IPC CH 3 Complete
IPC CH 3 Complete
Unit
Unit Name Major Learning Objectives Topics and Sub Topics
No.
Introduction of Process
Justify need for
Measurement:
instrumentation in
Importance of instrumentation
chemical plant.
in chemical plant
Classify instruments in Classification of instruments
chemical plant
Describe Basic elements of Basic elements of instruments
Introduction to
instruments.
Process
3 Measurement Compare Static and Static and dynamic
(3 hr, 8 marks) Dynamic Characteristics of characteristics
instruments
Selection criteria for various
Select appropriate measuring devices in chemical
instrument for industry for:
measurement based on Temperature
instrument range. Pressure
Flow measurement Liquid level
instrument interacts with the process, and produces an output which is in some
sense related to this input and this output should be in a form which can which can
be interpreted by the observer.
Direct Measurement
This type of measurement is an important approach in modern industry. For example
in manufacturing a mechanical part in a lathe section of a machine shop, the purpose
is to produce a part with a given physical conditions. During and after the production
of the part, the measurements are usually made. This type of measurement is direct
measurement in which the meaning of measurement (determining the physical
dimensions) and purpose of processing operation (producing goods of given
specification) are both the same.
Thus if the primary purpose of making a measurement is to determine the quality of
product one must use Direct Measurement.
Examples:
The measurement of temperature of fluid by means of thermocouple/thermometer;
measurement of pressure in the reactor using pressure gauge/ differential pressure
transmitters; measuring the level of liquid in a tank using sight glass tube; measuring
the flow of fluid through pipe using a rotameter etc. are some examples of direct
measurement.
In-Direct Measurement
This can be well understood by taking an example of temperature measurement in
milk pasteurizer. The purpose of pasteurizing is to remove bacteria. This is indirect
Transmitting
Here the instrument conveys information concerning the measured quantity over
some distance to a remote point. So, the instrument will measure the quantity and
convey the information from one place to another a homely example is telephone.
Signaling
Here the instrument indicates the general value or range of values of its measured
quantity. Some grosses scale indicates the general value of what it has measured.
Registering
The instruments merely indicate by numbers or some other symbols of discrete
increments the value of some quantity. For example, a water meter which uses
discrete numbers to indicate how much of water has been consume
Indicating
The instrument indicates, the value of the measured quantity using a calibrated
pointer and scale. For example some of instruments used in laboratory like use for
pressure gauge which uses a pointer and scale to indicate the value of the measured
quantity which is pressure in case of pressure gauge.
Recording
The instrument keeps a written record of measured quantity and usually it is
recorded against time.
On the basis of energy consideration we can classify instruments into two categories
Passive Instruments and Active Instruments. Passive instruments are those whose
output energy is supplied entirely almost entirely by its input signal or by the energy
of the input signal. These instruments do not need any auxiliary source of power
here. These instruments are Self Operated Instruments; it may be noted here, that
the output signal and the input signal may be of same form or they are may be an
energy conversion. Some of the examples of passive instruments are ordinary
mercury in glass thermometer or clinical thermometer, a bourdon tube, which is use
for measurement of pressure or a pitot tube.
On the other hand Active Instruments are those, which require an auxiliary source of
power. So, these not self operated instruments, but are Power Operated
Instruments. Again the output and input signals may be of the same form or there
may be an energy conversion involved. Examples of active instruments are electronic
amplifier differential transformer for displacement measurement, etc.
We can also classified the instruments on the basis of analog and digital mode of
operation, if the instrument follows analog mode of operation we call the
instruments, as Analog Types of Instruments or if the instruments follows digital
mode of operation, we call those as Digital Types of Instruments. Majority of the
primary sensing elements are of analog types. They present the information of about
the measure variable in the form of continuous variation with respect to time. On the
other hand digital types of instruments represent the measure variables by discrete
quantities or digital quantities, which are discrete in nature.
The next classification is based on whether the instrument is contacting type or non
contacting type. As the name suggest the instrument as contacting type, when it is
necessary to bring the instrument in direct contact with the measuring medium. For
example clinical thermometer, the ordinary clinical thermometer used to determine
the temperature of human body is a Contacting Type of Instrument. On the other
hand an optical pyrometer or radiation pyrometer measures the temperature of the
furnace; but you do not have to bring the pyrometer in direct contact with the
furnace which is an example of Non Contacting Type of Instrument.
Scheme-2
An instrument generally consists of the following functional elements:
i. Primary Sensing Element
ii. Variable Conversion Element
iii. Variable Manipulation Element
iv. Data Transmission Element
v. Data Presentation Element
result Pressure is developed within the bulb. The Temperature Signal is being
converted to a Pressure Signal. This is also a Variable Conversion Element. Both the
functions are performed by bulb. Thus it is a Primary Sensing Element and Variable
Conversion Element.
Static Characteristics are associated with static measurement. These are set of
criteria that are used when you measure a quantity or a condition that is either
constant or changes very slowly with time. So, Static Characteristics are those
characteristics which we must consider to analyze the performance of an instrument
i.e. measuring a medium which is constant or varying very slowly with time.
The Static Characteristics can be classified into two categories Desirable Static
Characteristics and Undesirable Static Characteristics. Under Desirable Static
Characteristics we have Accuracy, Sensitivity and Precision as various characteristics.
Similarly under Undesirable Static Characteristics we have Static Error, Dead zone
and Drift.
Desirable Static Characteristics Un-Desirable Static Characteristics
Accuracy Static Error
Reproducibility Drift
Sensitivity Dead Zone
Range:
The range of an instrument is the lowest and highest values it can measure within its
specifications.
Span:
The span of an instrument is the high end of the range minus the low end of the
range.
Example:
The lowest point of calibration is “a” units.
The highest point of calibration is “b” units.
The range of instrument is “a to b”.
The span of instrument is “ b-a”.
Resolution:
Resolution is the smallest amount of input signal change that the instrument can
detect reliably.
Accuracy:
Accuracy of a measurement describes how close the measurement approaches the
true value of the process variable. So, it is a measure of how close the measured
value is to the true value.
Accuracy can be expressed in many ways accurate within plus minus x percent
means accurate to within plus minus x percent of instrument span at all points of the
scale.
Accuracy can also be expressed in terms of percentage True Value which can be
expressed as Measured Value minus True Value divided by True value multiplied by
100.
% True Value = [{(Measured Value) – (True Value)}/ (True Value)]*100
Similarly, accuracy can also be expressed in terms of percentage Full scale deflection
and this can be represented as Measured Value minus True Value divided by
Maximum Scale Value multiplied by 100.
% True Value = [{(Measured Value) – (True Value)}/ (Maximum Scale Value)]*100
Static Error:
If, accuracy is measure of how close the measured value is to the true value static
error must be the difference between the measured value and the true value of the
quantity under static conditions. It is usually expressed as “+a units” or “-a units”.
Static error is the difference between the measured value and the true value of the
quantity.
True Value + Static Error = Instrument Reading
The static correction of an instrument is given as
True Value = Instrument Reading + Static Correction
Thus static error and static correction are related as
Static Correction = -Static Error
Reproducibility:
The reproducibility of an instrument is the degree of closeness with which a given
value may be repeatedly measured.
Drift:
Drift is the change in the indicated reading of an instrument over time when the
value of the measuring quantity remains constant. Drift can be a Zero drift or Zero
Error, Span drift or Sensitivity Drift, and finally Zonal Drift.
Zero Drift:
If the calibration of the equipment changes gradually by a same amount over a
period of time it is called as a Zero Drift. This can be seen in some of the instruments.
For example a pressure gauges. In a pressure gauge when there is no pressure input
to the instrument, the instrument still shows of small positive value which is a zero
error. We should take a note of this zero error, so that we can apply the correction
factor to the measured value being indicated by the instrument.
Span Drift:
A span drift involves a gradual change in which the calibration from zero upward
changes a proportional amount. This may be cause by gradual change in the spring
characteristics of the instruments.
Precession:
Precision is the Ability of an instrument to reproduce a certain set of readings with a
given accuracy.
Sensitivity:
It is defined as Ratio of change in the output or response of instrument to a change
of input or measured variable.
Dead Zone:
Dead Zone is the Largest range of values of a measured variable to which the
instrument does not respond. This is sometimes called dead spot or hysteresis. It
generally occurs due to friction in an indicating or recording instrument. The
Hysteresis is the characteristic loop we find when the instrument is calibrated first in
one direction and then, in the other direction this is caused by friction or backlash.
Dynamic Characteristics
Dynamic Characteristics are associated with dynamic measurements. Dynamic
Characteristics are those characteristics which we must consider if inputs are varying
with time.
Similar to static characteristic we have few Desirable Dynamic Characteristics and we
have few corresponding Undesirable Dynamic Characteristics. The Desirable dynamic
Characteristics are Speed of response and Fidelity and the undesired Dynamic
Characteristics are Lag and Dynamic Error.
1.8 Selection criteria for various measuring devices in chemical industry for
Temperature, Pressure, Flow measurement Liquid level
1.8.1 Selection criteria for various measuring devices in chemical industry for
Temperature
Selecting measuring devices for temperature in the chemical industry requires
careful consideration of several factors to ensure accuracy, reliability, and safety.
Some key criteria to consider are as below:
a) Principle of Measurement: On the basis of principle of measurement
appropriate temperature measuring device must be selected which are as
below:
Thermal Expansion
Solid Expansion Bimetallic Thermometer
Liquid Expansion Liquid in Glass Thermometer, Pressure
Thermometer
Gas Expansion Vapor Pressure Thermometer, Gas Thermometer
Thermostatic Sensor Thermocouple
Electric Resistance Resistance Temperature Detector (RTD)
Sensor Thermistor
Radiation Method Optical Pyrometer
Radiation Pyrometer
1.8.2 Selection criteria for various measuring devices in chemical industry for
Pressure
Selecting measuring devices for pressure measurement in the chemical industry
requires careful consideration of several factors to ensure accuracy, reliability, and
safety. Some key criteria to consider are as below:
a) Principle of Measurement: On the basis of principle of measurement
appropriate pressure measuring device must be selected which are as below:
Measurement of pressure by balancing Various Manometers
against a column of liquid of known
density
Balancing against a unknown force Piston Type, Ring Balance, Bell
Type Gauge
Balancing a force produced on a known Bourdon Tubes, Diaphragm Tube,
area against a stress in an elastic medium Bellows
Moderate Pressure Measurement
Device
Liquid Column Elements Barometers, Various Manometers
Mechanical Displacement Type Ring Balance manometer
Elastic Pressure Transducer Bourdon Tube,
Diaphragm Tube,
Bellows gauge
Electric Pressure Transducer Resistance Type, Inductive Type,
Piezoelectric Type etc.
Very High Pressure Measurement Electric gauge based on change in
Device resistance of Manganin or gold-
chrome wire.
1.8.3 Selection criteria for various measuring devices in chemical industry for Flow
Measurement
Selecting measuring devices for flow measurement in the chemical industry requires
careful consideration of several factors to ensure accuracy, reliability, and safety.
Some key criteria to consider are as below:
a) Principle of Measurement: On the basis of principle of measurement
appropriate flow measuring device must be selected which are as below:
Flow of fluid in closed pipe
Constant area – variable Orifice plate, venturi meter, pitot tube, flow
pressure drop nozzle
Variable area – constant Rotameter
pressure drop
Mass flow meter Coriolis
Flow of fluid through open Weir and Notches
channel
Type of flow Laminar, Turbulent and Transition Flow
1.8.4 Selection criteria for various measuring devices in chemical industry for Level
Measurement
Selecting measuring devices for level measurement in the chemical industry requires
careful consideration of several factors to ensure accuracy, reliability, and safety.
Some key criteria to consider are as below:
a) Principle of Measurement: On the basis of principle of measurement
appropriate level measuring device must be selected which are as below:
Direct Level Measurement Indirect Level Measurement
Dipstick Hydrostatic head type
Hook Type Purgle Type (Bubbler)
Sight Glass Capacitance Type
Float type Ultrasonic Type
Displacer Type Radiation Type
g) Reliability and Durability: One should select device which are more reliable
and highly durable. The longevity of the device is essential to minimize
replacement and maintenance costs.
h) Cost effectiveness: When selecting any level measuring device, the initial cost,
as well as long-term operating and maintenance expenses must be taken into
consideration. One should select devices that provide the best value over their
lifecycle.
i) Regulatory Compliance: Ensure that the selected devices meet relevant
industry standards and regulatory requirements for level measurement in the
chemical industry, such as ISO, ASTM, and ANSI standards.