Scotch-Weld^

§frucfiKal Adhesive Primer

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Technical Data Issue No. 3

Introduction 3MrM Scotch-WeldrM Structural Adhesive Primer EC-3917 is a primer for 3MrM
Scotch-WeldrM epoxy based fi1m adhesives. EC-3917 prime¡ contains a cor¡osion
inhibitive pigment for added corrosion protection. Priming with EC-3917 offers the
following advantages:

AdYantages Insures complete wetting ofthc adhcsivc to thc adhcrcnds

Improves durabiliry of bondedjoint

Protects cleaned surfaces

Can bc brushcd or sprayed

( ¡n bc u.rd a: J (orro\ron resislant co¡tine

Description Note: The follo\ving tcchnical iriformation and data should be considered representative
or typical only and should not be used for specific¡tion purposes.

Color: Yellow - oreen

Base: Synthetic Resin

Net Weight: 7.2 lbs./gallon (0.863 Kg/liter) [approximate]

Sol¡ds Content: 12!1%

Flash Po¡nt: 20"F C6.67'C) [Closed Cup]

Note: EC-3917 primer must be thoroughly stirred prior to use.

Product Performance All data ¡eported in this section is Rpical data obtained on EC-3917 primed aluminum
surfaces. Prior to priming, the metal was etched as described in the surface preparation
section ofthis data sheet. Where noted, the etch was followed by chromic acid
anodization. After primer application a¡d dry, the bonds we¡e assembled and cu¡ed
for 60 minutes at 350'F (177'C) (250"F [12]'C] for the 3MrM Scotch-WeldrM Film
Adhesive AF 126 se¡ies and AI 163-2 series). A 4-5'F/minute (2.2-2.8'C/minute) rise
rate to tempe¡ature and 45-50 psi (3.1-3.4 bar) pressure was used. Parts were cooled
to betow 200"F (93oC) before the pressure was removed.
Scotch-Weld''
Structural Adhesive Primer
EC-3917

Product Performance (cofltifl ue.l)

Note: The follorving technical information and data should be considered representative or typical onh and should not
b€ used for specification purposes.

l. Metal to Metal Oyerlap Shear

AII properties rverc measu¡ed on 1 " widc,
I /2 " overlap specimcns cut frorr 0.063 " thick 4" x 7" bonded panels of
2024-T3 alclad aluminum. Tests wcrc conducted per MMM-A-132.
Note: AF 163-2K (.06 wt.) tests werc conducted on unsealed chromic acid anodizcd panels. (Scc 3M Test
Method C-2801.)

Test 3M Adhes¡ves
Temperature AF 126-2 (.06 wt.) AF 147 (.075 wt.) AF 1¡13-2 (.10 wt.) AF 16s-2K (.06 wt.)

-67'F (-55'C) 3000 psi 20.7 MPa 3500 psi 24.1 MPa 2600 psi 17.9 MPa 6000 psi 41.3 MPa
75"F \24"C) 4000 ps¡ 27 .6 MPa 4500 psi 31.0 MPa 3250 psi 22A MPa 5800 psi 40.0 I\4Pa
250'F (121'C) 700 psi 4.8 MPa 3500 psi 24.1 MPa 2700 psi 18.6 MPa 1500 psi 10.3 MPa
300'F (149'C) not tested not tested 2200 psi 15.2 MPa 2700 ps¡ 18.6 MPa not tested not tested

2. Metal to Metal T-Peel

T-Pccl strength was mcasu¡ed on 1" wide specimen cut from unsealcd, chromic acid anodized, ti" x 8" x .020"
bonded panels of2024-T3 alclad alurniuum. Tests rvc¡c conducted pcr MMM-A-132.

Test 3M Adhesives
Temperature AF 126-2 (.06 vrt.) AF 147 (-07s wt.) AF 143.2 (.10 wt.)

-67'F (-55'C) 25 piw 111.2 N/25mm 25 piw 111.2 Nl2srntn 30 piw 133.4 N/25rnm
75',F 124"C) 30 piw 133.4 N/25r¡m 30 piw 133.4 Ni25mm 45 piw 200.2 N/25mm
180"F (82"C) 25 piw 111.2 N/25mm 25 piw 1l'1.2 N/25mm 35 piw 155.7 N/25mm

3. Metal to Metal Floating Roller Peel

Pecl strength was measured on 1" widc spccimens cut from a 3" x 8" x .063" 2024-T3 bare alurninum pancl
bondcd to a 3" x 10" x .025" 2024-T3 bare parcl. Tests wcrc coDducted per ASTM D-3167.

Test 3M Adhesives
Temperature AF 126.2 (.06 wt.) AF 147 (-075 wt.) AF 143-2 (.r0 wr.)

75"F 124'c) 50 p¡w 222,4 Nl2srl,n], 30 piw '133.4 Ni25mm 6 piw 26.7 N125nn

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Scotch-Weld"'
Structural Adhesive Primer
EC-3917

Product P€rformance Note: The following technical information and data should be considered representative
(continued) or typic¿l only and should not be used for specification purposes.

EC-3917 with 3MrM Scotch-WeldrM Structural Adhesive Film AF 191M (.035 wt.)
Floating Roller Peel Result at -67"F (-55'C) and 75'F (24'C) versus Primer Thickness

Pr¡mer Thickness (lb/in) (lb/in)

(mil) 67"F G55'C) RT

0.08 37

0.10 31 39

36

0.20 I 28

4. Resistance to Environment
When used as a primer,EC-l9|7 attack by salt spray, high humidity, a¡d aircraft
test fluids.
Given below is typical data on AF 126-3 (.06 wt.) on EC-3917 primed
aluminum prepared as in section Metal to Metal Overlap Shear. The overlap shear
and environmental tests were according to MMM-A-132.
Scotch-Weld"'
Structural Adhesive Primer
EC-3911

Application Proper primer application is as important as proper bond design and adhesive choice to
obtain maximum joint properties. lmproper adhcsive application techniques can result
in partial or completc failure ofan assembly.

EC-3917 primer will give exccllcnt results under the following suggested procedurcs.
Variations from these procedures should be fully evaluated to insure bond properties
sumcient to mcet the requirements ofyour particular assembly.

Surface Preparation Suggested Cleaning Procedures lbr Aluminum

A thoroughly cleaned, dry greasc-free surface is essential for maximum performance.

Cleaning methods which will produce a breakf¡ee water film on metal surfaces are
generally satisfactory. Surface preparation should be fully evaluated with the adhesive,
especially ifresistance to specific cnvirorunents is anticipated.

l. Alkaline Degrcasc - Oakite 164 solution (9- 1 I oz./gal. water) at l90oFr lo"F
(87 *
5.6"C) for 10-20 minutes. Rinse immediately in large quantitics ofcold
running water.
2. Optimized FPL Etch Solution ( I liter):
Material Amount
Distilled Water 700 ml plus balance of liter (sec below)
Sodium Dich¡omate 28 to 67.3 grams
Sulfuric Acid 287.9 to 310.0 grams
Aluminum Chips 1.5 grams/litcr of mixed solution
To prepare I litc¡ ofthis solution, dissolve sodium dicbromate in 700 ml ofdistillcd
water. Add sulfuric acid and mix we[l. Add additional distillcd water to fill to 1 liter
Heat mixed solution to 66 to 71'C ( 150 to 160'F). Dissolve 1 .5 grams of 2024 barc
aluminum chips per liter of mixed solution. Gentle agitation will help aluminum
dissolve in about 24 hours.
*Note: Revicw and fbllow safety and health information provided by suppliers of
these materials prior to prcparation ofthis solution.
To FPL ctch panels, place them in the abovc solt¡tion at 150 to 160'F (66 to 7l'C)
for 12 to l5 minutes.
3. Rinse - Rinse panels in clear running watcr.
4. Dry - Air dry 30 minutes; forcc dry 30 minutes at 140"F (60"C).

5. It is advisable to coat the ficshly cleaned surfaccs with EC-39 t 7 within four (4)
hours añer surfacc preparation.
6. Care should be taken to avoid contaminating the clca¡ed aluminum by any substance
which will hinder the wefting acrion ofEC-3917.

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Scotch-Weld"'
Structural Adhesive Primer
EC-3917

Surfáce Preparation Primer Applicatlon: EC-3917 is satisfactorily applied by brush coating to spraying.
(continued) Primer must be thoroughly stinedjust prior to application.

Spray Gun
A. Spray Procedure DeVILBISS JGA BinksNo.62
Air Cap 30 66SD
Fluid Tip and Needle AV-IS-FX 66-365
Cup Prcssure 2-4 psi (13.78-27.56 MPa) Siphon Feed
Line P¡essure 30 psi (0.207 MPa) 30 psi (0.207 MPa)
Distance from Panel 9 t3 in. (228.6 + 76.2 mm) 6-9 in. (152.4-228.6 mm)
Primer Thick¡ess 00005-00015 in. (1.27-3.81 micron)
Primer Wcight 140-420 mg/sq. ft.

B. Primer Dry and Cure

Air dry for 30 minutes minimum at 75oF (24'C) followed by force cure for 60 minutes
at 2s0oF (r 2l oc).

Note: The above primer application procedures will give satisfactory perfbrmance with
3Mrv Scotch-WeldrM Epoxy Adhcsives. Howevcr, review the particular product
technical sheet for üc optimum primcr application to be used with that product.
Thc primed surf'ace should be protected from contamination intoduced by dust,
fingcrprints, oil, ctc.

Ifextended periods ofstorage are required, wrap thc pans in unplasticized Kraft paper. lf
the cured, primed surface is contaminated with dust, it may be cleaned prior to bonding by
wiping with clcan unsized cheesccloth and ketone* type solvents.

Cleanup: Excess primer and equipmcnt may be cleaned up, prior to curing with ketone*
type solvents.
*When using solvents, extinguish all sources ofignition in the area, rcview and follow
suppliers precautionary information prior to handling these materials.

Adhesive: EC-3917 primer performs satisfactorily wirh AF 126, AF 126-2, AF 143-2,

AF l4'7, AF 453-2, AF l9l, AF 163-2 and A-F 163-3MrM Scotch-WeldrM Structural
Adhcsives. See rcspective technical data shect for adhesive application.

Storage & Handling Storing and Aging Precautions Avoid heat and dampness in stomge. Store ncw
shipments behind older lots. Refrigerated or freezer storage,40'F (4.4'C) or below is
¡ecommended for EC-3917. Rotate stock on a "fi¡st in - fi¡st out" basis.

Caution: Primer should be permitted to thoroughly waIm to ¡oom temperature bcfore

being used in order to prevent moisture condensation.

3M Standard shclf lile olEC-3917 primer is 6 months from date ofshipment fiom 3M
when stored at 40"F (4.4"C) or below in its original unopened containcr.

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Scotch-Weld'
Structural Adhesive Primer
EC-3911

Precautionary See Product Label and Mater¡al Safety Data Sheet for health and safety information
Information before using this product. For additional health and safety information call 1-800-364-
3577 or 651-737-6501

For Additional To request additional product ¡nformation or to arrange for sales assistance, call toll
Information free (800) 235-2376. Our fax number ¡s (417) 869-5219. Address correspondence to:
3l\4 Aerospace Central, 321 1 E. Chestnut Expressway, Springfield, l\.4O 65802.

Important Notice 3M I\,4AKES NO WARRANTIES, EXPRESS OR fu]PLIED, INCLUD NG, BUT NOT LIi,4ITED To, ANY
II\,,IPLIED WARRANTY OF ]\,4ERCHANTABLLITY OR FITNESS FOR A PARTICULAR PURPOSE, USCT iS
respons b e for determ¡niñg whether the 3N4 producl is fil for a particu ar purpose and su table for users
method ofapp icaUon. P ease remember that many faclors can affect the use and performance of a 3M
Adhesives D¡vislon product in a particular appl cation. The rnaierials io be bonded wilh ihe product, lhe
sulace p¡eparaton ofthose materia s, the product se ected for use, the conditions in wh¡ch the product ls
used, and the tir¡e ánd environmenial condlUons in which the product ¡s expected to perform are among
the rnany factors that can áffect the use and performance of a 3lV product. Given ihe variety offactors
that can affecl the use and performance of a 3[,] producl, some ofwh ch are un¡q!rety within the user's
knowedge and contro, it is essential ihat the user evaluate the 3l\l product to determine whether ¡t ¡s fit
for a parlicular purpose and suilable for the users method of app icat on.

Limitation of Remedies lfthe 3lvl product is proved to be defective, THE EXCLUSIVE REMEDY AT 3M'S OPT|ON, SHALL BE TO
and Liability REFUND fHE PURCHASE PRICE OF OR TO REPAIR OR REPLACE THE DEFECTIVE 3I\,1 PRODUCT.
3l\, shall not otheMise b6 liable fer loss or damages, whelher direct, indirect, special, incidentat, or
consequential, regardless of the legaltheory asserted, including. but not limitod to, contract, negligence.
warañty, or slrict liability.

This Adhesives Division produciwas manufactured under a 3lV qualiiy system registered to ISO 9002 standaEs.

For Additional Product Safety and Heálth Info¡mation, See Material Safety Data Sheet, or call:

f,ut
Adhesives Division
3M Center, Building 220-8E-05
St. Paul.MN 55144-1000
Phone: I-800-364-3577 or 651fi37-6501 1t)%p¡? tohttr|r
www.3M.con¡/Adhesives l1)% pa!¡ .ottsu Pr o3M PC2000 78 6900 9357 5

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