iCAP 6000 Series

ICP-OES Spectrometer

Reference Guide

Site pre-installation guide

Instrument overview
Instrument safety information
Pre-installation checklist

Thermo Fisher Scientific Page 1 of 38 iCAP 6000 Reference Guide v 1.2

© April 2011 Thermo Fisher Scientific Inc.
www.thermoscientific.com
8499 400 90031

Sales contact:

Service contact:

Thermo Fisher Scientific Page 2 of 38 iCAP 6000 Reference Guide v 1.2

 Purpose of this document

This document provides the following

 A brief introduction to the iCAP 6000 Series of

instruments, including a list of common accessories
available for your instrument

 Details of where to find further information about using

your instrument

 Pre-installation Guide - Important information on what

preparations need to be made before you receive your
instrument

 Important safety information

 EC Declaration of conformity

 Checklist to ensure that your lab is ready before your

instrument arrives

Thermo Fisher Scientific Page 3 of 38 iCAP 6000 Reference Guide v 1.2

Thermo Fisher Scientific Page 4 of 38 iCAP 6000 Reference Guide v 1.2
 Contents
1 Introduction to the iCAP 6000 Series .................................... 7
1.1 Overview.................................................................................. 7
1.2 Further information ................................................................. 8
1.3 User Guide............................................................................... 8
1.3.1 Hardware Manual .............................................................. 8
1.3.2 iTEVA Help ...................................................................... 9
1.3.3 Online ............................................................................... 9

2 System Accessories................................................................... 9

3 Pre Installation Guide ........................................................... 11

3.1 Transportation ....................................................................... 11
3.1.1 Package Size ..................................................................... 11
3.1.2 Short Term Storage.......................................................... 11
3.1.3 Transit Damage ............................................................... 12
3.1.4 Warranty.......................................................................... 12
3.2 Working Area Requirements .................................................. 12
3.2.1 Introduction..................................................................... 12
3.2.2 Before installation ............................................................ 13
3.2.3 Location........................................................................... 13
3.2.4 Environmental Requirements........................................... 14
3.2.5 Electrical .......................................................................... 16
3.2.6 Spectrometer Size............................................................. 17
3.2.7 Gas Requirements ............................................................ 18
3.2.8 Gas Consumption ............................................................ 18
3.2.9 Water Temperature Control ............................................ 19
3.2.10 Waste Storage ................................................................ 19
3.2.11 Spectrometer Fume Extraction....................................... 19
3.2.12 Sample Fume Extraction ................................................ 21
3.3 Communications Interface..................................................... 22
3.3.1 On the Spectrometer........................................................ 22
3.3.2 On the Data Station......................................................... 22

4 Safety....................................................................................... 23
4.1 iCAP 6000 Safety................................................................... 23
4.2 iCAP 6000 Sicherheit............................................................. 27
4.3 Sécurité pour iCAP 6000 ....................................................... 30

5 EC Declaration of Conformity.............................................. 33

6 Special Agreements................................................................ 35

7 Pre-Installation Checklist...................................................... 37

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Thermo Fisher Scientific Page 6 of 38 iCAP 6000 Reference Guide v 1.2
 1 Introduction to the iCAP
6000 Series

1.1 Overview The iCAP 6000 Series is a range of Inductively Coupled Argon Plasma
Optical Emission Spectrometers (ICP-OES) which use an Echelle
optical design and a Charge Injection Device (CID) solid-state detector
to measure trace elemental concentrations in a wide range of samples.
Most samples are liquids that are pumped through a nebuliser to
produce a fine spray. The large droplets are removed by a spray
chamber and the small droplets then pass through to the plasma. The
solvent is evaporated and the residual sample decomposes to atoms and
ions that become excited and emit characteristic light which is
measured and corresponds to the concentration of each element type in
the original sample.
Control of the spectrometer is provided by PC-based iTEVA software.
To avoid loss of analytical performance and compromising safety only
Thermo Scientific specified parts should be used.

The iCAP 6000 spectrometer consists of several major components:

 plasma torch and sample introduction parts
 radio frequency power generator
 optical system
 CID detector with thermoelectric cooling

Warning: Before operating your iCAP ensure you read and understand
all the safety information at the end of this document. ▲

To comply with safety and warranty requirements, the iCAP 6000,

accessories and associated equipment must be installed by a Thermo
Scientific-trained and certified engineer.

Specific site requirements are required for the iCAP 6000. Please see
the Working Area Requirements section below for details.

Thermo Fisher Scientific Page 7 of 38 iCAP 6000 Reference Guide v 1.2

 1.2 Further Detailed information on laboratory requirements for your iCAP 6000
series ICP-OES spectrometer can be found the Pre-installation Guide
information
section later in this document.

Help with running your instrument, including narrated tutorials and

comprehensive software user guides can be found in the iTEVA Help
topics (see screenshot below).

Figure 1. iTEVA Help topics screenshot

1.3 User Guide The user guide includes basic information required to get you started
with operating your iCAP 6000. More advanced operating instructions
can be found in the Hardware Manual, and from the iTEVA software’s
built-in Help.

1.3.1 Hardware The Hardware Manual details the operation and maintenance of your
Manual instrument hardware. It also includes full information about the safety
hazards involved in working with the spectrometer and its accessories,
and the means by which such hazards can be minimised. This manual is
supplied in Adobe PDF format on the Supplementary Information CD
supplied with your instrument.

Note: ensure you have read and understood all the safety instructions
contained at the end of this document before operating your iCAP.

Thermo Fisher Scientific Page 8 of 38 iCAP 6000 Reference Guide v 1.2

 1.3.2 iTEVA Help As mentioned above, the iTEVA Software has its own active Help
system that describes features and functions of the software. This can be
accessed by clicking on Help Topics from the Help dropdown menu
(shown below) Relevant help topics for particular areas of the software
can also be found by pressing the F1 key at any time.

Figure 2. Help Topics in iTEVA

1.3.3 Online For information about Thermo Scientific and your iCAP 6000 Series
ICP-OES Spectrometer, including application notes and other material
visit the Thermo Scientific website:
www.thermoscientific.com/ICP
www.thermoscientific.com/iTEVA-software

2 System Accessories
Required:
 Recirculating chiller unit (see specification below)
 Data Station (see specification below)

Optional:
 Cetac ASX-520 Autosampler (requires dedicated RS232 on Data
Station)
 Cetac ASX-260 Autosampler (requires dedicated RS232 on Data
Station)
 Cetac EXR-8 Autosampler (requires dedicated RS232 on Data
Station)
 Cetac ASX 1400 Autosampler (Stirring)
 Cetac U-6000AT+ Ultrasonic Nebuliser
Thermo Fisher Scientific Page 9 of 38 iCAP 6000 Reference Guide v 1.2
  Elemental Scientific, Inc. SC SC4 Autosampler
 Elemental Scientific, Inc. SC4 Fast Autosampler
 Argon Humidifier
 SSEA – Solid sampling device (requires dedicated RS232 on Data
Station and iCAP 6000 accessory board)
 Laser – Solid sampling device (requires dedicated RS232 on Data
Station and iCAP 6000 accessory board)
 High Solids Sample Introduction kit
 HF Acid Sample Introduction kit
 Organics Sample Introduction Kit
 Volatile Organics Sample Introduction kit
 iTEVA Security Software
 iCAP Validator Package

Please request site requirement guides for any purchased accessories.

Thermo Fisher Scientific Page 10 of 38 iCAP 6000 Reference Guide v 1.2

 3 Pre Installation Guide

3.1 Transportation The spectrometer is supplied with all compatible accessories that have
been purchased to meet the customer's system requirements. Items may
be shipped in separate packages.

WARNING: All items should be transported to the installation site on

pallets, in their original packaging and the right way up. Under no
circumstances may any package be moved without its pallet unless
under the direct control of an authorised Thermo Fisher service
engineer.
Proposed routes from the customer receiving area to the installation
site must be checked for suitability. The largest pallet size should be
used to calculate clearances.

WARNING: The boxed Spectrometer should be moved using a

mechanical lift. Care should be taken in doorways, corridors or when
lowering to avoid trapping fingers.

3.1.1 Package Size The instrument will be supplied inside especially designed packaging.
The dimensions are shown in the table below.

Width Depth Height Weight

980 mm 900 mm 920 mm 105 Kg
(38.6 in) (35.4 in) (36.2 in) (230 Ib)

Table 1. Packaged Dimensions and Weight

Transportation to some destinations may necessitate additional

packaging, for example a packing crate. Dimensions and exact
specifications may vary.

3.1.2 Short Term To maintain the instrument in serviceable condition and to comply
Storage with the conditions of warranty, ensure that storage of each item is
maintained within the stated parameters detailed for the Working Area
Requirements below. Make sure that the packages are stored the
correct way up.

Thermo Fisher Scientific Page 11 of 38 iCAP 6000 Reference Guide v 1.2

 Note: Do not open the Packages without the permission of the
Thermo Fisher-trained engineer

When the packages are opened prior to installation, the contents will be
checked against the packing list(s).

3.1.3 Transit Before accepting delivery of any equipment, the packages should be
Damage inspected for signs of obvious damage. The nature of the damage
should be noted on the delivery notice and signed by the carrier's
representative.
Within the time stated in the Thermo Fisher terms and conditions an
inspection should be made for concealed damage. The local Thermo
Fisher organisation should be advised of any damage in writing and, on
receipt of specific instructions, the customer should return the
equipment complete and in the original packing material.

3.1.4 Warranty Note that the instrument is warranted against defects in material and
workmanship for a period of 12 months from installation, or 15
months from shipment, whichever comes first. This warranty does not
cover damage sustained as a result of improper storage by the
customer prior to installation, or resale to a third party.
Note: Warranty is not transferable to a third party without written
approval from Thermo Fisher Scientific.

3.2 Working Area It is critical that certain requirements are met before an
Requirements installation engineer arrives on site. Failure to do so may
result in delays to installation

3.2.1 Introduction This section is designed to help ensure that your iCAP 6000 Series ICP-
OES Spectrometer will be installed efficiently and will be able to meet
your requirements quickly and completely.
It will minimise installation time if the services and facilities detailed
here are available before the equipment is delivered.
Properly installed and maintained, your system will provide you with
years of reliable service. Please inform your local Thermo Fisher
organisation what aspects of support are most important to you and a
tailored agreement can be provided to prolong the life of your
instrument.
This section describes the environment and the resources
required at the installation site of the iCAP 6000 Series ICP-OES
Spectrometer and associated equipment. Safety requirements for
the installation are also detailed.

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 Warning: The installation of all services must comply with the
appropriate rules and regulations required by the local authorities
responsible for those services in the workplace. An installation
engineer is not responsible for the fitting or compliance of the
facilities or services.
The choice of an operating site for the instrument will be influenced by
local considerations for example, ease of access and availability of
electrical power.
Logical planning of the installation can save both time and money. The
objective of this manual is to provide information that will enable the
best site to be chosen and to highlight the essential requirements.
If further information or advice is required, contact your local Thermo
Fisher organisation. A list of Thermo Fisher organisations and agents
can be found at www.thermoscientific.com.

Installation of the system will include some familiarisation training;

however comprehensive method development and software training
will require additional training that should be ordered separately.
Pre-installation visits can be made on request, but may be chargeable.

3.2.2 Before Prior to installation make sure that the proposed area is compatible
installation with the conditions specified. The laboratory must offer a dry, even
temperature and dust-free conditions, with no possibility of
condensation forming. Sample preparation activities and corrosive
materials should be located in a separate room to avoid problems due
to corrosive fumes.
A comprehensive ‘Risk Assessment’ should be carried out that is
specific to the handling of solvents, samples and sample preparation.
Particular consideration should be taken to avoid direct sunlight,
proximity to heat sources, draughts and vibration. Do not locate the
system where sudden changes in temperature can occur, for example
near a door or window, care should be taken with the location of
items such as air conditioning vents and heating vents.

3.2.3 Location The choice of site will be influenced by the dimensions and weights of
the spectrometer and accessories. Other factors are the environment
and the availability of electricity, water and gas supplies, as well as the
need for a suitable ventilation system to dispose of the exhaust gases.
All of these factors are covered in the following sections.
The instruments are designed for use on a normal laboratory bench.
Ideally the instrument should be placed on a moveable bench with 0.5
meters of access behind the instrument. The mounting surface must be

Thermo Fisher Scientific Page 13 of 38 iCAP 6000 Reference Guide v 1.2

 level and the instruments must not be placed on any type of cushioning
as this could block ventilation.
The mounting arrangements should be capable of supporting the
weight of the spectrometer and its accessories. Make sure that the
working surface is sufficiently rigid to prevent vibration as this may
affect the optical alignment of the spectrometer and accessories.
To avoid the possibility of liquid ingress into the top of the
spectrometer the location should ensure it is not possible to store
sample or other liquids directly above the instrumentation.
Organic or volatile solvents should not be stored, even for a short time,
near the instrument.
Do not position the equipment so that it is difficult to operate the
extraction, electrical supply, cooling water, purge gas and plasma gas
controls.

3.2.4 Environmental The atmospheric temperature requirement is 15 to 35°C (60 to 95°F),

Requirements the temperature should not change by more than 2°C per hour.
Atmospheric humidity should be 20 to 80% m/v for an ambient
temperature between 15 and 30°C and 20 to 60% m/v for an ambient
temperature between 30 and 35°C. Atmospheric conditions must be
non-condensing. The instrument room should be at a positive pressure
with respect to rooms with a corrosive atmosphere.
Warning: Argon is an asphyxiant; if the extraction is turned off
sufficient air must be supplied to prevent the concentration of argon
reaching a harmful level.

Thermo Fisher Scientific Page 14 of 38 iCAP 6000 Reference Guide v 1.2

 In order to ensure optimum analytical performance, reliability and
longevity of your iCAP 6000 Series product it is important that a
number of basic laboratory considerations are observed as listed in the
table below:

Consideration Why is this aspect important?

General The environmental conditions of the
environmental laboratory should be maintained in compliance
conditions of the with Good Laboratory Practice (GLP) to
laboratory ensure a clean and safe work environment for
laboratory personnel.
Appropriate The iCAP, as with all ICPs, draws air through
placement of the the unit as a source of cooling. If the
instrument with laboratory air contains a high content of
availability of a clean particulates, exhibits high humidity and/or is
air supply contaminated with corrosive gases this could
lead to premature corrosion, component failure
and aging of the instrumentation.
Appropriate Liquid autosamplers should be installed to
placement of sample ensure that there is sufficient air clearance
introduction around the base of the iCAP instrument. It is
accessories when also recommended that a cover and/or
working with appropriate extraction is utilised in association
corrosive or volatile with this accessory when working with
liquids corrosive/volatile liquids.
Placement of sample Sample preparation accessories should be
preparation installed and operated in an area which is
accessories if completely separated from the instrument
working with acids or laboratory when performing operations with
volatile liquids corrosive or volatile matrices.
Chemical storage and It is recommended that the handling of
spillage control chemicals and reagents is kept to a minimum
in the instrument laboratory. Any chemical or
reagent spillages should be cleaned up
immediately to reduce contamination of the
laboratory air. All chemicals and reagents
should be handled and stored externally to the
instrument laboratory and in accordance with
the appropriate MSDS documentation.
Handling of If handling flammable liquids, the operator
flammable liquids should be aware of the basic standards which
apply to safe handling and storage of such
materials. It is recommended that procedures
to prevent accidents and protect people from
the hazards of flammable substances are put in
place.

Table 2. Laboratory Considerations

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 The spectrometer will require an electrical supply at 200 to 240 VAC
3.2.5 Electrical
4 kVA 50/60 Hz. The spectrometer will be supplied with a 2.5 m
mains cord.
For customers in the USA and Canada the mains cord supplied will
terminate in a NEMA L6-20P Twist&Lock plug. (Coding is black (X –
AC high), white (Y – AC low), green (G – earth/ground).

Figure 3. NEMA L6-20P plug for USA/Canada

For customers in the rest of the world the mains lead is shipped with
no terminating plug, but with wires ready for a suitable 20 A plug.
Coding is blue (neutral), brown (live), green/yellow (earth/ground).
Connection to the laboratory supply should be with an appropriately
rated plug conforming to local electrical guide lines and local
requirements. It must be possible to electrically isolate the
instrumentation.
Additional standard mains sockets will be required for the Data Station
PC, and for an autosampler, chiller, printer or any other additional
accessory required.
Each electrical outlet must have an effective earth/ground connection.
This protection must not be negated by the use of an extension cable
without a protective earth conductor.

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 3.2.6 Spectrometer Width Depth Height Weight
Size
832 mm 744 mm 589 mm 92 Kg
(32.7 in) (29.3 in) (23.2 in) (203 lbs)

Table 3. Spectrometer Dimensions and Weight

831.2mm

Figure 4. iCAP 6000 Series Front View

510mm

Figure 5. iCAP 6000 Series Top View

Thermo Fisher Scientific Page 17 of 38 iCAP 6000 Reference Guide v 1.2

 3.2.7 Gas The spectrometer will require argon at 5.5 bar (80 psi) (minimum
Requirements quality of 99.995 % pure with less than 10 ppm water and less than
10 ppm oxygen - used for operation and optical path purge). The
maximum flow requirement will be 25 l/min during installation
For purging the optical path in the spectrometer the same argon
supply can be used, or nitrogen at 1.0 bar (15 psi) (minimum quality of
99.995% pure with less than 10 ppm water and less than 10 ppm
oxygen) can be used instead of argon. The maximum flow requirement
will be 15 l/min during installation. For optimum performance, a
quality of 99.998% pure nitrogen is recommended.
If an additional gas accessory is required (optional), clean oil-free air is
required at a pressure of 2.5 bar (35 psi) and a flow of approx 100
ml/min.
The instrument will be supplied with two 3 m lengths of plastic tubing
(6 mm outer diameter Polyolefin) for the purge and the plasma gas.
Connection to the laboratory gas supply should be within 1 m of the
instrument. A regulator should be close to the connection. The
instrument will be supplied with particulate gas filters and these must
be correctly fitted and maintained.
Care should be taken to ensure that laboratory gas lines do not
contaminate the gases used for the iCAP.
If liquid argon is not used it is recommended that banks of cylinders be
used with switch over valves so that the gas supplies can be used
continuously.
Warning: Nitrogen and argon gas may cause asphyxiation at high
concentrations; appropriate care should be taken.

PLEASE NOTE: GAS REQUIREMENTS ARE

NOT THE SAME AS FOR PREVIOUS
THERMO ICP SPECTROMETERS.
3.2.8 Gas The gas consumption of an iCAP 6000 instrument varies with plasma
Consumption conditions and purge operating parameters. The table below shows the
approximate gas consumption for plasma gas and purge gas at different
conditions.
Purge gas Plasma gas (cool + aux + neb)
(6300 and 6500 instruments only*) min - max
Trickle 1.2 l/m iCAP 6200 12 – 15 l/m
Normal 3.2 l/m iCAP 6300 12 – 15 l/m
Boost 5 l/m iCAP 6500 10 – 23.5 l/m

Table 4. Typical iCAP gas consumption

*Note that a 6200 instrument does not use purge gas but requires
1.2 l/m for plasma interface gas.
Thermo Fisher Scientific Page 18 of 38 iCAP 6000 Reference Guide v 1.2
 3.2.9 Water A recirculating chiller should be used to remove waste heat from the
Temperature spectrometer. The water temperature should be set to 5 °C below the
Control ambient temperature (and must be set between 15 °C and 30 °C).
The water used in the chiller must be distilled or deionised water
containing 5 % by volume of the correct inhibitor (included with a
new instrument and a maintenance kit which can be ordered from your
local Thermo Fisher organisation. See consumables listing at the end of
this document).
Temperature variation must be less than 0.2 °C per hour
The flow requirement of the spectrometer is 5 l/min and a cooling
capacity in excess of 900 W.
The chiller must provide 50 micron particulate filtration.
A suitable chiller (ThermoFlex 900) can be supplied from your local
Thermo Fisher organisation.

The spectrometer will be supplied with plastic connecting tubing that

has a 12 mm outside diameter.
Connection to the water chiller should be within 3 meters of the
instrument, or insulated tubing must be used.

3.2.10 Waste Storage The analysis of a sample, by ICP-OES, usually involves production of a
fine mist from a liquid sample. Waste will be produced that could be
corrosive and toxic, or an organic solvent.
An appropriate container is required that is solvent proof, shatterproof
and vented away from the instrument. Ensure the waste container does
not constitute a spill or trip hazard. It may be necessary to neutralise
waste to prevent any toxin build up. Appropriate facilities should be
provided for the disposal of any waste which should be disposed of
following local procedures and regulations.

3.2.11 Spectrometer This instrumentation is designed for operation in clean air

Fume conditions. The laboratory must be free of all contaminants that could
Extraction have a degrading effect on the instrument components.
Dust, acid and organic vapours must be excluded from the work
area. The warranty will be void if the equipment is operated in sub-
standard conditions.
WARNING: The spectrometer must never be operated without an
effective fume extraction system attached to the torch compartment
chimney.

Thermo Fisher Scientific Page 19 of 38 iCAP 6000 Reference Guide v 1.2

 Hot fumes, which may be corrosive and toxic, are discharged from the
instrument chimney during operation. To ensure a safe working
environment and safe removal of waste combustion products, an
effective extraction system must be installed, this should include
appropriate filtering of hazardous toxic fumes.
The extraction must be set to the following, measured in the centre of
the extraction tube at the spectrometer end, while disconnected from
the instrument, as shown in figure 6 below. The extraction tube has
an inlet diameter of 125 mm (5 in).

An iCAP 6000 Duo instrument will require an

extraction of 10 m/s (33 ft/s; 22.4 mph).
An iCAP 6000 Radial instrument will require an
extraction of 5 m/s (16 ft/s; 11.2 mph).
The extraction flow must be adjustable to enable the installation
engineer to correctly set the flow and achieve the required extraction.
This can be achieved with a butterfly valve, or an adjustable gate as
shown in figure 6 below.
The extraction system must not be affected by external weather
conditions or other uses the system may be used for.

Extraction fan specification varies depending on lab

layout, and lengths, diameters and type of tubing
required to reach the instrument. Consult a qualified
extraction specialist to ensure that the correct flow is
achieved at the instrument.

Thermo Fisher Scientific Page 20 of 38 iCAP 6000 Reference Guide v 1.2

 Measure flow rate at
instrument end of
extraction system

Figure 6. iCAP 6000 Extraction System

PLEASE NOTE: EXTRACTION

REQUIREMENTS ARE NOT THE SAME AS
FOR PREVIOUS THERMO FISHER ICP
SPECTROMETERS.

3.2.12 Sample Fume Additional, separate, extraction should be considered if significant

Extraction numbers of volatile, or acidic, samples are left in the proximity of the
instrumentation. If an autosampler is used with volatile or acidic
samples a separately vented enclosure should be used.

Thermo Fisher Scientific Page 21 of 38 iCAP 6000 Reference Guide v 1.2

3.3 Communications An Ethernet connection is used between the instrument and a
computer for Data Station communication. Therefore, if the Data
Interface
Station computer is connected to a local area network, an additional
Ethernet port is required for connection to the instrument.
3.3.1 On the
Spectrometer Note: The Instrument Ethernet port must be configured to allow it to
communicate with the instrument.
Any firewalls installed on the PC must be disabled for the Instrument
Ethernet adaptor, or alternatively configured to allow the
appropriate instrument communications socket traffic. The
Ethernet adaptor is dedicated to the instrument and will not be
connected to any other networks, therefore there is no security risk
associated with allowing communication via the Instrument Ethernet
adaptor.
The IP address of the Instrument Ethernet adaptor will by default be
configured by the installation engineer to 90.0.0.1. The Instrument IP
address will be 90.0.0.50.
An optional accessory control PCB may be fitted for additional
communication requirements for some accessories. The use of each
connection is specified in the user manuals for each accessory.

The Data Station requirements will normally be met by a PC meeting

3.3.2 On the Data the minimum specification:
Station
 Windows XP Professional (Service pack 3 or higher) or Windows 7
Professional 32 bit
 20 GB Hard drive
 512 MB RAM
 Dedicated Ethernet card for spectrometer communication
 Some accessories require a dedicated RS232 port
 A separate Ethernet card will be required for networking
 A printer port maybe required
A suitable PC is available from your local Thermo Fisher organisation.
The installation engineer is not responsible for network and customer
specific set-up of the PC.

Thermo Fisher Scientific Page 22 of 38 iCAP 6000 Reference Guide v 1.2

 4 Safety

4.1 iCAP 6000 Read this chapter carefully before installing and operating the
instrument and its accessories. The safety standards contained in this
Safety
manual comply with the requirements of the Health and Safety at Work
Act 19741 as published by the United Kingdom Health & Safety
Executive (HSE).

4.1.1 Introduction The instrument and accessories described in this manual are designed
to be used by properly trained personnel only. Any adjustment and
repair of this equipment must only be carried out by a Thermo
Scientific certified field service engineer who is aware of the hazards
involved.

1
www.hse.gov.uk/legislation/hswa.htm
Thermo Fisher Scientific Page 23 of 38 iCAP 6000 Reference Guide v 1.2
 E

4.1.2 Safety For the correct and safe use of the instrument and its accessories it is
Precautions essential that the operating and service personnel follow generally
accepted safety procedures in addition to the specific precautions
specified in this manual. Specific warning and caution statements and
symbols are included in the relevant sections of this manual.
Warning and caution statements and symbols are marked on the
apparatus where appropriate. The symbols are described in the table
below:

Yellow/black or Red/white WARNING: the operator must refer to

an explanation in the User Documentation.▲

White/black/moulded Protective earth (ground) terminal▲

Yellow/black Surfaces which may be hot▲

Yellow/black Hazardous voltages present. Handle by insulation only.

Do not touch terminal points.▲

Yellow/black Radio Frequency Radiation, Specific safety details in

user manuals.▲

Yellow/black UV Radiation, Specific safety details in user manuals.▲

Yellow/black Do not open the instrument or remove covers. No user

serviceable parts inside. ▲

Unless otherwise stated in this manual, the covers of the instrument

and accessories should only be removed by qualified, appropriately
trained service personnel.
All spare parts and consumables items must be approved by Thermo
Scientific.
Some of the chemicals used in spectrometry are corrosive and/or
flammable, and samples maybe radioactive, toxic or potentially
infective.
Normal laboratory procedures and regulations for handling such
materials should be followed.

Thermo Fisher Scientific Page 24 of 38 iCAP 6000 Reference Guide v 1.2

 4.1.3 Electrical All mains powered equipment is designed for operation with a fully
Safety earthed mains supply. The mains earth connection to the equipment
must be connected, otherwise safety may be impaired.
Where reference is made to electrical safety the national regulations for
the country of use when fitting the power cord plugs should followed.
A qualified electrician should be consulted for all electrical connections.
If liquid is spilled on, or adjacent, to the instrument immediately isolate
the instrument and accessories from the electrical supply, by turning off
the power remote to the instrumentation.

4.1.4 Equipment It is the user’s responsibility to carry out appropriate cleaning and
Cleaning and decontamination of the equipment if hazardous material is spilt on or
Decontamination inside the equipment. Cleaning and decontamination are specified in
the relevant sections of this manual. Before using any other procedures,
users should check with the manufacturers that the proposed method
will not damage the equipment.

4.1.5 Impaired Whenever Safety Protection has been impaired the instrument and
Safety accessories must be made inoperative and secured against any
Protection unintended operation. The matter should then be referred to the local
Thermo Scientific service organisation. Safety protection is likely to be
impaired if the instrument fails to operate normally, or shows visible
damage. If the equipment is used in a manner not specified by the
manufacturer the safety protection provided by the equipment may be
impaired.
4.1.6 WEEE This product is required to comply with the European Union’s Waste
Compliance Electrical & Electronic Equipment (WEEE) Directive 2002/96/EC. It
is marked with the symbol:

Thermo Scientific has contracted with one or more recycling/disposal

companies in each EU Member State and this product should be
disposed of or recycled through them. Further information on the
compliance of Thermo Scientific with these directives, the recyclers in
your country and information on Thermo Scientific products which
may assist the directive are available at
www.thermo.com/WEEERoHS.

4.1.7 Regulatory The iCAP 6000 spectrometer and accessories are CE marked, indicating
Notices compliance with the following European Directives:
2004/108/EC Electromagnetic Compatibility Directive (EMC
Directive)
2006/95/EC Electrical Equipment designed for use within certain
voltage limits (Low Voltage Directive).

Thermo Fisher Scientific Page 25 of 38 iCAP 6000 Reference Guide v 1.2

 For further details, refer to the regulatory notice for the iCAP 6000
spectrometers and accessories, which is reproduced below.

Thermo Fisher Scientific Page 26 of 38 iCAP 6000 Reference Guide v 1.2

 4.2 iCAP 6000 Lesen Sie diesen Abschnitt besonders sorgfältig vor der Installation und
Sicherheit dem Gebrauch des Gerätes.

4.2.1 Einführung Die hier beschriebenen Geräte erfordern gründlich ausgebildetes

Bedienungspersonal. Spezielle Justierungen, Wartungen und
Reparaturen am geöffneten Gerät dürfen nur von autorisierten
Personen durchgeführt werden.
4.2.2 Allgemeine Fūr die korrekte und sichere Handhabung des Gerātes und des
Richtlinien zur entsprechenden Zubehörs ist es unbedingt erforderlich, dass das
sicheren Bedienungs- und Service-Personal den in der Bedienungsanleitung
Handhabung angegbenen Richtlinien Folge leistet.
des Gerätes Spezielle Vorsichts- und Warnungshinweise finden Sie im der
Bedienungsanleitung besonders vermerkt

Gelb/Schwarz oder Rot/weiß WARNUNG: Bitte konsultieren Sie

das Benutzerhandbuch.▲

Weiß/Schwarz: Masse / Schutzkontakt▲

Gelb/Schwarz Heiße Oberfläche▲

Gelb/Schwarz Gefährliche Hochspannung. Nur an der Isolierung

berühren. Niemals Kontakte anfassen.▲

Gelb/Schwarz Radiofrequenzstrahlung, spezifische Sicherheit

schildert das Benutzerhandbuch.▲

Gelb/Schwarz UV-Strahlung, spezifische Sicherheit schildert das

Benutzerhandbuch. ▲

Gelb/Schwarz Öffnen Sie das Instrument nicht und entfernen Sie

keine Abdeckungen. Im Gerät befinden sich keine vom Benutzer
wartbaren Teile .▲

Außderdem befinden sich am Gerät, wo erforderlich, Hinweisschilder.

Die Geräteabdeckung sollte ausschließlich durch einen qualifizierten
Thermo Scientific Service-Ingenieur enfernt werden. Alle Ersatzteile

Thermo Fisher Scientific Page 27 of 38 iCAP 6000 Reference Guide v 1.2

 und Verbrauchsmaterialien müssen Thermo Scientific genehmigt
werden.
Einige der in der Spektroskopie zur Anwendung kommenden
Chemikalien sind ätzend, leicht entzündlich, radioaktiv, infektiös oder
toxisch.
Daher muss dafür Sorge getragen werden, dass die normalen
Laborrichtlinien zur Handhabung dieser Chemikalien zur Anwendung
kommen.
4.2.3 Elektrische Vom Netz gespeiste Geräte sind so entwickelt, dass eine
Sicherheit Masseverbindung vorhanden sein sollte. Ohne Masseverbindung
könnte die elektrische Sicherheit beeinflusst werden.
Im Hinblick auf die elektrische Sicherheit müssen die folgenden Punkte
beachtet werden:
Die elektrische Installation muss nach den jeweiligen Bestimmungen
des Landes durch qualifiziertes Fachpersonal erfolgen.
Verschüttete Flüssigkeiten: Das Gerät und/oder Zubehör sofort
ausschalten.
4.2.4 Reinigung und Es liegt in der direkten Verantwortung des ANWENDERS und nicht
Dekontamination des Geräteherstellers, eine Dekontamination des Gerätes
der Geräte durchzuführen, falls sich toxische Substanzen im System befinden.
Reinigungs- und Dekontaminationsarbiten sind in der
Bedienungsanleitung beschrieben.
Bevor Sie eine Reinigungs- bzw. Dekontaminierungsmethode einsetzen,
die nicht vom Hersteller empfohlen wird (vgl. Wartungshinweise dieser
Bedienungsanleitung), sollten Sie zusammen mit dem Hersteller
sicherstellen, dass diese Vorgehensweise das System nicht beschädigt.
4.2.5 Beeinträchtigung der Immer dann, wenn eine Beeinträchtigung der Sicherheit vorliegt, muss
Sicherheitseinrichtungen dafür Sorge getragen werden, dass keine weitere unbefugte Bedienung
des Gerätes oder des Zubehörs erfolgen kann und der autorisierte
Service-Ingenieur informiert wird.
Eine Sicherheitsbeeinträchtigung liegt z.B. dann vor, wenn nicht mehr
die erwarteten Ergebnisse oder eine sichtbare Beschädigung vorliegen.
Wenn das Gerät nicht gemäß Spezifikationen des Herstellers eingesetzt
wird, könnte die Sicherheit beeinträchtigt werden.

Thermo Fisher Scientific Page 28 of 38 iCAP 6000 Reference Guide v 1.2

 Dieses Produkt muss die EU Waste Electrical & Electronic Equipment
4.2.6 WEEE
(WEEE) Richtlinie 2002/96/EC erfüllen. Das Produkt ist durch
Konformität
folgendes Symbol gekennzeichnet:

Thermo Scientific hat Vereinbarungen getroffen mit Verwertungs-

/Entsorgungsanlagen in allen EU-Mitgliederstaaten und dieses Produkt
muss durch diese Firmen wiederverwertet oder entsorgt werden. Mehr
Informationen über die Einhaltung dieser Anweisungen durch Thermo
Scientific, die Verwerter und Hinweise die Ihnen nützlich sein können,
die Thermo Scientific Produkte zu identifizieren, die unter diese RoHS
Anweisung fallen, finden Sie unter www.thermo.com/WEEERoHS.

4.2.7 Übereinstimmung Alle Spektrometer der iCAP 6000 tragen das CE Zeichen und
mit Regularien entsprechen damit den europäischen Regelwerken.
2004/108/EC Elektromagnetische Kompatibilität (EMC)
2006/95/EC Elekrische Geräte, die für den Einsatz innerhalb
bestimmter Spannungsgrenzen konzipiert sind (Regularien zur
Minimalspannung)
Weitere Angaben über die oben genannten Standards finden Sie auf der
nächsten Seite im Auszug aus den Regelwerken für die Spektrometer
der iCAP 6000.

Thermo Fisher Scientific Page 29 of 38 iCAP 6000 Reference Guide v 1.2

 4.3 Sécurité Lire attentivement cette page avant d’installer et d’utiliser l’instrument
et ses accessoires. Les normes de sécurité continues dans ce manuel
pour iCAP 6000
sont conformes aux recommandations du «Health and security at work
act 1974».

4.3.1 Introduction L’instrument et les accessoires décrient dans ce manuel sont conçus
pour être utiliser uniquement par un personnel proprement qualifié.

4.3.2 Précautions de Le réglage, la maintenance et les réparations de l’équipement doivent

Sécurité être seulement réalisés par des ingénieurs de maintenance qualifiés qui
connaissent les risques encourus.
Pour un usage correct et sûr de l’instrument et de ses accessoires, il est
essentiel que les utilisateurs et le personnel de maintenance suivent les
procédures de sécurité généralement acceptées en plus des précautions
spécifiques indiquées dans ce manuel.
Les indications et les symboles spécifiques de mis en garde et de
précaution sont incluses dans les sections appropriées de ce manuel.
Les indications et les symboles de mis en garde et de precaution sont
marqués sur l’instrument où cela est approprié. Ces symboles sont
décris dans le tableau suivant:

Jaune/Noir ou Rouge/Blanc AVERTISSEMENT: l’opérateur doit

se référer à une explication dans la Documentation d’utilisateur.▲

Blanc/Noir Terminaison de mise à la terre (masse). ▲

Jaune/Noir Surfaces pouvant être brûlantes▲

Jaune/Noir Présence de tensions dangereuses. Manipuler uniquement

par l’isolation. Ne pas toucher les extrémités.▲

Jaune/Noir Rayonnement de Radiofréquence, détails spécifiques de

sûreté dans le manuel de l’utilisateur.▲

Jaune/Noir Le rayonnement ULTRAVIOLET, détails spécifiques de

sûreté dans le manuel de l’utilisateur.▲

Jaune/Noir Ne pas retirer les panneaux de l’instrument ou l’ouvrir.

Aucune pièce requière maintenance à l’intérieur.▲

Thermo Fisher Scientific Page 30 of 38 iCAP 6000 Reference Guide v 1.2

 Sauf indication contraire dans ce manuel, les panneaux de l’instrument
et des accessoires doivent être seulement retirés par un ingénieur de
maintenance proprement qualifié de Thermo Scientific. Toutes les
pièces de rechange et les articles consommables utilisés doivent être
approuvés par Thermo Scientific. Certains produits chimiques utilisés
en spectrométrie sont corrosifs et/ou inflammables, et les échantillons
peuvent être radioactifs, toxiques ou potentiellement contagieux. Les
procédures et règlements normaux de laboratoire pour la manipulation
de tels matériels doivent être observés.
4.3.3 Sécurité Tous les équipements alimentés par un courant électrique sont conçus
Electrique pour fonctionner avec une alimentation électrique avec prise de terre.
L’équipement doit être raccorder à la terre, dans le cas contraire, la
sécurité peut être compromise.
Suivre les règlements nationaux du pays d’utilisation lors de
l’installation électrique. Un électricien qualifié doit être consulté.
Si un liquide est renversé ou est à proximité de l’instrument, isoler
immédiatement l’instrument et les accessoires de l’alimentation
électrique.
4.3.4 Nettoyage et C’est la responsabilité de l’utilisateur de procéder au nettoyage et à la
Décontaminati décontamination appropriés de l’équipement si des matériaux
on de dangereux ont été renversés sur, ou dans, l’équipement.
l’Equipement
Les procédures de nettoyage et de décontamination sont spécifiées dans
les sections appropriées de ce manuel.
Avant d’utiliser toutes autres procédures, les utilisateurs doivent vérifier
avec le constructeur que la méthode proposée ne peut pas endommager
l’équipement.
4.3.5 Altération des Si jamais les Protections de Sécurité ont été altérées, l’instrument et les
Protections de accessoires doivent être rendus inopérants et protégés contre toute
Sécurité utilisation involontaire. La cause du problème doit alors être
communiquée au Service Après Vente le plus proche de Thermo
Scientific. Les Protections de Sécurité sont susceptibles d’être altérées si
l’instrument ne fonctionne normalement, ou montre des dommages
évidents. Les Protections de Sécurité peuvent être compromises si
l’utilisation de l’équipement n’est pas conforme aux spécifications du
fabriquant.

4.3.6 Conformité Ce produit doit être conforme á la directive européenne (2002/96/EC)

DEEE des Déchets d’Equipments Electriques (DEEE). Il est marqué par le
symbole suivant:

Thermo Scientific s’est associé avec une ou plusieurs compagnies de

recyclage dans chaque état membre de l’Union européenne et ce

Thermo Fisher Scientific Page 31 of 38 iCAP 6000 Reference Guide v 1.2

 produit devra être collecté ou recyclé par celles-ci. Davantage
d’informations sur la conformité de Thermo Scientific à ces directives,
les recycleurs dans votre pays, et les informations sur les produits
Thermo Scientific qui peuvent aider la détection des substances sujettes
à la directive RoHS sont disponibles sur:
www.thermo.com/WEEERoHS.

4.3.7 Conformitè Tous les spectromètres iCAP 6000 et accessoires sont marqués CE,
Normative indiquant leur conformité avec les Directives Européennes suivantes:
2004/108/EC Directive de Compatibilité Electromagnétique (Directive
EMC).
2006/95/EC Equipement Electrique conçu pour une utilisation avec
des limites de tension fixées (Directive Basse Tension).
Pour plus de détails sur ces normes, se référer à la notice de conformité
fournie avec les spectromètres iCAP 6000, reproduite sur la page
suivante.

Thermo Fisher Scientific Page 32 of 38 iCAP 6000 Reference Guide v 1.2

 5 EC Declaration of Conformity

Thermo Fisher Scientific Page 33 of 38 iCAP 6000 Reference Guide v 1.2

Thermo Fisher Scientific Page 34 of 38 iCAP 6000 Reference Guide v 1.2
 6 Special Agreements
This section should detail any special agreements, which have been
arranged with your local Thermo Fisher organisation

Thermo Fisher Scientific Page 35 of 38 iCAP 6000 Reference Guide v 1.2

Thermo Fisher Scientific Page 36 of 38 iCAP 6000 Reference Guide v 1.2
7 Pre-Installation Checklist
This checklist is to be filled in by the customer to confirm that all relevant factors concerned with
the installation have been considered and dealt with.
On completion of the list, a copy should be forwarded to the local Thermo Fisher
organisation with a request for installation to be carried out. Failure to send the checklist may
result in delays with the instrument installation, any delays may incur extra charge.

Company name:

Company representative name:

Position:

Required Checked
Location

Table dimensions for the spectrometer 900 x 600 mm

Table dimension for the auto sampler (right side of the
machine) 600 x 550 mm
Extraction
Tube diameter for extraction 125 mm
10 m/s (Duo)
Extraction capability
5 m/s (Radial)
Adjustable valve in the extraction tube Yes
Electrical supply
Plug 200-240 VAC, 32A single phase 4000W, 50Hz Yes
Standard mains plug 200-240 VAC for each accessory Yes

Argon Gas

Regulator valve in the wall 0 -10 bar (0 – 100 PSI) Yes

6 mm (1/4 inch
Gas union dimension at the exit of the regulator valve adapter supplied
with instrument)
Maximum distance between the instrument and the regulator
valve 2m

99,995% 02<10
Purity of argon (Gas or Liquid)
ppm H20<10 ppm
Pressure required at the input of spectrometer 5.5 bar (80 PSI)

Thermo Fisher Scientific Page 37 of 38 iCAP 6000 Reference Guide v 1.2

Optic nitrogen purge (Optional)

Regulator valve in wall 0 – 10 bar (0 – 100 PSI) Yes

Plastic 6 mm (1/4
inch adapter
Gas tubing from iCAP termination
supplied with
instrument)
Maximum distance between the instrument and the regulator
valve 2m
> 99.995%; 02<10
Purity of nitrogen (Gas or Liquid)
ppm; H20<10 ppm
1 – 5.5 bar
Pressure required at the input of spectrometer
(15 - 80 PSI)
Waste
Waste container, a minimum of 5 l for liquids waste Yes
Auto Sampler rinse and waste
Minimum 1 l container for the rinse supply station and waste 2 needed
Chiller
Maximum distance from the spectrometer 3m
Pipe supply outer diameter dimension 12 mm
Cooling capability 900 W
Flow rate (all chillers) 5 l/min
Pressure at 5 L/min (Thermoflex 900 chiller only) 80 psi (5.5 bar)
Chiller inhibitor Yes
PC and printer (if not bought with the instrument)
512 MB RAM, 20 GB HDD, 2 Ethernet ports, 1 serial port,
USB ports, monitor, ink jet printer Yes
Windows XP Professional (Service pack 3 or higher) or
Windows 7 Professional 32 bit Yes

iTEVA Security and/or Validator package (Optional)

Completed iTEVA Security Pre-Installation checklist
(contained in the separate document - iTEVA Security Pre- Yes
Installation Manual)

Caution: The instrument installation will not start before Thermo Fisher
receives this document back completed. In the case of false information
causing the installation to be stopped, a travel cost may be charged.
I certify the exactness of the information supplied in this document.
Signature: Date:

Thermo Fisher Scientific Page 38 of 38 iCAP 6000 Reference Guide v 1.2