SSI-ICP-08-2016

Multitype ICP Emission Spectrometer

ICPE-9000 Series
Supplies and Maintenance Parts
Contents
Sample Introduction .................................................................................................. 3

Torches ................................................................................................................ 3
Nebulizers/Tubing ................................................................................................ 6
Spray Chambers .................................................................................................. 7
Drains .................................................................................................................. 9
Orifices ............................................................................................................. 10
Miscellaneous .................................................................................................... 10

ICPE-9000 ................................................................................................................. 12

Main unit .......................................................................................................... 12

Plasma Stand .................................................................................................... 12
Argon Supply .................................................................................................... 14
Vacuum System ................................................................................................. 15

ASC-6100F ................................................................................................................ 16

Maintenance Parts ............................................................................................ 16

Sample Cups / Accessories ................................................................................ 16

Peripheral Equipment ............................................................................................. 17

Software ........................................................................................................... 17
Auto-Samplers .................................................................................................. 17
High-Sensitivity Analysis ..................................................................................... 18
Peristaltic Pumps ............................................................................................... 18
Chillers/Cooling Kits .......................................................................................... 20

Chemical Compatibility Charts ................................................................................. 21

ASC-6100F......................................................................................................... 21
Organic Solvents ............................................................................................... 22

Sample System Configurations ................................................................................ 23

Sample Introduction
See System Configurations chart on page 21.

Torches

P/N Part Name Remarks External Appearance

211-81448-00 Mini Torch Mini torch (comes standard)

Used when introducing an undiluted

solution of a sample where the base
204-74323-00 High Salts Torch
element is on the percent order of
concentration

204-70272-00 Standard Torch Used with non-volatile organics

Used when analyzing organic solvent

Volatile Organics
204-77296-00 samples that are difficult to inject into
Torch
the plasma

Semi-Demountable Used for samples in HF

220-95356-20
Torch (see replacement parts – page 4)

Used for samples in HF

205-09627-01 Demountable Torch
(see replacement parts – page 5)

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Semi-Demountable Type

Semi-Demountable
220-95356-20 Used for samples in HF
Torch

Semi-Demountable
220-95356-30
Torch Body

Semi-Demountable
220-95356-31
Torch Adaptor

Tapered Alumina
220-95356-32
Injector 1.5mm

220-95356-33 Joint Clip B14-Nickel

GazFit Connectors for

220-95356-34 4mm OD side arm
(PKT4)

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Demountable Type

205-09627-01 Demountable Torch Used for samples in HF

Plasma Torch
205-09631-00
Sheathing

205-09630-00 Sapphire Chip 1.8 mm

205-09632-01 Injector Tube

036-11213-00 O-Ring, 4DP12

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Nebulizers
Part Name P/N Remarks External Appearance
046-00092-20 Standard Nebulizer
Includes:
046-00092-09 Connector, QSM
046-00092-10 Tube adaptor, 0735
Nebulizer, 10UES
037-61113-01 Clamp, SNP-1

046-00092-18 Take-up tube ASSY, NFTS-075

046-00092-21 For small sample amounts

Includes:
046-00092-09 Connector, QSM
046-00092-10 Tube adaptor, 0735
Nebulizer, 07UES
037-61113-01 Clamp, SNP-1

046-00092-18 Take-up tube ASSY, NFTS-075

220-95356-25 For samples containing >5% HF

Includes:
220-95356-13 Sample Tubing ASSY, NFT-050
Nebulizer, DuraMist 046-00092-09 Connector, QSM
046-00092-10 Tube Adaptor, 0735
037-61113-01 Clamp, SNP-1
046-00092-19 Ratchet UniFit Kit

220-95356-26 For samples containing ≤5% HF

Includes:
220-95356-14 Sample Tubing ASSY, NFT-075

Nebulizer, OpalMist 046-00092-09 Connector, QSM

046-00092-10 Tube Adaptor, 0735
037-61113-01 Clamp, SNP-1
046-00092-19 Ratchet UniFit Kit

046-00092-12 For samples with up to 20% TDS

Includes:
Nebulizer, SeaSpray, 046-00092-09 Connector, QSM
ARG-1-USS2S 046-00092-10 Tube adaptor, 0735
037-61113-01 Clamp, SNP-1
046-00092-18 Take-up tube ASSY, NFTS-075

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 220-95356-01 For samples with up to 40% TDS

Nebulizer, Includes:
Noordermeer, 01-801-
0749 037-61113-01 Clamp, SNP-1

-- Take-up tube ASSY

Used to flush nebulizer with cleaning

Eluo™ Cleaning Tool 220-95356-02
solution to dislodge particle build-up

Spray Chambers
P/N Part Name Remarks External Appearance

Cyclone For use with Mini Torch and High Salts

Chamber, HE Torch
046-00093-02

Includes:
046-00093-92 Locking Screw
046-00093-93 Seal

Twister Spray
220-95356-11 For use with non-volatile organics
Chamber

Temperature-controlled sample
introduction system. Programmable
from -10°C to +60°C.
IsoMist Kit
Ideal for volatile organics. Also aids in
stability for long durations of
220-95356-10 continuous analysis.
Includes:
220-95356-12 PuraFlex Transfer Tube
046-00093-01 Drain
-- Bench-top Jack
210-15508-01 Ball Joint Clip

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 Tracey TFE Spray
220-95356-22 For use with HF system
Chamber

Old Style

Straight Chamber
211-80437-01 For use with non-volatile organics*
Drain

Water-Cooled
211-43472-00 For use with VOC torch
Chamber Kit

HF Chamber
205-07778-02 For use with HF system
ASSY

*Requires Nebulizer Holder Kit, Type 2 (see page 10)

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Drains
P/N Part Name Remarks External Appearance

Drain Trap
046-00093-01 Drain for cyclone spray chamber
(Leveler)

016-31429-10 Drain Tube For use with Drain Trap

Drain device used with Tracey HF

220-95356-23 HF Drain
System

Old Style

Used for straight chamber, water-

Drain Kit cooled chamber, organics, and HF
system

211-86140-91
Includes:

035-65014-13 Half Union, HZ-01-0-PP

035-65102-01 Union, FZ28-00-PP

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Orifices

P/N Part Name Remarks External Appearance

For use with Standard configuration and Small

211-84352-91 Orifice ASSY, L
Sample Amounts configuration

211-43740-00 Orifice ASSY For use with High Salts or Standard Size torch

Miscellaneous
P/N Part Name Remarks External Appearance

Used to prevent blockages in the nebulizer

204-19281-00 Water Bubbler
when analyzing high salt samples

Nebulizer Holder
211-48062-00 Includes organic-solvent resistant O-rings
Kit, Type 2

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 211-86533-00 Connect Pipe L Connects torch to sample introduction accessories

210-15508-01 Ball Joint Clip Used with Connect Pipe L

046-00993-01 Clip Attaches Drain Trap to Cyclone Chamber

037-61113-04 Clamp, SNP-10 Attaches drain tubing to Drain Trap

220-95356-21 PFA Adapter Connect Pipe used with HF System

Old Style

211-84175-00 Connect Pipe HFS Connect Pipe used with HF System

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ICPE-9000
Main Unit
P/N Part Name Remarks Replacement External Appearance

211-86308-00 Filter, Bottom RF Cooling Intake 1 Year

211-86287-00 Filter, Left Electronics Cooling 1 Year

Plasma Stand
For sample introduction accessories, see pages 3-9

P/N Part Name Remarks Replacement* External Appearance

Auxiliary gas and carrier gas

016-31404-00 Tygon Tubing 1/8" x 1/16" 1 Month
Specify length (meters)

Plasma Gas Tube

211-85118-91 Tube for plasma gas 1 Month
ASSY

Tygon tubing
016-31429-10 Drain Tube 7/16" x 1/16" 3 Months
Specify length (meters)

Tygon tubing
Leveler Exhaust
016-31428-00 3/16" x 5/16" x 7/16" 3 Months
Tube
Specify length (meters)

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 Partition Window
211-86114-95 Axial view window
Holder

*Varies by sample type

P/N Part Name Remarks External Appearance

Protects RF Induction Coil

211-80620-00 Bonnet
Only used with radial view kit

211-81444-00 Torch Adapter Used with Mini Torch

Torch Positioning
211-86093-91 Used to set torch height
Jig

211-88275-91 Axial Mirror Located in cooling jacket

Argon purge pipe for radial

211-85422-91 Ceramic Purge Pipe
view

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Argon Supply
P/N Part Name Remarks Replacement External Appearance

210-14037-00 Inline Filter For argon supply 1 Year

035-69703-01 Insert, B-405-170 Two used when replacing filter 1 Year

035-62974-01 Sleeve Set, B400SET Two used when replacing filter 1 Year

Argon supply
016-43505-00 Tube, 44PP, White --
Specify length (meters)

Connect argon supply hose to

035-65503-00 Half Union, ¼” regulator. Comes with nut and --
ferrule.

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Vacuum System
P/N Part Name Remarks Replacement External Appearance

017-30166-01 Pump Oil, R-2 1L 6 Months

210-07003-04 Molecular Sieve 1 kg 6 Months

017-30813-01 Silicone Grease HVAG-G, 50 g 6 Months

042-00125-25 Oil Mist Trap OMT-050A 6 Months

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ASC-6100F
*Check Chemical Compatibility

Maintenance Parts

P/N Part Name Remarks External Appearance

206-50290-91 Nozzle ASSY, F Sample introduction nozzle for auto-sampler

Used to connect nozzle tubing to nebulizer

211-83697-00 Connection Tube
tubing

Sample Cups / Accessories

P/N Part Name Remarks External Appearance

046-00147-04 Vial, 16 mL Polypropylene vial, 16 mL

220-95369-00 Vials, 16 mL Polypropylene vials, 16 mL 1000/pk

200-93113-05 Reagent Tube Glass tube, 53 mL

046-00150-27 Vial, 12 mL Glass vial, 12 mL

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 220-95306-01 Vials, 12 mL Glass Vials, 12 mL 1000 /pk

Protects samples in auto-sampler from

206-50295-01 Turntable Cover
contamination

Peripheral Equipment
Software

P/N Part Name Remarks

211-44263-92 ICPEsolutions, v1.31 Win7 compatible (32-bit)
211-44280-91 QAQC Software Accuracy management software package
21 CRF Part 11 compliant.
Compatible with Win7 32-bit.
211-44482-93 ICPEsolution v2.00 For compliance, requires:
 QAQC Package (211-44280-91)
 CLASS-Public Agent (223-18236-92)

Auto-samplers

Part Name P/N Remarks External Appearance

Sample Capacity:
ASC-6100F 206-50100-30 60 x 15-mL sample tubes
8 x 20-/50-mL reagent cups

Sample Capacity:
220-95336-01 240 x 14-mL sample tubes
8 x 50-mL reagent vials
CETAC ASX-520 Requires:
211-83697-00 Connecting Tube

088-52848-42 CETAC/ICPE-9000 Comm. Cable

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High-Sensitivity Analysis

P/N Part Name Remarks External Appearance

Ultrasonic Nebulizer; Sample injection

system developed for high-sensitivity ICP
analysis. Uses ultrasonic energy to
nebulize a solution consisting of
220-95337-01 CETAC U5000 AT+
extremely fine particles. This enables the
ICPE-9000 to perform analyses at a
sensitivity 10 times higher than
conventional nebulizers

Hydride Vapor Generator; Provides high-

220-95370-01 ESI hydrideICP sensitivity measurement for Ge, As, Se,
Sn, Sb, Te, Pb, Bi, Hg

Peristaltic Pumps

Pumps

P/N Part Name Remarks External Appearance

220-95370-02 ESI MP2 Four-channel peristaltic pump

Shimadzu
One-channel peristaltic pump
Peristaltic Pump

211-88177-91 Includes:
016-31424-00 Tygon® tubing

205-09340-00 Retainer Strap

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Accessories

Part Name P/N Remarks

HVG Upgrade Kit 220-95363-03 Converts ESI MP2 pump to hydride vapor generator unit
Internal Standard Addition Kit 220-95363-30 Allows for in-line addition of internal standards
Includes nebulizer adapter, ¼-28 male/female barbed fittings (4
ICP Connection Kit 220-95370-03
each), and ASC nozzle

HVG Diagram:

Internal Standard Mixing Kit:

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Tubing

Part Name P/N Remarks

BLK/BLK, Santoprene 220-95363-20 2-stop, MPP-076-PHR, 12/pk
BLK/BLK, PVC 220-95363-23 2-stop, flared, MPP-076-F-PVC, 12/pk
BLK/BLK, Solva 220-95363-24 2-stop, flared, MPP-076-F-S, 12/pk
ORG/GRN, PVC 220-95363-25 2-stop, flared, MPP-038-F-PVC, 12/pk
RED/RED, PVC 220-95363-26 2-stop, MPP-114-PVC, 12/pk
GRY/GRY, Santoprene 220-95363-27 2-stop, MPP-130-PHR, 12/pk
BLK/BLK/BLK, Tygon 220-95363-40 3-stop, flared, ES-4397-3076, 12/pk
ORG/GRN/ORG Tygon 220-95363-41 3-stop, flared, ES-4397-3058, 12/pk
ORG/YEL/ORG PVC 220-95363-42 3-stop, flared, ES-4397-3051, 12/pk
YEL/BLU/YEL PVC 220-95363-43 3-stop, flared, ES-4397-3152, 12/pk

Probe ASSY 220-95363-50 For HVG; sample/reagents

Chillers/Cooling Kits

Part Name P/N Remarks External Appearance

Cooling water circulator for ICPE-

044-01813-01
9000
Cooling Water Requires:
Circulator, CA-
1115A-1
211-86152-91 Valve Kit

Low-temperature
Thermostatic
044-01910-01 Chiller for CCD
Chamber, NCB-
1200(SP)

Tap Water Required when tap water is used to

211-86153-91 --
Connection Kit cool ICPE-9000

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Chemical Compatibility: ASC-6100F

Chemical Sample Rinse Liquid

Water (<0.5% acid) ✓ ✓
Ethanol ✓ ✓
Hydrochloric acid ✓ ✓
Nitric acid ✓ ✓
Sulfuric acid ✓ X
Xylene X X
Perchloric acid ✓** X
Methanol ✓ ✓
Sodium hydroxide ✓ X
Gasoline X X
Petroleum X X
Acetic acid X X
MIBK X X
Butyl acetate X X
Acetone X X
IPA X X
THF X X

✓Can be used
X CANNOT be used

** Glass sample cups required

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Organic Solvents Compatibility
Boiling Point Vapor Pressure
Compound Torch Chamber
(°C) (mmHg)
Methanol 64.7 99 VOC Twister Spray Chamber
Ethanol 78.3 120 Standard Twister Spray Chamber
n-Propyl alcohol 97.5 15 Standard Twister Spray Chamber
Isopropyl alcohol 82.4 33 Standard Twister Spray Chamber
n-Butyl alcohol 117.5 4 Standard Twister Spray Chamber
n-Hexyl alcohol 157 3 Standard Twister Spray Chamber
Ethyl acetate 77.1 74 VOC Twister Spray Chamber
n-Butyl alcohol 126.3 10 Standard Twister Spray Chamber
Isobutyl acetate 118 13 Standard Twister Spray Chamber
Amyl acetate 148.8 Standard Twister Spray Chamber
Isoamyl acetate 142 4 Standard Twister Spray Chamber
Acetone 56.3 175 VOC IsoMist Spray Chamber
Dichloromethane 40 349 VOC Twister Spray Chamber
1,2-dichloroethane 83 64 VOC Twister Spray Chamber
Methyl isobutyl ketone (MIBK) 117 5 Standard Twister Spray Chamber
Di-isopropyl ketone 125 3 Standard Twister Spray Chamber
Di-isobutyl ketone (DIBK) 168 2 Standard Twister Spray Chamber
Acetylacetone 140.5 Standard Twister Spray Chamber
Acetic acid 117.8 12 Standard Twister Spray Chamber
Proprionic acid 141 2.8 Standard Twister Spray Chamber
n-Butyl Cellosolve 171.2 Standard Twister Spray Chamber
Chloroform 61.2 160 Standard Twister Spray Chamber
Carbon tetrachloride 76.7 90 Standard Twister Spray Chamber
o-Dichlorobenzene 180 1 Standard Twister Spray Chamber
Toluene 110.6 21 VOC Twister Spray Chamber
Xylene 138-144 47 Standard Twister Spray Chamber
Nitrobenzene 210.9 <1 Standard Twister Spray Chamber
Aniline 184.6 <1 Standard Twister Spray Chamber
Pyridine 115.5 15 Standard Twister Spray Chamber
Acetonitrile 81.6 70 Standard Twister Spray Chamber
Benzyl alcohol 205.4 <1 Standard Twister Spray Chamber
Tributyl phosphate 289 Standard Twister Spray Chamber
Dimethyl sulfoxide (DMSO) 189 0.4 Standard Twister Spray Chamber
n-Methyl-2-pyridone (NMP) 202 Standard Twister Spray Chamber
N,N-dimethylacetamide (DMA) 165.5 Standard Twister Spray Chamber
Gasoline 35-200 VOC IsoMist Spray Chamber
Kerosene 150-300 Standard Twister Spray Chamber
Light oil 220-350 Standard Twister Spray Chamber
Naphtha 30-200 VOC IsoMist Spray Chamber

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 System Configurations

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