3/8/24, 11:13 AM Selective Determination of Mercury(II) Ion in Water by Solvent Extraction Followed by Reversed‐Phase HPLC

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Selective Determination of Mercury(II) Ion in Water by Solvent Extraction

Followed by Reversed‐Phase HPLC

January 2004 · Journal of Liquid Chromatography & Related Technologies

27(11):1785-1798
DOI:10.1081/JLC-120037371

Authors:

Susumu Naomi Youichi

Ichinoki Kitahata Fujii

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Citations (54) References (10)

Abstract

A selective determination method for Discover the

mercury(II) ion in water by reversed‐ world's research
phase high performance liquid
25+
chromatography (HPLC) has been
million
developed. A water sample of 5 mL was
members
put into a 10‐mL centrifuge tube with a
stopper. Then, 1 mL of 2‐mol/L (M) 160+
acetate buffer solution of pH 5.5 was million
added into the centrifuge tube. After publication
mixing the contents, 1 mL of 0.5 M pages
tetrabutylammonium bromide (TBA‐Br) 2.3+
solution and 0.3 mL of 1‐octanol were
billion
added. A mercury ion was extracted into Join for free
citations
an organic layer by shaking the
contents for 10 min. The organic layer of
8 µL was injected into a C18 column
with an eluent of methanol/water/0.5 M
TBA‐Br (65:31:4, v/v), and the effluent
was monitored at 255 nm. The detected
mercury compound was estimated as
[(TBA)2 · HgBr4 ]. The correlation
coefficient of the calibration curves
(metal concentration vs. peak area),
obtained with 5 mL of mercury standard,
was more than 0.999 over the range of
10 ng/mL (ppb) to 10 µg/mL (ppm). The
detection limit of Hg ion in a 5‐mL
solution was 0.8 ppb, which
corresponded to three times the
standard deviation of the blank peak
area. Reproducibilities (RSD) of peak
areas for 5‐, 0.5‐, and 0.05‐ppm Hg ion
were 1.8%, 0.6%, and 0.6%,
respectively (N = 5). Recovery tests
were carried out by the presented HPLC
method with spiked river water samples.
The recoveries for 5‐, 0.5‐, and 0.05‐
ppm Hg ion were 99.5%, 102.9%, and
99.8%, respectively. Effects of foreign
ions on the method were investigated
with 0.2‐ppm Hg standard and 55 metal
ions. Tolerance limits of Be(II) and
Sc(III) were 20 ppm, and those of Bi(III)
and Pd(II) were 40 ppm. The other
metal ions of 100 ppm, or more, did not

https://www.researchgate.net/publication/244594554_Selective_Determination_of_MercuryII_Ion_in_Water_by_Solvent_Extraction_Followed_b… 1/16
3/8/24, 11:13 AM Selective Determination of Mercury(II) Ion in Water by Solvent Extraction Followed by Reversed‐Phase HPLC
interfere with the determination of
mercury(II) ion.

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Citations (54) References (10)

... The LOD and LOQ were 0.089 and 0.297

mg/L for Hg (II), and 0.042 and 0.143 mg/L
for As (III), respectively. Even though other
methods obtain low LODs for Hg (II) and As
(III) than those presented here, such as
HPLC [61] , Electrochemistry [62],
Fluorimetry [63], and Amperometry [64],
which present very low LODs for Hg (II),
and other methods also show low LODs for
As (III) such as arsenic detection based on
G-quadrupole complex method [65],
electrodes coated with gold nanoparticles
[66], colorimetric arsenic detection method
[67], electrochemical analysis utilizing
rGO/AuNPbased sensor platform [68], and
other advanced approaches for detecting
arsenic at trace levels [69], these methods
cannot be easily utilized in-field and are not
as portable. ...

A Portable Microfluidic Device-Based

Colorimetric Naked-Eye Sensors for…

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Mar 2024 · PLASMONICS
Zaidon T. Al-aqbi · Hassan Abdulsahib ·
Faris Aldoghachi

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... Therefore, developing reliable methods

for qualitative and quantitative
determination of these ions in aqueous
media is particularly interesting. Several
analytical techniques, including inductively
coupled plasma mass spectrometry [19,20],
inductively coupled plasma-atomic emission
spectrometry [21,22], atomic
absorption/emission spectrometry [18,23],

https://www.researchgate.net/publication/244594554_Selective_Determination_of_MercuryII_Ion_in_Water_by_Solvent_Extraction_Followed_b… 2/16
3/8/24, 11:13 AM Selective Determination of Mercury(II) Ion in Water by Solvent Extraction Followed by Reversed‐Phase HPLC
atomic fluorescence spectrometry [24][25]
[26], high-performance liquid
chromatography [27] , voltammetry [28],
and flame photometry [29] are used for the
determination of Hg and Cd ions. Despite
their excellent performance, these methods
require expensive apparatus, complicated
sample preparation, and are time-
consuming. ...

Simultaneous detection of mercury and

cadmium ions: A colorimetric method in…
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Behzad Pourbadiei · Bagher Eftekhari-Sis ·
Azadeh Kordzadeh · Ali Pourjavadi

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... Due to its non-biodegradable properties,

Pb 2+ is easily amplified through the food
chain and eventually enters the human
body. Traditional heavy metal ion detection
methods include the following:
spectroscopic analysis, including atomic
absorption spectroscopy (AAS) [15],
fluorescence spectroscopy [16,17], and
other methods [18][19][20][21][22], and
chromatographic analysis, including gas
chromatography (GC) [23] and high-
performance liquid chromatography (HPLC)
[24] . The main method of electrochemical
analysis is electrochemical sensing [25,26].
...

Surface Enhanced Raman Spectroscopy Pb2+

Ion Detection Based on a Gradient Boosting…

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Sep 2023
Minghao Wang · Jing Zhang

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... Mercury (Hg) is one of the most

hazardous metal ions for the environment,
and because it is distributed in air, water,
and soil, it poses the most common toxic
risks for human specially in contacting
areas as a result of natural processes.
Several methods for determining Hg 2+ ion
concentration have been reported, including
atomic absorption spectroscopy, inductive
coupled plasma mass spectrometry, high-
performance liquid chromatography coupled
with UV-Vis spectrometer, flame
photometry, and ion-selective electrode
[18] [19][20][21]. However, these methods
have limitations like time-consuming,
laborious procedures, and the requirement
of high-cost equipment [22]. ...

Nannorrhops ritchiana Leaf-Based

Biomolecular Extract-Mediated Silver…
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Feb 2023
Sehrash Khan · Shaukat Shujah · Umar
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... OES), atomic fluorescence spectrometry

(AFS), cold vapour atomic absorption

https://www.researchgate.net/publication/244594554_Selective_Determination_of_MercuryII_Ion_in_Water_by_Solvent_Extraction_Followed_b… 3/16
3/8/24, 11:13 AM Selective Determination of Mercury(II) Ion in Water by Solvent Extraction Followed by Reversed‐Phase HPLC
spectrometry (CVAAS), high-performance
liquid chromatography (HPLC), gas
chromatography, auger electron
spectroscopy and other methods are
currently used to detect Hg 2+ ions in the
aquatic medium [5] . These classic
methods are excellent in their performance,
but the tedious laboratory procedures and
expensive instruments complicate the use
of such methods. ...

Biofabrication of Silver Nanoparticles for

Selective and Sensitive Colorimetric Detectio…
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Dec 2022
K.S. Sreebamol · J. Devika · Gopinath Anu

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... An easy and short procedure was

conducted to investigate the efficiency of
Ag-NPs@AG as a rapid colorimetric sensor
to detect mercury ions in an aqueous
solution. A group of 5 mL glass vials was
arranged and filled with 3 mL of different
concentrations of mercury ions
(10,20,30, 40, 50,60,70,80,90, and 100
mg/L). It was shown that the yellow color of
AgNPs@AG disappeared rapidly after each
addition of silver nanoparticles to the
mercury solution, indicating that AG@NPs
worked as an efficient probe against
mercury ions in an aqueous solution. ...

catalysts-12-01464
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Nov 2022
Osama Zebari

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... An easy and short procedure was

conducted to investigate the efficiency of
Ag-NPs@AG as a rapid colorimetric sensor
to detect mercury ions in an aqueous
solution. A group of 5 mL glass vials was
arranged and filled with 3 mL of different
concentrations of mercury ions
(10,20,30, 40, 50,60,70,80,90, and 100
mg/L). It was shown that the yellow color of
AgNPs@AG disappeared rapidly after each
addition of silver nanoparticles to the
mercury solution, indicating that AG@NPs
worked as an efficient probe against
mercury ions in an aqueous solution. ...

Rapid Detection of Mercury Ions Using

Sustainable Natural Gum-Based Silver…
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Nov 2022
Samie Yaseen Zeebaree · Osama Ismail Haji ·
Aymn Yaseen Sharaf Zeebaree · Emad
Hameed Hanna

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... Nowadays, different techniques have

been used for the detection of Hg 2+ .
These include, inductively coupled plasma
mass spectrometry (Rodrigues et al. 2009),
atomic spectroscopy (Serafimovski et al.
2008;Shah et al. 2012), reverse-phase

https://www.researchgate.net/publication/244594554_Selective_Determination_of_MercuryII_Ion_in_Water_by_Solvent_Extraction_Followed_b… 4/16
3/8/24, 11:13 AM Selective Determination of Mercury(II) Ion in Water by Solvent Extraction Followed by Reversed‐Phase HPLC
liquid chromatography (Ichinoki et al.
2004) , electrochemical Zaib et al. 2015),
spectroelectrochemistry (Wang et al.
2016a(Wang et al. , 2016b, fluorescence
spectroscopy Sarkar et al. 2016), and
surface-enhanced Raman spectroscopy
(Kandjani et al. 2015;Song et al. 2020).
Time-consuming sample pretreatment
processes, high cost, and sophisticated
operations of the instruments, however, limit
their application as a standard assay for
monitoring of Hg 2+ (Hasan et al. 2020). ...

Biosynthesis of bifunctional silver

nanoparticles for catalytic reduction of organ…
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Jun 2022 · ENVIRON SCI POLLUT R
Melisew Tadele Alula · Mildred
Madingwane · Hongdan Yan · Markus Etzkorn

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... 12 Until now, trace level concentrations

of Hg 2+ have been conventionally detected
by surface resonance Raman scattering,
atomic absorption spectrometry, UV-vis
spectrometry, inductivelycoupled plasma
mass spectrometry, high-performance liquid
chromatography, atomic fluorescence
spectrometry, colorimetric analysis, capillary
electrophoresis, Auger-electron
spectroscopy, and polarography. [13][14]
[15][16][17][18][19] [20] [21] These methods
have inherent disadvantages like the need
for skilled operators, time-dependency, non-
portable instruments, high cost, poor
selectivity, and sensitivity. Hence the
development of a suitable approach for
determining Hg 2+ gains significant interest
among the researchers in the scientific
community. ...

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Benadict Joseph · Abhikha Sherlin V · Sea-
Fue Wang · Mary George

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... Spectroscopic assays include atomic

absorption spectroscopy (AAS) [11], atomic
emission spectroscopy (AES) [12], atomic
fluorescence spectroscopy (AFS) [13],
inductively coupled plasmamass
spectrometry (ICP-MS) [14], colorimetry
[15,16], and fluorescence spectroscopy
[17,18], among others. The main methods
of chromatography are gas chromatography
(GC) [19] and high-performance liquid
chromatography (HPLC) [20] . Although
these methods can achieve highly sensitive
detection for heavy metal ions, they also
have some disadvantages. ...

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based on surface-enhanced Raman scatterin…
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Peng Song · Guangda Xu · Lixin Xia

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https://www.researchgate.net/publication/244594554_Selective_Determination_of_MercuryII_Ion_in_Water_by_Solvent_Extraction_Followed_b… 5/16
3/8/24, 11:13 AM Selective Determination of Mercury(II) Ion in Water by Solvent Extraction Followed by Reversed‐Phase HPLC

... The existing routine toolbox available for

this goal mainly include techniques such as
atomic absorption/emission spectrometry
[9,10], inductively coupled plasma mass
spectrometry [11], atomic fluorescence
spectrometry [12], high-performance liquid
chromatography [13] , ion-selective
electrode and flame photometry [14]. A
series of new methods have also been
recently developed for the Hg 2+
determination, for example, fluorescence
[15] and Raman [16] spectra approaches
and electrochemical sensors [17]. ...

Tyndall-effect-enhanced supersensitive naked-

eye determination of mercury (II) ions with…
Article
Jun 2021 · SENSOR ACTUAT B-CHEM
Jinkun Huang · Xiaomei Mo · Haiyan
Fu · Yun Zhang

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... Conventional techniques for mercury (Hg

2+ ) detection including, atomic
absorption/emission/fluorescence
spectroscopy [22][23][24][25], high-
performance liquid chromatography (HPLC)
coupled with UV-visible or fluorescence
[26] , ion selective electrode (ISE), flame
photometry and inductively coupled plasma
mass spectrometry (ICP-MS) were widely
used [27][28][29][30][31][32][33]. Although
they offer high precision and accuracy,
these methods requires highly sophisticated
and expensive instrumentation, skilled
person and also time-consuming. ...

Naked-Eye Detection of Mercury Ions from

Morphological Transition of Silver Nanocube…
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Apr 2021
Jeevika Alagan · Ravi Shankaran Dhesingh

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... Among them, mercury (Hg) is considered

one of the most dangerous metal ions for
the environment and has most commonly
toxic risks for human contacting areas as a
result of natural processes, because it is
widely distributed in air, water and soil [31].
There are several methods such as
inductive coupled plasma mass
spectrometry (ICPMS) [32], atomic
absorption spectroscopy (AAS) [33] , high-
performance liquid chromatography (HPLC)
coupled with UV-vis [34], and ion-selective
electrode (ISE) and flame photometry [35]
are being reported for the determination of
Hg 2+ ion. However, these methods have
limitations with respect to several factors
such as time-consuming, complex
procedures, and need high-cost types of
equipment. ...

Green synthesis of khat mediated silver

nanoparticles for efficient detection of mercu…
Article Full-text available
May 2020
Meresa Girmay Tsegay · Henok Gidey
Gebretinsae · Juliet Sackey · Zebib Yenus

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3/8/24, 11:13 AM Selective Determination of Mercury(II) Ion in Water by Solvent Extraction Followed by Reversed‐Phase HPLC
(Z Y) Nuru

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... Thus, to get rid of the hidden risk, a

particular reliable method is necessary for
the monitoring of mercuric ion and removal
(or degradation) of organic pollutants in
their earliest propagation stage. Hopefully,
the regular endeavour of scientists has
been able to develop some ultrasensitive
conventional destructive methods for the
detection of mercuric ions at the trace level,
such as inductively coupled plasma mass
spectrometry (ICPMS), 11 atomic emission
spectrometry (AES), 12 flame photometry,
13 atomic fluorescence spectrometry (AFS),
14 high-performance liquid chromatography
(HPLC), 15 and ion selective electrode
(ISE). In this connection, additionally, we
would like to mention that fluorescence
techniques also get the attention in sensing
research and many outstanding articles
have been published by scientists for
detecting copper ion, mercuric ion,
coumarin, and MoS 2 . ...

A compact prospective investigation on

colorimetric recognition of Hg2+ ion and…
Article
Oct 2019
sharmistha Bera · Anukul Maji · Somnath
Das · Maidul Hossain

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... Liang Electrochemical method [86] 6 0 n

M . L −1 20-250 nM.L −1 Solvent extraction
followed by reversed phase HPLC [87] 0.8
nM.L −1 10-100 nM.L −1 HPLC/ICP-MS [88]
0.4 nM.L −1 2.5-250 nM.L −1 RRS
technique using dsDNA-Au NPs [85] 0.4
nM.L −1 2.5-60 nM.L −1 RRS technique
using Au NPs-HAuCl 4 [84] 3 n M . L −1 8-
1330 .L −1 [92] 62nM .L −1 0.13-1.12 ...

Gold and silver nanoparticles in resonance

Rayleigh scattering techniques for chemical…
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Sep 2019 · MICROCHIM ACTA
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... Therefore, design of competent tools for

selective and sensorial tracking out of these
two metal ions has become inevitable
nowadays. In this context, the most familiar
and highly sensitive methods available for
the determination of these two ions are
Inductively Coupled Plasma Mass
Spectrometry (ICPMS) [9], Atomic
Absorption/Emission Spectrometry
(AAS/AES) [10], Atomic Fluorescence
Spectrometry (AFS) [11], High-Performance
Liquid Chromatography (HPLC) [12] and
Ion Selective Electrode (ISE) [13] etc.
However, these techniques are found to
suffer from short route sample preparation,
cost saving, easy operation, and even
restricted to on-site real-time in-situ
detection of metal ions. ...

https://www.researchgate.net/publication/244594554_Selective_Determination_of_MercuryII_Ion_in_Water_by_Solvent_Extraction_Followed_b… 7/16
3/8/24, 11:13 AM Selective Determination of Mercury(II) Ion in Water by Solvent Extraction Followed by Reversed‐Phase HPLC
A sensorial colorimetric detection method for
Hg2+ and Cu2+ ions using single probe sens…
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Apr 2019
Mt. Nasima Aktara · Somnath Das · Sk
Nayim · Maidul Hossain

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... By taking into account of severe

disadvantages of mercury contaminations, it
is crucial to develop a sensitive, selective,
economical and quick response method for
quantitative determination of Hg 2+ ion in
aqueous medium. In past few decades, the
number of methods has been reported for
the detection of Hg 2+ ion namely high
performance liquid chromatography [29] ,
flame photometry [30], stripping
voltammetry [31], X-ray fluorescence
spectrometry [32], atomic absorption
spectrometry [33], ion selective electrodes
[34] and spectrophotometry [35]. The time
consuming process to prepare samples and
high cost of instrumentation are the hurdles
to use these techniques to achieve results
in short time. ...

Gallotannin mediated silver colloidal

nanoparticles as multifunctional Nano…
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Balasaheb Daniyal Vanjare · Ki Hwan Lee

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... Consequently, the environmental concern

about regulating this contaminant demands
the development of new mercury detection
methods that are cost-effective, rapid and
facile in nature [8]. Certain conventional
techniques such as atomic absorption
spectroscopy (AAS) [9], inductive coupled
plasma mass spectrometry (ICPMS) [10],
high performance liquid chromatography
(HPLC) [11] , ion selective electrode (ISE)
and flame photometry [12] are currently
used for the determination of Hg 2+ .
Electrochemical analysis is demonstrated
as an excellent tool in terms of device
operation, cost of instrumentation and
instantaneous application. ...

Functionalized Silver Nano-Sensor for

Colorimetric Detection of Hg2+ Ions: Facile…
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Chandan Shivamallu

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... Thus, the easy detection of Hg 2+ is very

important to increase the consciousness of
human. The various technologically sound
process are applying to detect Hg 2+ ion
aqueous medium such as high-performance
liquid chromatography (HPLC) [7] , atomic
absorption or emission spectrometry (AAS
or AES) [8], flame photometry [9], inductive
coupled plasma mass spectrometry

https://www.researchgate.net/publication/244594554_Selective_Determination_of_MercuryII_Ion_in_Water_by_Solvent_Extraction_Followed_b… 8/16
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spectrometry (AFS) [11]. ...

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... Hg (II) is widely distributed in water, air,

soil and dairy foods [29][30][31][32][33] and
long-term exposure to that causes serious
health problems within the brain, kidneys,
heart, lungs, central nervous system (CNS)
and immune system to all human kinds and
animals of all ages [34][35][36]. Up to date,
numerous methods have been reported for
detection of Hg (II) including atomic
absorption spectrometry [37], stripping
voltammetry [38], inductively-coupled
plasma atomic emission spectrometry [39],
high-performance liquid chromatography
(HPLC) [40] and ion selective electrode
(ISE) and flame photometry [41]. However,
employment of these techniques is
thoroughly limited due to their high
operation expenses and sophisticated
instructions. ...

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... Optical sensors especially the fluoro-

sensors due to their emission behaviour,
easy signals detection, low costs, sensitivity
and selectivity offer many advantages over
other systems in this area of toxic metal
detection [20][21][22][23][24][25]. In recent
years much attention has been given to the
recognition and detection of Hg 2+ via
fluorescent chemosensors [5,[26][27][28]
replacing the costly and sophisticated
instrumental detection tools such as high-
performance liquid chromatography (HPLC)
[29] , inductively coupled plasma mass
spectrometry (ICPMS) [30][31][32][33], and
atomic absorption/emission spectrometry
(AAS/AES) [34][35][36]. ...

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... Several conventional methods such as

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coupled plasma mass spectrometry

https://www.researchgate.net/publication/244594554_Selective_Determination_of_MercuryII_Ion_in_Water_by_Solvent_Extraction_Followed_b… 9/16
3/8/24, 11:13 AM Selective Determination of Mercury(II) Ion in Water by Solvent Extraction Followed by Reversed‐Phase HPLC
(ICPMS) [24,25], high-performance liquid
chromatography (HPLC) coupled with UV-
vis or fluorescence [26] , ion selective
electrode (ISE) and flame photometry [27]
are being used for the determination of Hg
2+ . However, these methods have
limitations with respect to several factors
such as time-consuming for sample
preparation, complex procedures, and
special technical support and needs high
cost equipments. ...

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visual colorimetric sensing of mercury
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... A number of methods to detect trace

concentrations of Hg 2+ in different samples
have been explored, such as circular
dichroism 17 , high performance liquid
chromatography (HPLC) [18] [19] ,
inductivelycoupled plasma mass
spectrometry (ICP-MS) 20-21 ,
electrochemical method and atomic
absorption/emission spectrometry
(AAS/AES) 22-26 , atomic fluorescence
spectrometry (AFS) 27-28 , flame
photometry (FP) and ion selective electrode
(ISE) 29 . However, all of these procedures
have limitations that include the need for
sophisticated instrumentation and technical
expertise, as well as long analysis time. ...

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3/8/24, 11:13 AM Selective Determination of Mercury(II) Ion in Water by Solvent Extraction Followed by Reversed‐Phase HPLC

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