Bell’s Method
Gives satisfactory predictions for HTC & DP in Shell side of HX
Effects of leakage, bypass, flow in Flow & window Zone, constructional tolerances are
accounted
Limitation: ??? By-pass flow area > 30% of CFA
𝐵𝑢𝑛𝑑𝑙𝑒𝑐𝑟𝑜𝑠𝑠 sec 𝑡 𝑖𝑜𝑛𝑎𝑙𝑎𝑟𝑒𝑎𝑖𝑛𝑊𝑖𝑛𝑑𝑜𝑤𝑧𝑜𝑛𝑒
𝑅𝑎′ =
𝑇𝑜𝑡𝑎𝑙𝐵𝑢𝑛𝑑𝑙𝑒𝑐𝑟𝑜𝑠𝑠 sec 𝑡 𝑖𝑜𝑛𝑎𝑙𝑎𝑟𝑒𝑎
Nc: No. of tubes in cross flow zone
Shell side heat-transfer coefficient
hoc HTC for CF over an ideal tube bank
Total correction : 0.6 - 0.9
hoc: Ideal cross flow coefficient
For 10 tube rows
Fn: Tube row correction factor
Flow Regime : laminar & Turbulent
Fn = 1
Fn is function of number of tune rows between baffle tips
Fw: Window correction factor
Effect of flow through Baffle window
This is function of HTA in window zones & the total HTA
Rw : Ratio of number of tubes in window zone to the
number of tubes in bundle
Bundle cross sec tional area in Window zone
Ra' =
Total Bundle cross sec tional area
For no sealing Strips:
Fb: Bypass correction factor
Fb: Leakage correction factor
Total Shell side Pressure Drop
affects the pressure drop in cross flow zone
affects both cross flow zone and window zones
No leakage in end zones, Only Window Zone
CONDENSATION
Types of Condensation
Film-wise Condensation
Drop-wise Condensation
Selection ……
Horizontal Shell side
Vertical Tube side
Reasons
Condensation Outside the Horizontal tube
Condition….???
Vapor shear forces & non condensable gases
HTC increases & HTC decreases
Condensation flow over tube banks Condensation inside the Horizontal tubes
No correction is required
Low condensate & High vapor & low
vapor flow rates condensate flow rates
Boyko & Kruzhilin Correlation for Annular flow:
Based on Vapor Quality at inlet and outlet conditions
If saturated vapor and total condensate
For Stratified flow:
Condensation inside/Outside the Vertical tubes
Condensation on the Vertical surfaces
Horizontal Position – Natural Convection –
No Reliable correlations are there
Increase the area, Increase the length
PROCESS DESIGN KETTLE TYPE REBOILER
Perfect pool Boling
Heat transfer in nucleate boiling region
Maximum Heat transfer in – Nucleate Boiling regime
Excess Temp: less than or close to Critical temperature drop
For Water : 20-30 oC, For light organics : 20-50 oC
Boiling side pressure drop is negligible – High vacuum distillation
column
PROCESS DESIGN KETTLE TYPE REBOILER
1. Calculation of heat duty
Energy balance around Distillation column
2. Fix the DTm, th = DTm + tb
3. Select the suitable heating medium
4. Mass flow rate of heating medium required
5. Estimate the heat transfer area
6. Fix do (25.4 mm OD), L,
Square pitch, U tube arrangement,
Pitch : 1.5 -2 do , Vapor Blanketting
% Baffle cut : 0, Bs = Ds
7. Shell side boiling coefficient – Monstinski Equation
8. Tube side heat transfer coefficient
9. Calculate Overall heat transfer coefficient
10. Calculate Heat transfer area
11. % excess area : 10-20%
12. Calculate actual heat flux = Heat duty/Aprovided
13. Actual heat flux <= 0.7 Critical heat flux at critical temp drop
14. Critical heat flux : Zuber Equation
15. Find the shell diameter
Shell ID = Liquid level + 0.15 to 0.25 m
Liquid level = Tube bundle diameter + 50 to 100 mm
Heat flux Shell ID/Tube bundle dia ratio
< 25000 W/m2 1.2 – 1.5
25000 - 40000 W/m2 1.4 – 1.8
> 40000 W/m2 1.7 – 2
16. Check liquid entrainment, Vmax = 0.2 {(rLiq - rVap)/rVap}0.5
Actual vapour velocity should be less than Vmax (Vact @liq surface = (mv/rv)/(Liq Surface area)
Monstinski Equation
PROCESS DESIGN VTSRB
1. Calculation of heat duty
Energy balance around Distillation column
2. Fix the DTm, th = DTm + tb
3. Select the suitable heating medium
4. Mass flow rate of heating medium required
5. Assume overall HTC, Uo = 1000 W/m2 oC &
Estimate the heat transfer area
6. Fix do, L, Pitch,
Pitch : 1.5 -2 do , Vapor Blanketting
% Baffle cut : 15 -45%, Bs = Ds
7. Recirculation Ratio (4 -24)
.0
m Lo mLo - Mass flow rate of liquid at outlet of reboiler
Liquid recirculation = 0 mvo - Mass flow rate of vapor at outlet of reboiler
m Vo
PROCESS DESIGN VTSRB
8. Do the pressure balance:
At SS Condn., Available differential head = Pressure loss in the circuit
DPavail = DP in base of DC + DP in Piping & Nozzles
+ DP in reboiler (Tube side DP)
Velocity at DC bottom << Velocity of liquid through pipes
Piping is smooth & higher in sizing
At SS Condn., DPavail = DP in reboiler (Tube side DP)
DPavail = L (rL - rav) g ,
rL Density in cold leg, rav Density in hot leg, L : Length of the tube
Vo mvo + mLo
ln rV r L
Vo =
Vi
r avg = mvo − mLo
Vo − Vi Vi = 1
rL
9. Compare both DPavail & DPt , Five Different cases are possible.
Five Different cases are possible:
1. DPavail = DPt 1. Proceed to next step
2. DPavail > DPt 2. RCR assumed < RCR actual
3. DPavail >> DPt or DPavail /DPt > 50 3. RCR assumed << RCR actual
4. DPavail < DPt 4. RCR assumed > RCR actual
5. DPavail << DPt 5. RCR assumed >> RCR actual
Case 3: DPavail >> DPt
DPavail = L’ (rL - rav) g
DPavail = DP t + DP Flow meter + DP Control Valve
Case 4: DPavail < DPt
DPavail = L (rL - rav) g + r g h
Increase the No. of tubes and decrease the length
What will happen?
Case 5: DPavail << DPt
Actual RCR is very low…or < 4
When viscosity is low, this is possible.
Pump in the inlet line to the reboiler
10. Estimate the Tube side HTC
In addition Kern mentioned that
if hi is more than 1700 W/m2 oC,
take 1700 W/m2 oC
11. Shell side HTC : 6000 W/m2 oC
12. Calculate Overall heat transfer
coefficient
13. Calculate Heat transfer area
14. % excess area : 10-20%
15. Find the shell side Pressure drop
Forced Circulation Reboiler
1-2 HX : When process fluid in Shell side
1-1 HX : When process fluid in Tube side
High tube velocities : 3-9 m/s
Commercial Reboiler:
Heat Flux < 63 000 W/m2 for Organics
Heat Flux < 95 000 W/m2 for Water & Aq. Solutions
CONVECTIVE BOILING
Different from Pool Boiling
Role of State of the fluid
Single Phase flow Region:
Liquid below its boiling point
Sub-cooled Boiling Region:
Near the wall – Boiling Point
Saturated boiling Region:
Bulk boiling of the liquid – Nucleate boiling –
Different flow patterns
Dry wall Region: Mist flow – Both Cvn & Rdn
CHEN’s METHOD
hcb : Forced Convective HTC
h’fc : Convective Boiling HTC
h’nb: Nucleate Boiling HTC
Convective Boiling HTC
Nucleate Boiling HTC
Chen’s Method for Vertical tubes – Suitable Correlations can be used to predict hfc
Vapor Quality changes continuously – Section wise HTC & HTA Estimation
Example : 12.8 CR- Vol 6
EVAPORATOR
EVAPORATOR
Evaporation : Concentrating the solution (Non volatile solute + Volatile Solvent)
Examples: Sugar from aq. Solns., NaCl, NaOH, Milk, Glycerol, Orange Juice, Water
from Sea water
Chemical Evaporators
Power plant Evaporators
Processing factors:
Concentration (Density, Viscosity & Boiling Point)
Solubility, Temperature sensitivity, Pressure & Temperature, Foaming, Scale,
Types of Evaporation – Single & Multistage
Main Components of the Evaporator:
1. Tube Bundle surrounding the shell (Calendria) Dia : 1 m – 6 m,
2. Evaporator body (Vapor release Chamber) OD : 25 mm – 75 mm
3. Two heads L : 750 mm – 2000 mm
Central Down Take :
40-100% of C/S Area of Tubes
• Standard Vertical Short Tube Evaporator (Calendria)
Area occupied by each tube:
Area occupied by ‘n’ tubes:
Types of Evaporator:
1. Open Pan/Kettle Es
2. Hztl tube Natural Circulation Es
3. Vertical Natural Circulation Es
4. LTVEs
5. Falling film Es
6. Forced Circulation Es
7. Agitated film Es
8. Open pan solar Es
Boiling Point Elevation
Boiling Point Elevation
MULTIPLE EFFECT EVAPORATOR
CALCULATION OF MULTIPLE EFFECT EVAPORATOR
The Known values:
(i) Feed Conditions & Flow in I Effect
(ii) Steam Pressure in I effect
(iii) Final effect Pressure in vapor space
(iv) Final Concentration in the liquid leaving the last effect
(v) Physical Properties such as enthalpies,/ Cp of L & V
(vi) Overall HTC in each effect
1. From known concentration & ‘Pressure’ in last effect - Estimate the ‘BP’
in last effect, BPE can be from Duhring line plot
2. Estimate the Vapor evaporated from OMB
First Trial, V1 = V2 = … =Vn
From MB in each effect, Calculate L1 = L2 = … =Ln
From Solute Balance, find out Solids concentration in each effect
3. Using the equation, ,
estimate
If Cold feed, extra heating load, proportionately large
4. Using Material and Energy Balance in each effect, Calculate Vapor & Liquid flow
rate in each effect.
Compare this values with Initial assumption on V1 , V2 , … Vn
If difference is more, Repeat the procedure using calculated values of
V1 , V2 , … Vn
5. Once arrived the satisfied values, Calculate the value of ‘q’ transferred in each effect
Calculate the Area using rate equation for each effect, A1 , A2 , …
An
Calculate the average value
If Areas are not nearly equal, Second trial should be tried
6. Obtain new values of
A solution having 10% dissolved solids is to be concentrated to 30%
solids by weight in a triple effect evaporator at the rate of 10 TPH.
The feed is at 100oC. Low pressure steam is available at 1.5 kg/cm2
gauge. A forward feed configuration is used with a vacuum of 660
mm Hg maintained in the final effect using a single stage steam jet
ejector. The BPE in the final effect is 10oC and in the absence of
more data, the BPE can be approximately taken to be proportional
to the solid concentration in wt.% If the overall heat transfer
coefficients in the effects are 2500, 2000 and 1000 kcal/h mr2 oC
respectively, calculate the evaporator area in each effect.
A Triple effect forward feed evaporator is being used to evaporate a sugar
solution containing 10 wt % solids to a concentrated solution of 50%. The
boiling point rise of the solutions can be estimated from
BPR (oC) solution = 1.78x + 6.22x2,
where x is wt fraction of sugar in solution.
Saturated steam at 205.5 kPa is being used. The pressure in the vapor
space of the third effect is 13.4 kPa. The feed rate is 22680 kg/h at 26.7oC.
The heat capacity of the liquid solutions is Cp = 4.19 – 2.35x kJ/kg K.
The heat of solution is considered to be negligible. The coefficients of heat
transfer have been estimated as U1 = 3123 W/m2 K, U2 = 1987 W/m2 K and
U3 = 1136 W/m2 K. Calculate the area and other dimensions of the
Evaporator.