Agilent 5110 and 5100 ICP-OES
Preventive Maintenance Checklist
Agilent Preventive Maintenance provides factory recommended service for your analytical systems to
assure reliable operation and the accuracy of your results. Delivered by highly-trained and certified
service engineers using genuine Agilent parts and supplies, Agilent Preventive Maintenance provides
everything you need to reduce unplanned downtime and keep your systems operating at their peak.
For more information about Agilent Technologies services please visit our web site using the following
URL http://www.agilent.com/en-us/services/analytical-instrument-services
Customer Information
Customers should provide all necessary operating supplies upon request of the engineer.
For customers using HF applications, the instrument should be returned to its standard sample
introduction system.
A customer representative should be available to the engineer while performing the preventive
maintenance procedures.
Any parts, not included in the Parts Lists section of this document, are not part of the recommended
Preventive Maintenance service, nor are they included in the price of this service.
If a system requires the use of additional or special procedures and/or parts for the instrument
service, then these must be ordered separately and charged as a repair, which may incur additional
Service Engineer’s Responsibilities
Only complete/printout pages that relate to the system being serviced.
Complete empty fields with the relevant information.
Complete the relevant checkboxes in the checklist using a “X” or tick mark “” in the checkbox.
Complete Not Applicable check boxes to indicate services not delivered, as needed.
Complete the PM service in the order of the tasks listed.
Complete the Service Review section together with the customer.
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Agilent 5110 and 5100 ICP-OES
Preventive Maintenance Checklist
System Information
Instrument system name and ID ICP 5100/5110 VDV
Instrument system site and location BTKL PP KELAS 1 PALEMBANG
List system component product numbers List the serial numbers of each component
1. ICP 5100/5110 OES 1. MY15130012
2. SPS 4 AUTOSAMPLER 2. MY15250007
3. 3.
4. 4.
5. 5.
6. 6.
7. 7.
8. 8.
9. 9.
10. 10.
ICP-OES Configuration table Circle the type or write in the type if other
Nebulizer Type SeaSpray | OneNeb | other
Spray Chamber Cyclonic Single Pass | Cyclonic Double Pass | other
Torch Radial |Dual View| other
Injector Diameter 2.4mm | 1.8mm | 1.4mm | 0.8mm | other
Injector Material Quartz | Ceramic | other
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Agilent 5110 and 5100 ICP-OES
Preventive Maintenance Checklist
General Preparation
Discuss any specific questions or issues with the customer prior to starting.
Review the instrument logbook.
Perform general external inspection of system for cleanliness.
Check for proper installation of safety-related parts, assemblies, sensors etc.
Check for required firmware/software updates and verify with customers if they would like it
installed.
For HF application systems, if standard sample introduction system was not installed, ask the
customer to install it.
Run Instrument Performance test and record results in Instrument Performance Test Results Table -
Pre PM.
Inspect and clean the system
Look for any obvious external damage or problems.
Inspect water cooling hoses, gas lines and power cord for excessive wear or damage.
Perform a general internal inspection of the system for excessive dust accumulation, clean if
necessary.
Inspect sample introduction components and record any required maintenance in the Service
Engineer Comments and notify the customer as the required actions required.
Record the instrument operating conditions in the ICP-OES Status Results Table.
Replace the polychromator purge filter.
Replace the radial pre-optics window
Replace the axial pre-optics window for SVDV and VDV instruments.
Check exhaust flow for the correct positive extraction at the exhaust duct to insure they meet
minimum specifications.
Replace air inlet dust filter.
Replace high capacity air inlet dust filter element if installed.
Remove and clean instrument water inlet filter.
G8481A Cooling water system
Section NOT Applicable
Drain cooling fluid and remove any particles from the chiller reservoir
Remove, clean and reinstall water inlet metal mesh filter.
Re fill with Polyclear cooling fluid.
Clean the cooling system Air filter and the condenser by compressed air or vacuum cleaner.
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Agilent 5110 and 5100 ICP-OES
Preventive Maintenance Checklist
SPS 3 Auto Sampler
Section NOT Applicable
Power cycle the autosampler and verify successful initialization.
Inspect X and Z axis belts for wear. Replace is necessary.
Clean X and Z axis slide shafts.
Using customer’s racks and the Agilent software move the sample probe to the 4 outermost corners
and rinse port, ensure that the probe is approximately centered in the vial.
SPS 4 Auto Sampler
Section NOT Applicable
Clean the spill tray, rack location mat, end frames and chassis with a damp soft cloth and diluted
mild detergent.
Clean the auto sampler cover panels, if cover kit is installed, with domestic window cleaner
Check the X-axis and Z-axis drive belts for cracks, splits, damaged teeth, excessive fraying, color
changes or degradation from fumes.
Check the X-axis, Theta-axis and Z-axis FFC cables for cracks, incorrect positioning, damaged edges
or damaged connectors.
Pump Tubing Replacement. Replace peristaltic pump tubing. Replace all tubing that goes from the
rinse station to the pump and from the pump to the waste/rinse bottles
AVS 4, 6, 7
Section NOT Applicable
Replace valve rotor seal
Check fittings for signs of leaks
Check tubing including autosampler tubing for kinks or excessive wear
Check high flow pump for signs of leaks
Instrument Adjustment
Check position of Zn peak, adjust if required.
Check Argon Ratio, adjust to specified value if required.
Perform Detector Calibration.
Perform Instrument Calibration.
Run Instrument Performance Test and record results in Instrument Performance Test Results Table -
Post PM.
For systems using ICP Expert version 7.3 and above run the following Instrument tests and record
the result in the Instrument Test Results Table
Subsystem Communications Test
Air Flow
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Agilent 5110 and 5100 ICP-OES
Preventive Maintenance Checklist
Water Flow
Gas Flows
RF Generator
Camera Test
Optics Test
Nebulizer Test
Instrument Performance Test Results Table
Note: These measurements do not form part of any specification and are for reference only.
Pre PM Sensitivity Check Post PM Sensitivity Check
Radial Axial * Radial Axial*
Zn 213.857 nm SRBR 3980.6 9636.0
Mn 257.610 nm SRBR 10974.2 33048.0
Al 396.152 nm SBR 16.0 16.0
K 766.491 nm SBR 9.1 9.1
* Axial result is not applicable for G8016AA, G8012AA Radial View instruments.
Instrument Test Results Table
Note: The Instrument Test results are for systems using ICP Expert version 7.3 and above only.
Instrument Test Result
Subsystem Communications Test PASS
Air Flow PASS
Water Flow PASS
Gas Flows PASS
RF Generator PASS
Camera Test PASS
Optics Test PASS
Nebulizer test PASS
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Agilent 5110 and 5100 ICP-OES
Preventive Maintenance Checklist
ICP-OES Status Results Table
Note: These measurements do not form part of any specification and are for reference only.
Measurement Standby Mode Plasma On
Mains Voltage 220.349 VAC 215.536 VAC
Mains Current 0.208 A 0.104 A
Instrument Temperature 22.2 °C 23.9 °C
RF Air Flow (sensor speed) 25 Hz 12 Hz
Plasma Exhaust Temperature No measurement 64.3 °C
Water Flow Oscillator No measurement 1.34 L/min
Water Flow Detector 0.92 L/min 0.92 L/min
Water Inlet Temperature 20.7 °C 20.8 °C
Polychromator Temperature 35 °C 35 °C
CCD Temperature -40 °C -40 °C
Thermal Stabilizer 35 °C 35 °C
Argon Supply Pressure 554.63 kPa 536.75 kPa
Purge Gas Supply Pressure*1 600.68 kPa 573.63 kPa
Option Gas Supply Pressure*1 -0.58 kPa -0.79 kPa
Nebulizer Flow No measurement 0.8 L/min
Nebulizer Back Pressure No measurement 333.51 kPa
Plasma Gas Flow No measurement 15.02 L/min
Auxiliary Gas Flow No measurement 1.2 L/min
RF Power No measurement 1200 W
RF Supply Current No measurement 8.678 A
RF Supply Voltage No measurement 184.279 V
*1 If option installed
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Agilent 5110 and 5100 ICP-OES
Preventive Maintenance Checklist
ICP-OES Parts List Table
Part description Part Number Product /Model # where used Quantity Consumed
G8010A, G8011A,
Axial Pre-Optic Window G8010-68014
G8014A/G8015A
Radial Pre-Optic Window G8010-68015 All
Polyclear Cooling Fluid G3292-80010 G8481A
Purge Gas Filter G8010-60136 All
Air inlet filter G8000-68002 All
High Capacity Air Filter G8010-60189 Optional
Rotor seal for 6-7 port valve for
G8494-60002 G8494A/G8495
AVS6/7
Rotor seal for 4 port valve for
G8493-60002 G8493A
AVS4
Rinse solution to rinse station
G8410-80123 SPS 4
2.5mm id x 1m
Barb connector 2.5mm-1.5mm ID G8410-80124 SPS 4
PVC waste tubing,8mm od x 5mm
G8410-80122 SPS 4
id, 2m
Additional Parts may be required from engineers stock:
X axis drive belt 5410047500 SPS 3
Z axis drive belt 5410047400 SPS 3
Peristaltic pump tubing, PVC
3710049000 SPS 4
SolvaFlex, 3 bridged,
Restore system
For HF applications, ask the customer to reinstall their sample introduction system.
Leave system in an idle state: on and purging.
Guidance: If the PM service is performed prior to a qualification service, then use the qualification
procedure as a guide for final instrument set up and checkout.
Service Review
Affix the PM sticker to the system or instrument logbook based on the customer's request.
Complete the Service Engineer Comments section below if there are additional comments.
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Agilent 5110 and 5100 ICP-OES
Preventive Maintenance Checklist
Review the service and any test results with the customer.
If the Instrument firmware was updated, record the details of the change in the Service Engineer's
Comments box below or if necessary, in the customer's IQ records.
Service Completion
Service request number __________________ Date service completed ________________________
Agilent signature __________________ Customer signature ________________________
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