CONTROL TEST CARD

Use in conjunction with:

DOSAGE REQUIREMENTS PAGE
ONBOARD LOG

COOLING WATER TREATMENT – LIQUIDEWT HIGH-RANGE

Read SDSs before running these tests. Before testing, samples should be cooled to 25°C (77°F).

CWT TITRETS PROCEDURE WEEKLY TEST – SYSTEM WATER

Note: If the sample is colored or turbid, filter before running the test. If the sample remains cloudy after the first filtering, the sample should again be filtered through the same paper since the filter becomes more retentive on the second filtration.
1. Fill the Sample Cup (included) to the 25 ml mark with treated cooling water sample (Fig. 1).
2. Slide the flexible rubber end of the Valve Assembly over the tapered tip of the Titret to the white Reference Line for a snug fit (Fig. 1 2 Slide Over 3 Snap
Valve
2). ml
Score
Valve
Score Assembly
25 Assembly
3. Snap the tip of the Titret (ampoule) at the Score Mark (Fig. 3). 20 Mark Mark
4. Lift the control bar and insert the Titret assembly into the body of the Titrettor (Fig. 4). 15 3
10 Reference
5. With the tip of the Valve Assembly immersed in the sample, press the control bar firmly, but briefly, to pull in a small amount of 5 Line
Titret Titret
sample (Fig. 5). The contents will turn a GREEN color. CAUTION: Do not press the control bar unless the tip of the Valve Assembly is
immersed below the surface of the liquid.
6. Press the control bar again briefly to allow another small amount of sample to be drawn into the Titret (Fig. 5). 4 Titrettor 5 6
Watch for
7. After each addition, rock the entire assembly to mix the contents of the Titret. Watch for color to change from GREEN to BRIGHT Lift
Color Change 1.4
Here Value
ORANGE. NOTE: Immediately before the contents turn BRIGHT ORANGE, they will briefly turn BLUE. Make further additions with care. Control Insert 1.5
= 1.5
Bar Here Read
8. Repeat steps 5 through 7 until a permanent color change occurs. Press Here 1.6
Control Bar
9. When the color of the liquid in the Titret remains BRIGHT ORANGE, remove the Titret from the Titrettor. Hold in a vertical position
Sample
and carefully read the depth scale on the Titret that corresponds to the liquid level at the bottom of the concave meniscus (Fig. 6).
Refer to the chart below for dosage adjustments.
TEST RESULTS AND CONTROL DOSAGE REQUIREMENTS CONVERSION CHART
DEPTH SCALE UNITS 1.0 1.1 1.2 1.3 1.4 1.5 1.6 1.8 2.0 2.5 3.0 3.5 4.0 5.0 7.0 10.0
LIQUIDEWT (PCN 0097403)
AS PPM PRODUCT 8,000* 9,000 10,000 11,000 12,000 13,000 14,000 15,000** 17,000 22,000 26,000 30,000 34,000 43,000 60,000 86,000
DOSAGE in liters/ton
6 5 4 4 3 3 2 OK OK OK OK OK HIGH HIGH HIGH HIGH HIGH HIGH
Initial = 13.0 liters/ton No Dosing No Dosing No Dosing No Dosing No Dosing
*If readings are below 8,000 (scale unit 1.0), add 10.0 ltr/ton and retest. If system has been partially drained As long as the system is not foaming and is at or under a product
and refilled, use initial dosage. Within Control Limits ppm of 60,000, the high levels can be reduced by the normal
**OEM minimum requirements for High-Range Engine Program. There is no need to go significantly above makeup process if that will occur within a month, otherwise,
these requirements. partially drain and freshen the system.

COOLING WATER CHLORIDE TEST PROCEDURE WEEKLY TEST – SYSTEM WATER

Note: If the sample is colored or turbid, filter before running the test. If the sample remains cloudy after the first filtering, the sample should again be filtered through the same paper since the filter becomes more retentive on the second filtration.
1. Add one scoop (0.5 g) of Sample Pretreatment (available individually, not part of Chloride LMP Test Kit) to approximately 70 ml of
cooling water, collected in Beaker 100 ml - Clear Plastic, and stir until granules dissolve into solution (Fig. 1).
1 2 2 3
2. WAIT 2 MINUTES to allow precipitates to settle .
3. Filter the sample by folding Filter Paper in quarters and overlapping three sections to form a funnel. Pour water through the Filter
Paper and Funnel - Plastic (Fig. 2). Proceed with the chloride determination using the Chloride LMP Test Kit. OR

4. For samples < 100 ppm chlorides: Rinse the Plastic Vial and fill to the mark (10 ml) with the sample to be tested (Fig. 3). ~70 ml Sample
Pretreatment
WAIT 2 MINUTES 10 ml
2
then ml
For samples > 100 ppm chloride: Rinse the tall Glass Vial (test tube) and fill to the mark (2 ml) with the sample to be tested (Fig. 3). Filter Sample
5. Neutralize the sample by adding 3 drops of Phenolphthalein Indicator to the sample. Swirl to mix. If the sample turns PINK add
Sulfuric Acid N/10 drop by drop while swirling until the sample turns CLEAR. Afterwards, add one more drop (Fig. 4). 4 5 6
4
6. Adjust the color of the sample by adding 6 drops of Potassium Chromate. The sample will be YELLOW (Fig. 5).
7. Counting the drops, add Silver Nitrate N/10 drop by drop. Swirl between drops until the sample turns ORANGE (Fig. 6). OR &

8. Calculate the chloride concentration:

If plastic vial (< 100 ppm) was used in Step 4: - Number of drops of Silver Nitrate N/10 * 10 = ppm chloride # #
10 ml
If glass test tube (> 100 ppm) was used in Step 4: - Number of drops of Silver Nitrate N/10 * 50 = ppm chloride 10ml 10 ml 10 ml 10 ml

TEST RESULTS
Chloride 50 ppm (See Note 1) Maximum Limit
Note 1: If manufacturer’s recommendations are more stringent, take those limits into account.

CW_LIQUIDEWT HIGH-RANGE-CONTROLTEST CARD_R209

 MAKEUP WATER CONTAMINANTS WEEKLY TEST –MAKEUP WATER CONTAMINANTS
NOTE: The use of high quality, distilled makeup water is recommended as the best means to control scale. Makeup tanks
should be tested every week or more often if there is a change in the source or mixture of the water or any upset is suspected. PARAMETER MAXIMUM LIMIT
If at all possible, do not introduce makeup water with Chlorides above 50 ppm or Hardness over 170 ppm, especially if system Chloride 50 ppm Maximum Limit
water is not sufficiently below these limits to dilute the intended makeup water. Hardness 170 ppm Maximum Limit

MAKEUP WATER CHLORIDE TEST PROCEDURE WEEKLY TEST – MAKEUP WATER CHLORIDE
Note: If the sample is colored or turbid, filter before running the test. If the sample remains cloudy after the first filtering, the sample should again be filtered through the same paper since the filter becomes more retentive on the second filtration.

1a. For samples < 100 ppm chlorides: Rinse the Plastic Vial and fill to the mark (10 ml) with the sample to be tested (Fig. 1).
1 2
1b. For samples > 100 ppm chloride: Rinse the tall Glass Vial (test tube) and fill to the mark (2 ml) with the sample to be tested (Fig. 1).
2. Neutralize the sample by adding 3 drops of Phenolphthalein Indicator to the sample. Swirl to mix. If the sample turns PINK add OR &
Sulfuric Acid N/10 drop by drop while swirling until the sample turns CLEAR. Afterwards, add one more drop (Fig. 2). OR

3. Adjust the color of the sample by adding 6 drops of Potassium Chromate. The sample will be YELLOW (Fig. 3). 10 ml
2 10 #
ml
4. Counting the drops, add Silver Nitrate N/10 drop by drop. Swirl between drops until the sample turns ORANGE (Fig. 4). 10 ml 10 ml 10 ml

5. Calculate the chloride concentration:

If plastic vial (< 100 ppm) was used in Step 4: - Number of drops of Silver Nitrate N/10 * 10 = ppm chloride 3 4
If glass test tube (> 100 ppm) was used in Step 4: - Number of drops of Silver Nitrate N/10 * 50 = ppm chloride

TEST RESULTS 10 ml
#
10 ml
Chloride 50 ppm (See Note 1) Maximum Limit
Note 1: If manufacturer’s recommendations are more stringent, take those limits into account.

MAKEUP WATER HARDNESS TEST PROCEDURE WEEKLY TEST – MAKEUP WATER CHLORIDE
Note: If the sample is colored or turbid, filter before running the test. If the sample remains cloudy after the first filtering, the sample should again be filtered through the same paper since the filter becomes more retentive on the second filtration.
1. Rinse and fill the Sample Cup to the 25 ml mark with makeup water sample (Fig. 1).
2. Slide the flexible rubber end of the Valve Assembly over the tapered tip of the Titret to the white Reference Line for a snug fit (Fig. 1 2 Slide Over 3 Snap
2). Valve
Valve
ml Assembly
3. Snap the tip of the Titret (ampoule) at the Score Mark (Fig. 3). 25 Score
Mark
Assembly Score
Mark
20
4. With the tip of the valve assembly immersed in the sample, squeeze the bead valve briefly to add a small amount of sample to the 15
Titret (Fig. 4). The red indicator in the Valve Assembly will also be added to the Titret. 10
5
Reference
Line
NOTE: Do not squeeze the bead value unless the tip of the Valve Assembly is immersed below the surface of the liquid. Titret Titret
5. Rock the Titret to mix the contents. The contents of the Titret will turn a BLUE color.
6. Continue to add small amounts of sample until the liquid in the Titret turns from BLUE to PINK. Be sure to rock the Titret to mix the 4 55
contents after each addition of sample. When the color of the liquid in the Titret changes to PINK, the end point has been reached.
Squeeze 26
Stop the test, hold the Titret in a vertical position and carefully read the depth scale on the Titret that corresponds to the liquid level Bead Value
28
at the bottom of the concave meniscus (Fig. 5). Results are in ppm total hardness as calcium carbonate CaCO3. Valve Read
30
= 28
Here

TEST RESULTS
Hardness 170 ppm Maximum Limit

APPARATUS AND REAGENTS

CWT Titrets: CWT Titrets (PCN 0367012) Beaker 100 ml Plastic: Beaker 100 ml - Clear Plastic (PCN 0247016)
Chlorides: Chloride LMP Test Kit (PCN 0373019) Filter Paper: Filter Paper - 100/BX (PCN 0225012)
Pretreatment: Sample Pretreatment (PCN 0374025) (for SYSTEM Water Chloride Test) Funnel: Funnel - Plastic (PCN 0221010)
Hardness: Total Hardness Titrets (PCN 0378019) Stirring Rod: Stirring Rod - 150 mm Plastic (PCN 0417015)

CW_LIQUIDEWT HIGH-RANGE-CONTROLTEST CARD_R209