SOAL
Data Table Diketahui
T (K) X1 (mol/mol)
Y1 (mol/mol) P
351.45 0 0 101.325
349.55 0.033 0.111 kPa
347.15 0.078 0.216
343.95 0.149 0.345 X
342.25 0.195 0.41 Liq. mole fraction
338.75 0.316 0.534 Y
336.55 0.414 0.614 Vap. mole fraction
334.45 0.532 0.697
332.15 0.691 0.796
330.45 0.852 0.896
329.25 1 1
a) Process Flow Diagram
Total Condenser
Overhead Vapor
Reflux Dru
Reflux Distilate
Top Stage 1
Light-key Mole
Rectifying Section Fraction = Xd
Stages
Feed
f
Feed Stage
Light-key Mole Fraction
= Zf
Stripping Section
Stages
N
Bottom Stage Boilup
Partial Reboiler
Bottom
s
Light-key Mole
Fraction = Xb
gram
Reflux Drum
Distilate
Light-key Mole
Fraction = Xd
b) Mass Balance
0,85𝐷+0,05𝐵=84
0,05𝐵=84−0,85𝐷 𝐷+𝐵=200
𝐵=1680−17𝐷 𝐵=200−𝐷
Neraca Komponen Light Key Neraca Total
x 98.82 0 x 0 200
y 0 1680 y 200 0
Penyelesaian Neraca Massa
1700
1600
1500
1400
1300
1200
1100
1000
900
800
700
600
500
400
300
200
100
0
0 12.5 25 37.5 50 62.5 75 87.5 100 112.5 125 137.5 150 162.5 175 187.5 200
Solusi SPLDV Neraca Massa
D (kmol/h) 92.5
B (kmol/h) 107.5
b) Nmin
Data Table
X1 (mol) Y1 (mol)
Y vs X
1
0 0
0.9
0.033 0.111
0.078 0.216 0.8
0.149 0.345 0.7
0.195 0.41
0.6
0.316 0.534
0.414 0.614 0.5
0.532 0.697 0.4
0.691 0.796 0.3
0.852 0.896
0.2
1 1
0.1
0
0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1
45 Degree Line Garis Fraksi Distilasi Garis Fraksi Distilasi
x 0 1 x 0 0.85 x 0
y 0 1 y 0.85 0.85 y 0.05
Nmin=5,7
s Fraksi Distilasi
0.05
0.05
d) N equilibrium and e) Optimum Stage
Data Table 45 Degree Line Rectifying Line
X1 (mol) Y1 (mol) T (K) x 0 1 x 0
0 0 351.45 y 0 1 y 0.2125
0.033 0.111 349.55
0.078 0.216 347.15 Garis Fraksi Distilasi Zf & q Line
0.149 0.345 343.95 x 0 0.85 x 0.42
0.195 0.41 342.25 y 0.85 0.85 y 0
0.316 0.534 338.75
0.414 0.614 336.55 Garis Fraksi Distilasi
0.532 0.697 334.45 x 0 0.05
0.691 0.796 332.15 y 0.05 0.05
0.852 0.896 330.45
1 1 329.25
um and e) Optimum Stage
ectifying Line Y vs X
0.85 1
0.85 0.9
0.8
Zf & q Line
0.42 0.7
1 0.6
0.5 Opt. Feed Stage = Stage 5
0.4
0.3
0.2
0.1
0
0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1
Nequilibrium = 7,8 (6,8 stage + 1 partial reboiler)
Opt. Feed Stage = Stage 5
f) Qc and rate of cooling water
Diketahui: Data Senyawa di Distillate
Variabel Nilai Satuan Keterangan Compound Fraksi Hvap Hasil Kali
Distillate 92.5 kmol/h Ethanol 0.15 38.58 5.787
R 3 Unitless Acetone 0.85 30.2 25.67
Cp 4.18 kJ/kg K Total 31.457
Asumsi Suhu
Tb 25 °C
Td 120 °C
Perhitungan Qc dan rate condenser
Qc 3233.08055555556 kW
Rate 8.14172892358488 kg/s
g) Qr and rate of steam
Diketahui: Data Senyawa di Distillate
Variabel Nilai Satuan Keterangan Compound Fraksi Hvap Hasil Kali
Bottom 107.5 kmol/h Ethanol 0.15 38.58 5.787
Distillate 92.5 kmol/h Acetone 0.85 30.2 25.67
Feed 200 kmol/h Total 31.457
R 3 Unitless
Cp 4.18 kJ/kg K
Asumsi Suhu
Tb 25 °C
Td 120 °C
Perhitungan Qc dan rate condenser
Qr 3757.36388888889 kW
Rate 9.46200928957162 kg/s
h) Feed Stage Temperature (interpolasi)
T (K) X1 (mol/mol)Y1 (mol/mol) Xf 0.42
351.45 0 0
349.55 0.033 0.111 Jawaban
347.15 0.078 0.216 336.4432 K
Tf
343.95 0.149 0.345 63.29322 C
342.25 0.195 0.41
338.75 0.316 0.534
336.55 0.414 0.614
334.45 0.532 0.697
332.15 0.691 0.796
330.45 0.852 0.896
329.25 1 1
i) Column Efficiency and j) Nactual
Data Soal
Senyawa Nilai Satuan
Miu Acetone 0.317 mPa.s
Miu Ethanol 1.149 mPa.s
Fraksi Acetone 0.42 Unitless
Fraksi Ethanol 0.58 Unitless
Avg. Viskositas 0.79956
Efisiensi 19.78954924
N equilibrium 7.8
N actual 39.41474314
k. Column Height
Unit ft m Data
Column Height 92.829462 28.29442 Tray Spacing 2 ft
N actual 39.414731 Unitless
ata
Hasil Konversi
l. Column Diameter
a) Cari berbagai Faktor
Fst?
σ acetone 23 Fraksi acetone 0.42
Fst 1.023107
σ ethanol 22 Fraksi ethanol 0.58
Ff?
Acetone dan Ethanol tidak berbusa, maka nilai Ff = 1.
Ff 1
Fha?
Data
R 3 Unitless
D 92.5 kmol/jam
L 277.5 kmol/jam
V 370 kmol/jam 0.102777 kmol/s
Cari Data RhoV Bottom and Top
MW acetone 58.08 g/mol RhoV Top (kg/m³)
MW ethanol 46.07 g/mol
2.08316333072683
T Top 329.25 K
T Bottom 351.45 K RhoV Bottom (kg/m³)
R 8.314 kJ/kgK
1.95157640245215
P 101.325 kPa
Fraksi Acetone 0.85 Unitless
Fraksi Ethanol 0.15 Unitless
Cari Data RhoL
Rho Acetone 784.6 kg/m³ MW Liquid (kg/mol)
Rho Ethanol 789 kg/m³ 0.0511142
Fraksi Feed V Liquid (m³/mol)
Fraksi Acetone 0.42 Unitless 6.49569051516729E-05
Fraksi Ethanol 0.58 Unitless RhoL (kg/m³)
786.894016589145
Cari Data Rhov
Fraksi Feed MW Liquid (kg/mol)
Fraksi Acetone 0.05 Unitless 0.0466705
Fraksi Ethanol 0.95 Unitless Rhov (kg/m³)
1.61839861564617
Cari Flv dan Fha!
0.0385891136118599
Flv kurang dari atau sama dengan 0,1; maka Fha = 0,1.
Fha 0.1
Lanjutan caranya di bagian kanan atas…
Cf 0.38 ft/s
0.115824 m/s
Cari nilai C!
Fst Ff Fha Cf C
1.023107 1 0.1 0.38 0.038878
0.01185 m/s
Uf 0.856139
Dt 9.62957
2.935093
RhoV Top (lb/ft^3)
0.130051886737276
RhoV Bottom (lb/ft^3)
0.121836914805088
RhoL (lb/ft^3)
49.1257934556603
Rhov (lb/ft^3)
0.101036625574791
ft
