Astm D575 - 91 (2024)
Astm D575 - 91 (2024)
for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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D575 − 91 (2024)
5.2 Deflection Gage—The deflection shall be shall be cleaned of any dust, bloom, grease, or other foreign
read on a gage of dial type graduated in hundredths of material. Grinding is not required because tests on products
millimetres (or thousands of an inch). are intended to be nondestructive.
5.3 Micrometer—The thickness of the specimen shall be 8. Test Conditions
measured in accordance with Test Method A of Practice 8.1 The temperature of the testing room shall be maintained
D3767. at 23 6 2°C (73.4 6 3.6°F). The specimens to be tested shall be
kept in this room for at least 3 h prior to the time of testing.
Specimens that have compression properties affected by
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
atmospheric moisture shall be conditioned in an atmosphere
controlled to 50 6 6 % relative humidity for at least 24 h.
Test Method A—Compression Test at Specified Deflection
9. Nature of Test
9.1 In this test method the compressive forces are applied
and removed in three successive cycles. The first two cycles
are for the purpose of conditioning the specimen, and the
readings are taken during the third application of force.
10. Procedure
10.1 After measuring the thickness of the test specimen,
FIG. 1 Cutting Tool place the specimen between the platens of the testing machine.
Place sheets of sandpaper3 between the rubber surfaces and the
6. Test Specimens testing machine platens. The sandpaper resists lateral slippage
6.1 The test may be performed either on rubber products or of the rubber at the contact surfaces and should be slightly
on standard test specimens, as specified. larger than the specimen. Omit the sandpaper when the surface
of the specimen is bonded to metal.
NOTE 1—Comparable results are obtained only when tests are made on
specimens of exactly the same size and shape, tested to the same 10.2 Apply the force to produce a deflection rate of 12 6 3
percentage deflection, or tested under the same force.
mm/min (0.5 6 0.1 in./min) until the specified deflection is
6.2 Standard test specimens shall be 28.6 6 0.1 mm (1.129 reached, after which release the force immediately at the same
6 0.005 in.) in diameter (650 mm2 (1.000 in.2) in area) and 12.5 rate. Repeat this loading cycle a second time. Apply the force
6 0.5 mm (0.49 6 0.02 in.) in thickness, from which all molded a third time until the specified deflection is again reached.
surface layers have been removed. Read and record the force required.
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D575 − 91 (2024)
12. Procedure group of materials without documentation that they are
12.1 Apply a specified minor mass or force for a period long applicable to those particular materials and the specific testing
enough to adjust the deflection gage, after which apply the protocols that are included in this test method.
major force for 3 s. Read the deflection on the dial gage at the 14.3 Two separate precision programs were conducted for
end of the 3-s period. The reading shall not include any this test method, one in 1983 and a second in 1989.
deflection caused by the minor force. Calculate the percent 14.3.1 AType 1 (interlaboratory) precision was evaluated in
deflection on the basis of the original thickness of the both programs. Both repeatability and reproducibility are short
specimen. term; a period of a few days separates replicate test results. A
12.2 Report the median of values taken from three test result is the value, as specified by this test method,
specimens. obtained on a single determination(s) or measurement(s) of
the property or parameter in question. The third deflection
13. Report cycle is used for the measurement. For the 1983 program,
three different materials were used; these were tested in three
13.1 Report the following information:
laboratories on two different days.
13.1.1 Deflection expressed as a percentage of the original
thickness of the specimen, 14.4 For the 1989 program seven materials were tested in
13.1.2 Force in kilopascals or pounds-force per square inch, nine laboratories on two separate days.
based on original cross section, 14.4.1 The results of the precision calculations for
13.1.3 Description of sample and type of test specimen, repeatability and reproducibility are given in Tables 1-4, in
including dimensions, ascending order of material average or level, for each of the
materials evaluated. Table 1 and Table 2 are for the 1983
program (No. 1), and Table 3 and Table 4 are for the 1989
3
400 Grit waterproof sandpaper has been found satisfactory. program (No. 2).
TABLE 1 Program 1, 1983 Precision,A
Type 1 Precision—Method A (kPa)B
4
Supporting data have been filed at ASTM International Headquarters and may
NOTE 1— be obtained by requesting Research Report RR:D11-1058.
Sr = repeatability standard deviation, in measurement units, r
= repeatability, in measurement units, TABLE 2 Program 1, 1983 Precision,A
(r) = repeatability, (relative) percent, Type 1 Precision—Method B (% DEF)
SR = reproducibility standard deviation, in measurement units, NOTE 1—
R = reproducibility, in measurement units, and (R) = Sr = repeatability standard deviation, in measurement units, r
reproducibility (relative) percent. = repeatability, in measurement units,
(kPa) Within Laboratories Between Laboratories (r)= repeatability, (relative) percent,
Material Average
Sr r (r) SR R (R) SR = reproducibility standard deviation, in measurement units,
Level
R = reproducibility, in measurement units, and (R) =
No. 3 Cl-Butyl 1106 28.2 79.8 7.2 40.4 114 10.3
reproducibility (relative) percent.
No. 2 EPDM 1731 92.8 263 15.2 69.3 196 11.3
No. 1 SBR 1746 41.5 117 6.7 77.3 219 12.5
Pooled (average) 1528 60.9 172 11.3 64.3 182 11.9 Average Within Laboratories Between Laboratories
values Material
A
Level,% Sr r (r) SR R (R)
Three laboratories participating.
B
kPa = psi × 6.89.
No. 1 SBR 36.0 1.11 3.14 8.7 1.38 3.91 10.9
No. 2 EPDM 37.1 1.16 3.28 8.9 2.57 7.27 19.7
No. 3 Cl-Butyl 43.7 0.78 2.20 5.1 2.03 5.74 13.2
Pooled (average) 38.9 1.03 2.91 7.5 2.05 5.80 14.9
values
13.1.4 Description of test method and apparatus, and A
Three laboratories participating.
13.1.5 Date of test.
Precis
14. Precision and Bias4 TABLE 3 Program 2, 1989 i on,A
Type 1 Precision—Method A (kPa)B
14.1 This precision and bias section has been prepared in
accordance with Practice D4483. Refer to Practice D4483 for NOTE 1—
terminology and other statistical calculation details. Sr = repeatability standard deviation, in measurement units, r
= repeatability, in measurement units,
14.2 The precision results in this precision and bias section (r) = repeatability, (relative) percent,
give an estimate of the precision of this test method with the SR = reproducibility standard deviation, in measurement units,
materials (rubbers) used in the particular interlaboratory R = reproducibility, in measurement units, and (R) =
program as described in this section. The precision parameters reproducibility (relative) percent.
should not be used for acceptance/rejection testing of any Average Within Laboratories Between Laboratories
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D575 − 91 (2024)
Material Level, value” of r, R, (r), or (R), to be used in decisions about test
kPa Sr r (r) SR R (R)
results. The appropriate value is that value of r or R associated
with a mean level in the precision tables closest to the mean
NR/RSS 836 20.8 58.9 7.0 74.4 211 25.2
CR 1012 14.8 41.9 4.1 72.7 206 20.3
level under consideration at any given time for any given
SBR 1528 18.5 52.4 3.4 59.1 167 11.0 material in routine testing operations.
IIR 1564 18.8 53.2 3.4 120 340 21.7
14.6 Repeatability—The repeatability, r, of this test method
IR 1694 40.4 114 6.8 79.2 224 13.2
EPDM 2218 45.1 128 5.8 179 507 22.8
has been established as the appropriate value tabulated in the
SIR 20 2591 62.0 175 6.8 206 583 22.5 precision tables. Two single test results, obtained under
Pooled (average) 1636 36.2 102 6.3 118.5 335 20.5 normal test method procedures, that differ by more than this
values tabulated r (for any given level) must be considered as derived
A
Nine laboratories participating. BkPa from different or non-identical sample populations.
= psi × 6.89.
14.7 Reproducibility—The reproducibility, R, of this test
method has been established as the appropriate value tabulated
in precision tables. Two single test results obtained in two
14.5 The precision of this test method may be expressed in different laboratories, under normal test method procedures,
the format of the following statements that use an “appropriate that differ by more than the tabulated R (for any given level)
TABLE 4 Program 2, 1989 Precision,A 14.8 Repeatability and reproducibility expressed as a per-
Type 1 Precision—Method B
centage of the mean level, (r) and (R), have equivalent
—
N OTE
1 application statements as above for r and R. For the (r) and (R)
Sr = repeatability standard deviation, in measurement units, statements, the difference in the two single test results is r = repeatability, in
measurement units,
(r) = repeatability, (relative) percent, expressed as a percentage of the arithmetic mean of the two test
SR = reproducibility standard deviation, in measurement units, results.
R = reproducibility, in measurement units, and 14.9 The user of this test method should give greater
(R) = reproducibility (relative) percent.
Average Within Laboratories Between Laboratories
emphasis to Program 2 (1989) precision results. This 1989
Material Level, program was substantially more comprehensive and the results are
Sr r (r) SR R (R)
% more typical of the current status of this test method.
SIR 20 6.89 0.207 0.59 8.5 0.597 1.69 24.5
EPDM 8.90 0.246 0.70 7.8 0.658 1.86 20.9 14.10 Bias—In test method terminology, bias is the difference
IIR 9.42 0.252 0.71 7.6 1.50 4.24 45.0 between an average test value and the reference (or true) test
IR 10.7 0.218 0.62 5.8 0.711 2.01 18.8 property value. Reference values do not exist for this test method
SBR 11.6 0.237 0.67 5.8 1.62 4.59 39.4
since the value (of the test property) is exclusively defined by this
CR 17.3 0.433 1.23 7.1 1.35 3.83 22.2
NR/RSS 20.6 0.561 1.59 7.7 1.66 4.71 22.8
test method. Bias, therefore, cannot be determined.
Pooled (average) 12.4 0.334 0.94 7.6 1.27 3.60 29.1 15. Keywords
values A
Nine laboratories participating.
15.1 compression; compression deflection characteristics;
compression test at specified deflection; compression test at
specified force; compression testing of rubber; compressive
must be considered to have come from different or non- force; constant force; deflection; hysterisis; rubber in compres-
identical sample populations. sion
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