use must always be stored in dist. water.
© During measurement, ensure that no air bubbles adhere to the electrode.
‘© The cell constant value printed on the cell can change on dry storage or in
measurements in which the platinum surface is contaminated. For accurate
absolute measurements, it is thus necessary to redetermine the cell constant
(see section 4.4.3).
© The platinum electrodes are platinised to reduce the polarisation, i.e. coated
with extremely finely divided platinum black. This platinisation must not be
touched or damaged. Damaged electrodes or those changed by ageing can
be replatinised (see section 7.3).
8.712. 1003 Instructions for use (Chap. 3 ~ Installation 3.5 Attachment of devices to the analogue output
3.5.1 Details of the analogue outputs
The 712 Conductometer has two analogue outputs 10 for the conductivity and 11
for the temperature which are configured and operated via dialogue (see sec-
tions 4.4.2 and 4.5.2). The circuitry of the two analogue outputs is as follows:
3.712.010 External ‘Comments
Voltage range of the
l analog oat
* Output (red) Cee
2 Resolution: 0.5 mV (12 bit)
OV (black)
Roa > 1k
Fig. 4: Analogue output circuitry of the 712 Conductometer
3.5.2 Attachment of a recorder
Any laboratory recorder can be connected to the two analogue outputs 10 for the
conductivity and 11 for the temperature. The 586 Labograph recorder available
as an option from Metrohm is attached to the conductometer as follows:
6.218.010 Cable
Recorder for
temperature
6.2115.010 Cable
586 4] Recorder for
—_ 2 0 | conductivity
Fig. 5: Attachment of recorders to the 712 Conductometer
Chap. 3 = Installation 8.712. 1003 Instructions for use Q.Metrohm 9
3.5.3
Attachment to 536 Potentiograph
3.5.4
The analogue output signal of the 712 Conductometer can be used as an input
signal for the 536 Potentiograph. This instrument combination can be used to
perform conductivity titrations which have to be evaluated manually. The 712
Conductometer is attached to the 536 Potentiograph as follows:
6.2112:080 Cable
Fig. 6: Attachment of the 712 Conductometer to the 536 Potentiograph
Attachment to Titrinos
The analogue output signal of the 712 Conductometer can be used as an input
signal for Titrinos to transfer measured conductivity values or to perform con-
ductivity titrations. The transfer of measured values is possible with all Titrinos,
the performance and evaluation of titrations only with the 702 and 716 Titrinos to-
gether with the 6.6015.000 Metrodata program "Titrino Workcell”.
If only measurement of the conductivity of the analysis solution is required, the
712 Conductometer can be attached to measuring input 1 of the Titrino (see Fig.
7, upper drawing). If, on the other hand, other high resistance sensors such as
pH glass electrodes are used in addition to the conductivity cell, electrical isola-
tion must be ensured. This is achieved by connecting the conductivity signal to
the "Pol" input (with I= 0), whereas the pH is measured differentially. In such a
case, the conductivity cell also serves as an auxiliary electrode for the differential
analysis solution (see Fig. 7, lower drawing).
Conductivity call ~~
6.2116.000 Cable
pH glass electrode
Reference electrode
‘Conductivity cot
04.000 Adapter Cable
6.2176.000 Cable
Fig. 7; Attachment of the 712 Conductometer to Titrinos
8.712.103 Instructions for use Chap. 3 = Installation 10 &.Metrobm
Attachment of devices to the RS232 interface
Note: Before an external device is attached to RS232 interface 18,
the 712 Conductometer must always be switched off using
mains switch 14!
Fig. 8: Attachment of external devices to the RS232 interface
3.6.1___ Attachment of a computer
The below Table provides information on the attachment of IBM-compatible PCs
to RS232 interface 18 and shows the cables required as well as details of the
Conductometer and PC configuration.
PC Cable _| Settings on 712 Gonductometer | _ Settings on PC
‘Computer with Deont ig/print
25-pin RS232 | 6.2125.060 | Sent to: 18H
connector 2eontig/RS282 settings Setting of the RS
aud i parameters depends on
Computer with} 6.2125.060 | S888 pit: Settings ‘control program
Spin RS232 + parity: Sao!
connector 6.215.010 _| hanash
Remote control of the 712 Conductometer via the RS interface is described
section 5. For the transfer of experimental data of the 712 Conductometer to a
PC, Metrohm offers the optional PC program VESUV 2.0 (order number
6.6008.010).
3.6.2 Attachment of a printer
Any external printer with a serial interface and which is compatible with one of the
following printer drivers can be attached to the RS232 interface of the 712
Conductometer (see also section 4.3):
eM IBM Proprinter and compatible printers
Epson EPSON printers and compatible printers
Seiko Seiko printer DPU-411
citizen Citizen printer IDP560 RS
HP HP printers such as HP DeskJet ..., HP LaserJet ..., etc.
The below Table provides information on the attachment of several selected
printers and shows the cables required as well as details of the Conductometer
and printer configuration. if you attach a printer not included in the list of printers
below, please ensure that it can emulate a printer mode supported by the 712
Conductometer. If possible, select the same settings for printer and 712
Conductometer as for the emulated printer type.
(Chap. 3 - Installation 8.712.1009 Instructions for use Q.Metrohm
1
Setings on 772
Printer | cable | seltngson712 fetunge on printer
‘SEIKO. 6.2125.020 | Peontig/erint —- |_| DIP switch settings:
opustt-118, eendhees 2
ew Dont ig/nszae sett ngs PP
SEIKO aloe The pier as only a otcheble
Bebe -208 ee | Teast charctr st availa
ae en fone | wctrcon bs changed automat
yands| Hes: cally by the 712 Conductometer in.
oayenen seciceace wih hw sat Selous
at no | Sesee
Tength a german: S021 (german)
‘english: 'SO 6 (ANSI)
french: 1S069 (french)
‘spanish: 1SO 7 (spanish)
CITIZEN 6.2125.050 | reonfig/print DIP switch settings:
ome a |
dennrg/9ta2 satin
i; 4 ‘The printer has only a switchable
$ | TinASen cheact st avelblo
se fore | mrlchangeover tothe nebond
handshake: tats character sets is possible only
oan trough changing re positons of
Zest 19 | pepe ang Parner
v charactor aot
SORT oma
‘open | open | ISO 6 (ANSI.
closed | open | 18069 (french)
Sperish doos not hve is own
character set (it is best to use
‘rena
xooak asso | esa irerine Gatings va dntve-qided sotup
Diconix 180 si send tei ee procedure:
reerigsee ettngs |e aap
fei ot [eer 8
tle: RE Fat ne
"tt oy [OTR nih
EPSON P-40 6.2125.040 SOO ra Epson DIP switch settings:
Zagat ugraszae consis
2a ee
ate st
EPSON LQ-. 6.2125,040 | reont tg/print DIP switch settings:
EPSON IC 2 cpm
i | sve ASSP
See ee
sae An
8.712. 1003 Instructions for use
‘Chap. 3 ~ Installation 12
&©4Metrohm
Settings on 712
Printer | cabo | Settings on712 Sotings on printer
EPSON LG... |6.2125.040 | Yconfig/erint | DIP switch settings:
EDSON Ue i 7
EPSON PX 232 settings sw: Palle
fanaa ws
‘vice #314) : owe (aaa)
im
ase A
18M Proprinter | 6.2125.050 | Dconfig/erint Baud rato 9600
eat ag! ju a
ane Soper
Stop. bit XON off
ih orn ae
HP Deskjet 6.2125,050 | reontig/priat DIP switch settings:
Cee Sent nena
Wer | ont ig/a803 anteigs
a cenl
Seratprs | $88! a
otcor, | faceekines ASE
vonorigar | mreke
sorncedes | 20th Le
We tmeqats.. | exrannen | Dosatigrorie ronfaurced=l
send to: HP FONT NUMBER = 2
peonfig/RSZ32 settin 1s PAPER Aa
data bit = FORM 64 LINES
sep BE [Sts Se
Tongth 1.0 ROBUST KON = OFF
" cable, 2s. | Sond te: “ paPE a
(eg.HP. | gta Bit : RET MEDIUM
Cssn | RE eae ected
jandshake: His: FONT SOURCE = I
mt ue | Seen ches
a) ey ‘SERIAL MENU
DTR POLARITY = HI
Chap. 3 — Installation
£8.712,1003 Instructions for use Q.Metrohm 13
3.7 Attachment of devices to the remote interface
3.7.4 Details of the remote interface
Any external devices can be attached to the 25-pin remote interface 17. The 712
Conductometer can be remote controlled via the 8 input lines, whereas the 8 out-
put lines can be used to control external devices.
Fig. 9: Attachment of external devices to the remote interface
The pin assignment of the remote interface, its functions as well as the electrical
conditions and statuses are described in section 6.
3.7.2___ Attachment of a sample changer
The Metrohm 673/674 Sample Changer or the associated control ur attached
to remote interface 17 of the 712 Conductometer as follows:
622
'.980.3560 Cable
Fig. 10: Attachment of the 712 Conductometer to the 664 Control Unit
The following settings are needed for the above interconnection for measurement
of the conductivity on the sample changer:
(664 Control Unit! Mode 4
‘At1 =Wait time until the measurement (0...5 min).
On elapse of this wait timo, the command is initiated
con the 712 Conductometer.
712 Conductometer: Parameter "config/print meas.value/print crit.: = ined.”
Following the measured value printout initiated by the command,
the advance pulse (EOD) is outputted to the 664 Control Unit,
8.712.103 Instructions for use Chap. 3 ~ Installation 14
4.
Manual operation
41
Introduction to operation by means of examples
444
For you to perform the examples described in this section, the 712
Conductometer must be put into operation properly. If this has not already been
done, please proceed in the following sequence (you will find more detailed in-
formation in the specified sections):
1 Setting up instrument Section 3.1
2» Mounting accessory Section 3.2
3» Setting correct mains voltage Section 3.3.1
4» Mains connection Section 3.3.3
5» Switching on instrument Section 3.3.4
6? Attaching sensors Section 3.4
(Please also consult the notes regarding
handling of conductivity cells!)
The only thing still missing is an analysis solution. Fill the measuring vessel with
tap water and immerse the conductivity cell in the analysis solution until the vent
holes are covered. Ensure that no air bubbles adhere to the platinum electrodes.
We can now proceed with our short training course. Note that all displays of the
examples refer to the condition in which the instrument was first put into opera-
tion (initial condition). If you do not wish to run through these examples until later,
differences in regard to dialogue language and parameter values may appear
(please see section 7.6 for how to return to the initial condition).
Basic instrument mode, main and auxillary display
After the 712 Conductometer has been switched on, the instrument is always
automatically in the basic mode for conductivity measurement. The measured
conductivity value and the associated unit (either yS/om” or mS/cm") are shown
in the main display 1. The magnitude of the displayed conductivity should not
concern us at present as for an accurate measurement the cell constant of the
measuring cell and the measurement temperature have to be set correctly (more
about this later).
Below the main display you will see the dialogue display (the two-line LCD 2). In
the basic mode, this shows 3 numeric values and their associated units with the
following meaning:
Current measurement
temperature
(if you have attached a tempera
{ure sensor, the measured tem-
erature is displayed here)
Current temperature costticient
Current cell
‘constant
Before we concern ourselves further with the conductivity measurement, let us
first examine the basic principles of data entry.
(Chap. 4.1 — Introduction to operation £8.712,1003 Instructions for use QaMetroben
4.1.2 Data entry
15
The basic principle of data entry will be illustrated using the entry of the date and
time and switching the dialogue language to German. Process stepwise as de-
scribed in the sequence below.
1.000 Zen
20.0 °C
2.00 47°C
The 712 Conductometer is still i
ment mode.
the measure-
Now press the key.
cont
Deonf ig/print
The dialogue display shows the title of the "print"
group, which contains various inquiries concern-
ing print output on an external printer.
The key contains several such groups
of inquiries, which can be selected by repeated
pressing of this key. Each group has a title
marked by ">".
Press the key again.
contig
Deonf ig/print me
value
The display shows the title of the "print meas.
value” group, which contains various inquiries
concerning the printout of the measured values on
an external printer.
Press the key again.
conti
Deonfig/report type
The display shows the title of the "report type”
group, which contains various inquiries concern-
ing the report printout on an external printer in
calibrations.
Press the key again.
config The display now shows the title of the “auxiliaries”
group, which contains among other things the in-
Deonf ig/auxiiaries
quiries we seek concerning entry of the date, time
and dialogue language.
Now press the key to move from the ti-
tle to the individual inquiries of the "auxiliaries"
group. The title continues to be displayed in the
first line.
Deont ig/auxitiaries
The display shows the selection of the run num-
ber as the first inquiry. As we have no interest in
this, let us proceed immediately to the next in-
quiry.
Press the key.
8.712. 1003 Instructions for use
Chap. 4.1 — Introduction to operation 16
&\Metrohm
Deon ig/auxitiaries
date 94-07-04
The display shows the date with the numeric data
for year, month and day as the next inquiry. If the
date shown matches the current date, all you
need do is confirm it by pressing the
key.
However, should you wish to change this date, en-
ter the new numeric values in the order year -
month - day with the numeric keys, for example
*o4-09-06" for 5" September, 1994.
Confirm the new date you have entered by press-
ing the key.
Deonfig/auxiliaries
time 16:03:64
The display shows the current time with the nu-
meric data for hours, minutes and seconds as the
next inquiry. If the time shown matches the current
time, all you need do is confirm it by pressing the
key.
It you wish to change the displayed time, enter the
new numeric values in the order hours - minutes
= seconds with the numeric keys, for example
08:32:00".
Co
key.
irm the new time by pressing the
> xi s
a nglish
