Customer Details

Name of Company M/s SOHAM TRADING

& Address Vanka Mohalla,
Bilimora, Navsari,
Gujrat-396321
Contact Person Mr. Damodar
Contact Number 9325217177
Email Id [email protected]
Quotation Details
DVC Quotation Q/ST/070223/AA/231436/R0
Number
Quotation Date R0: 07/02/2023
Quotation for 20 TPD Multi-feedstock Batch type Biodiesel Plant
Sections Capacity comprising of following process stages:
• Water Washing
• Bleaching
• Glycerolysis cum De-acidification
• Trans-esterification
• Methanol Rectification
• FAME Distillation
• Crude Glycerin Treatment
• THERMIC FLUID HEATER
• Air Compressor, Air receiver
• Cooling Towers with Pumping
Feedstock’s Multifeedstock(Tallow & UCO,Palm Stearin, Palm & Other
Acid Oil, Spent Earth Oil,Palm Fattya acid distillate)
Sender’s Details
Name of Company DVC Process Technologists
& DVC HOUSE, Survey No.111/11/1, Plot No.4
Address Opp. BU Bhandari Mercedes Benz Showroom
Mumbai – Bangalore Highway Service Road, Baner,
Pune – 411045, Maharashtra, INDIA
DVC Contact Mr. Atul Amgaonkar +917447428336
Person Mr. Kiran Palkar +919900054933
Mr. Ajinkya Chame +919356938610
Email ID [email protected]
[email protected]
[email protected]
Website www.dvcprocesstech.com

Q/ST/231222/AA/231360/R0 1
 TABLE OF CONTENTS
Sr.No. Description Page
1. SECTION 1: INTRODUCTION 3
2. SECTION 2 : PROCESS STAGES
2.1 Water Washing 5
2.2 Bleaching
2.3 Glycerolysis cum De-acidification
2.4 Transesterification
2.5 Methanol Rectification
2.6 FAME Distillation
2.7 Crude Glycerin Treatment
3. SECTION 3 : PROCESS STAGES
3.1 Water Washing 37
3.2 Bleaching
3.3 Glycerolysis cum De-acidification
3.4 Transesterification
3.5 Methanol Rectification
3.6 FAME Distillation
3.7 Crude Glycerin Treatment
3.8 Control panel
3.9 Erection material
3.10 THERMIC FLUID HEATER
3.11 Air compressor, air receivers
3.12 Cooling towers with pumping
4. SECTION 4: SPECIFICATION IN GENERAL
4.1 Specification Of Equipment 40
4.2 Specification Of Utilities
4.3 Makes Of Standard Bought out
4.4 Makes Of Instruments
5. SECTION 5 : GUARANTEES
5.1 Warranty of Equipment 40
5.2 Guarantees for Process Parameters
5.3 Typical Product Specification
5.4 Guarantees for the Utilities & chemicals
6. SECTION 6 : TECHNICAL SERVICES
6.1 Documentation 48
6.2 Additional documentation
6.3 Specialists Services
6.4 Services for Installation & Commissioning
7. SECTION 6 : BATTERY LIMITS & EXCLUSIONS
7.1 Battery Limits for Process 48
7.2 Battery Limits for Utilities
7.3 Key Exclusions
7.4 Exclusions from Scope of Supply of Seller
8. SECTION 8 : COMMERCIAL 50

Q/ST/231222/AA/231360/R0 2
SECTION 1 : INTRODUCTION

DVC Process Technologists (DVC) is a Pune (India) based Original Equipment

Manufacturing Company, incepted in the year 2001. DVC has strong presence in the field of
edible oil and allied industries. Having expertise in process design, equipment design and plant
design, DVC has been serving the industry in supply, installation and commissioning of
Process Plants for Fats & Oils Processing.

DVC is showing continuous phenomenal growth due to its in-depth technological expertise,
understanding of Industry’s needs in better way in today’s competitive environment and trust
developed over the years.

Process innovation, excellent project management skills and continued customer support are
our core strengths. The company has a team of technologists and engineers, who have vast
experience in the vegetable oil processing and extraction Industry.

DVC offers single point solutions to the processors for the following:

• Edible Oil Refinery for all major feed-stocks like Soybean, Sunflower, Rapeseed, Palm,
Rice Bran and Cottonseed oils.

• By-products processing in Refinery like Wet Gum Drying (Lecithin) and Acid Oil etc.

• Biodiesel and Oleochemicals Production Plants

• Solvent Extraction Plants including Soy White Flakes production system by Flash De-
Solventization technique of the de-oiled soy meal.

• Complete PLC based process automation with reputed make hardware & field instruments
for its plants; this has helped in making PLC system affordable to every processor.

The company has its own equipment ISO certified manufacturing facility near Pune to
manufacture its state of art equipment with stringent quality control.

DVC has strong Customer Service arm, which ensures support to its customers on continual
basis. This dedicated wing of company also undertakes systematic technical audit of existing
process plants for identifying and addressing areas that need improvement in the process
plant, which can be converted for process optimization and quality of end product at best
possible commercial scale. Based on findings of technical audits the necessary modifications
/ up gradation in the existing plant are undertaken and completed in timeframe offered during
shutdown.
The company has long list of its satisfied domestic as well as overseas customers and many
of them have placed repeated orders showing their enhanced confidence.

Q/ST/231222/AA/231360/R0 3
DVC’s achievement includes:

➢ Over 200+ references including Europe, USA, Australia, Middle East & Africa.

➢ 60 Lecithin Plants including Medical Grade.

➢ > 52 Green Field Projects

➢ Successfully supplied & commissioned one 150TPD Biodiesel plant

➢ Another 30TPD Biodiesel plants under execution

➢ Introduced Gums (Lecithin) Drying Plants for Rice Bran Oil.

➢ Introduced Thermosiphon heating systems and Automation in small Cap. Plants.

➢ Successful Supply & Commissioning of Flash De-solventization Plant.

➢ Repeat Orders from several customers including MNC

With innovative skills in Process Development and Engineering, DVC is committed to serve the
Fats & Oils processing Industry in a best way in the times to come!

To know more, please visit us at: www.dvcprocesstech.com

or write to us with your queries / enquiries to:
[email protected], [email protected]
and we would be happy to reply!

Thank you,

D.V. Chame
Promoter & CEO

Q/ST/231222/AA/231360/R0 4
 SECTION 1. PROCESS STAGES

BIODIESEL COMPLEX

RUCO ACID Oil PALM STEARIN PFAD TALLOW

WASHING MINERAL ACIDITY

BLEACHING GLYCEROLYSIS

FFA: <10
CATALYST
1010 DEACIDIFICATION
FATTY ACIDS

FRESH TRANSESTERIFICATION
METHANOL GLYCEROL/HEAVY PHASE

HCL
RECTIFICATION FAME
DESOLVENTISATION ACIDULATION

FATTY
ACIDS

SOAPY WATER FAME PURIFICATION CRUDE GLYCERIN

(80%)
ACID TREATMENT FAME DISTILLATION

FATTY RECOVERY BIODIESEL (B100)

& RECYCLE

Q/ST/231222/AA/231360/R0 5
 2.1 WATER WASHING

Sr. Flowchart for DVC-WBLDO-10370

No. Reference
Process stages Description
1. CHARGING The batch is transferred from Purchaser’s bulk storage
Tank by Pump P301 to Reactor R302.
2. HOT WATER WASHING Hot water is charged from the hot water from tank T333
by pump P333 is sprayed in reactor T302. And steam
agitation is provided. The water removes mineral
acidity present in the acid oil.
3. RE-CIRCULATION Feedstock kept in circulation through inline heater
E302. By pump P302 in reactor T302.
4. SETTLING The feedstock is allowed to settle in the Reactor T302.
The wash water and sludge are discharged into Tank
T307 and sent to effluent treatment by Pump P307,
while the washed feedstock is sent for drying to Tank
T303.

Q/ST/231222/AA/231360/R0 6
 2.2 PRETREATMENT BLEACHING

Sr. Flowchart fo Reference DVC-WBLDO-10370

No. Process stages Description
1. PRETREATMENT Feed oil is charged in bleacher B602 through pump P601
BLEACHING via oil/steam PHE E601, heating of oil through steam
Calculated quantity of phosphoric acid is mixed into the oil
from tank T611. Calculated quantity of bleaching earth and
carbon sucked into the bleacher. After appropriate
bleaching time the slurry is transferred for filtration.

2. FILTRATION The slurry from Bleacher B602 is conveyed by slurry

Pump P602 to Pressure Leaf Filter PLF601.
3. POLISHING Bleached oil from filter is sent to the Polishing Filter PF601.
The filtered & polished bleached oil goes to De aerator Tank
T801.

Q/ST/231222/AA/231360/R0 7
2.3 GLYCEROLYSIS CUM DEACIDIFICATION

Sr. Flowchart For Reference DVC-WBLDO-10370

No. Process stages Description
1. DE-AERATION Bleached oil is received in Deaerated tank T801.
T801 is under vacuum and provided with spray system.
2. GLYCEROLYSIS The Free Fatty acid get converted into glycerides by
means of Glycerolysis process Inside D802.
Refined glycerin is added from dosing tank.
Note: Glycerolysis is carried out only for the feedstock
having %free fatty acid content more than 10%.
3. DE-ACIDIFICATION Oil from P801 is discharged to liquid distributor
mounted at top of packing of stripping column of
Deodorizer D802, where oil & live steam travel in
counter-current arrangement.
Due to enhanced surface area of structured packing,
FFA distillation occurs at faster rate.
FFA stripped oil enters in the deodorizer equipped with
sparge pipe arrangement.
Heating is done by thermal oil heater.
Residual impurities like secondary oxidation products
are removed which are responsible for the taste of final
products.
4. FATTY ACID SCRUBBING The fatty distillate vapors from D802, are taken to
Scrubber D804 bottom side of the scrubbing system,
where the vapors are scrubbed by the liquid fatty acid
in counter current circulation to distillate vapors.
The circulations of the liquid fatty acids facilitated by
pump P804 through fatty/water PHE E804 by using
cooling water in circulation.
5. VACCUM SYSTEM Four-stage vacuum system V800 maintains the
vacuum in the deodorizing section and vents the non-
condensable part of the distillates out through
barometric condenser and vent ejector to atmosphere

Q/ST/231222/AA/231360/R0 8
 2.3 TRANSESTERIFICATION

The pre-treated feedstock is subjected to transesterification reaction. This is reaction of lipid with an
alcohol to form esters and a byproduct. It is in principle the action of one alcohol displacing another
to from an ester, termed as alcoholysis. It is a reversible reaction therefore excess of alcohol is used
to shift the equilibrium to product side.

Triglyceride + Methanol (10.9%) Methyl Esters (100.45%) + Glycerol (10.4%)

884 96 888 92

Catalyst used are sodium methylate or sodium hydroxide (>1%)

Sr. Flowchart Reference No. DVC-FAME-23E13197-R1

No. PROCESS STAGE DESCRIPTION
1. MIXING OF REACTANTS The feedstock is transferred by P1801 to the reactors R1803.
AND CATALYST Methanol from Tank T1850 is transferred by pump P1850 and
is fed to reactors R1803. Similarly, catalyst solution is fed
from tank T1851 by Pump P1851 to reactors R1803.
2. TRANSESTERIFCATION The reaction mass is kept in recirculation by Pump P1803
REACTION through heater E1803 to control the temperature of the
reaction.
3. FAME AND GLYCERIN The reacted mass is allowed be settle in reactor. Two phases
SEPARATION i.e., methyl ester as a light phase and heavy phase of glycerol
is separated. The glycerol phase is drained from bottom of
both reactors & is conveyed pump P1803 and flashed in tank
T1812 to remove methanol.
4. REMOVAL OF EXCESS FAME is transferred into Flash tank T1807 where excess
METHYL ALCOHOL methyl alcohol is re-moved. The vessel T1807 is connected
to negative pressure ejector EJ1800 for efficient flashing of
solvent traces. Excess methanol vapors are condensed in
cooler E1823 and collected in tank T1855.
5. SOAP REMOVAL Citric acid is added in. the tank T1807 from tank T1811.The
traces of soaps are split with citric acid. Hot water is added in
tank T1807 from tank T1833 by pump P1833. FAME mass is
subjected for water wash with hot water to solubilize the
soaps. Pump P1807 is used for proper mixing of hot water
through heater E1807 for circulating the mass. Settling is
given for the batch and soapy water is decanted then sent for
the treatment for recover fatty mass.
6. DRYING OF BIO DIESEL FAME from the tank T1807, is transferred by pump P1807 to
(FAME) vacuum drying vessel D1808 via heater E1807. Dryer T1808
is connected to the high vacuum system V800 for complete
removal of moisture.
FAME is transferred by pump P1808 to Purchaser's
intermediate storage tank T2000 via heat exchanger E1808
to cool FAME prior to next storage or distillation process.

Q/ST/231222/AA/231360/R0 9
2.4 METHANOL RECTIFICATION

Sr. Flowchart Reference No. DVC-FAME-19066

No.
PROCESS STAGE DESCRIPTION
1. METHANOL The evaporated methanol from flash vessel & outlet of
CONDENSATION AND EJ1800 are taken in vent condenser E1823. Other vents
RECOVERY from reaction vessels are also connected to cooler. The
condensed mass then drained to receiving tank T1855.
2 METHANOL The methanol from tank T1855 is conveyed by pump
RECTIFICATION P1855 into the methanol rectification column D1858.The
column is working under atmospheric pressure.

The distillation column is provided with re-boiler E1857

and bottom pump P1856 for circulation and transfer of
mass to provide the heat to vaporize the methanol.

The methanol vapors are condensed in heat exchanger

E1859 and is receiver tank T1859. The condensed
methanol is partly circulated as reflux to get pure
Methanol.

Vent from the tank T1859 goes to heat exchanger E1861

where the vapors are cooled by chilled water.

Q/ST/231222/AA/231360/R0 10
 2.5 FAME DISTILLATION

Sr. Flowchart Reference No. DVC-FAME-23E13197-R1

No. PROCESS STAGE DESCRIPTION
1. FAME PREHEATING FAME from Purchaser’s intermediate storage Tank is
transferred by Pump P2001 and pre-heated in the
heat exchanger E2006A re-generatively by heat of
FAME vapors.
2. HEATING Preheated FAME enters in the bottom tray& the heat
is provided by thermal oil in E2003 at bottom of
column.
3. SCRUBBING FAME vapors are condensed by scrubbing via
recirculation by pump P2007 from tank T2007. The
level in the scrubber is maintained by level switches.
FAME is discharged through cooler E2008 to storage.
4. PITCH REMOVAL Pitch is removed from bottom by pump P2005 &
cooled in cooler E2004 before storage.

Q/ST/231222/AA/231360/R0 11
2.6 CRUDE GLYCERIN TREATMENT

Sr. Flow Chart: DVC-FAME-23E13197-R1

No. Process stages Description
1. HOMOGENIZATION The crude glycerin from the tank T1812 is transferred by Pump
& ACID ADDITION P1812 to acidulation reactor R1841.
The calculated quantity of Hydrochloric Acid is added from HCl
Tank T1846 to reactor by metering pump P1846 through inline
mixer IM1845A. The mixture is homogenized by circulation of
mass by Pump P1841.
2. SPLITTING Due to reaction of soap & Hydrochloric Acid, soap gets split
into FFA and salt.
3. SETTLING After completion of splitting reaction, settling of acidulated
mass into two layers is done. One at top as acid oil & glycerin
at bottom.
The lower layer is drained to the glycerin tank T1842 and then
send to storage.

4. HOT WATER Hot water is added to reactor R1841 through the inline mixer
WASHING IM1845A and kept in circulation by Pump P1841. Bottom layer
of acidic water is drained in Tank T1844 and send to ETP by
pump P1844. Acid oil is drained in the tank T1843 and is
transferred by Pump P1843 to Storage.

Q/ST/231222/AA/231360/R0 12
 SECTION 3 : SPECIFICATION OF EQUIPMENT

3.1 WATER WASHING

Eqpt. Description MOC of Capacity or Qty.

Code contact parts Size

T302 REACTION VESSEL

Reaction tank for washing the acid oil by CS & FRP Suitable 01
hot water. Cylindrical tank complete with coating
necessary nozzles for feedstock inlet &
outlet and level instruments. Provided with
wash water spraying, and live steam
sparging arrangement.

P302 PUMP
Pump for recirculation to washing reactor. Body CS with Suitable 01
Type: Centrifugal PVDF lining
Complete with casing, impeller, base plate,
mechanical seal and coupling & motor.

T307 TANK
Tank for receiving the wash water after CS with FRP Suitable 01
settling in the reaction vessel lining

P307 PUMP
Pump for conveying wash water to ETP Body CS with Suitable 01
Type: Centrifugal PVDF lining
Complete with casing, impeller, base
plate, mechanical seal and coupling &
motor

LIST OF INSTRUMENTS:
Sr. Instrument Description Qty.
No Code
1. PI 01 PRESSURE INDICATORS 1S
Pressure Indicators dial type with connection accessories
2. TI 21 TEMPERATURE INDICATORS 1S
Temperature indicators dial type with SS304 pockets for
connections.

Q/ST/231222/AA/231360/R0 13
 3.2
Eq. Description MOC of Cap. Qty.
Code contact &Size
Parts

F01 STRAINER CS with

Strainer for removing heavy impurities from the feed. SS304 Suitable 01
screen

E601 HEAT EXCHANGER (Heating)

Heat exchanger for balance heating of feed oil by LP Plates: Suitable 01
steam. The heat exchanger is complete with all the SS316 &
connections and gaskets. Gasket: HT
Type: Plate NBR

T611 TANK(Acid)
Tank for buffer storage of acid reagent. The cylindrical SS316 Suitable 01
tank with top lid is provided with necessary outlet nozzle
for acid.

B602 BLEACHER
Bleaching Reactor is designed to homogenize the earth SS304 Suitable 01
– oil slurry and providing necessary retention time
under vacuum of 50 mm of Hg for efficient bleaching.
The Bleacher is Cylindrical dished end design provided
with agitator complete with nozzles & manholes

P602 PUMP (earth-oil slurry)

Pump for conveying of earth-oil slurry from bleacher SS304 Suitable 01
B02 to pressure leaf filter.
Type: Centrifugal
Complete with casing, impeller, mechanical seal, and
motor.

Q/ST/231222/AA/231360/R0 14
Eq. Code Description MOC of Cap. Qty.
contact &Size
Parts

PLF601 PRESSURE LEAF FILTER

Pressure leaf filters are designed for filtration of SS304 Suitable 01
bleaching earth from Oil and bleaching earth
slurry pumped from Bleacher B602.
Pressure leaf filter comprises of cylindrical
pressure vessel with vertical filter element
mounting complete with leaves, mounting bar
assembly, necessary nozzles for oil, bottom
nozzle for spent earth discharge for filtration of
bleached oil slurry.

The Filters are provided with discharge chutes

for spent earth discharge at the bottom of filter
vessel Spent earth discharge valve at filter
bottom with pneumatic actuator and accessories.

PF601 POLISHING FILTERS

Polishing filters (bag type) for polishing filtration SS304 & Rated 01
of bleached oil and entrapping foreign matter of Bags capacity
size 10 micron and above. Nylon
Cylindrical filter casing fitted internally with nylon
Filter bag with bag removal facility. The bags
are heat sealed for avoiding any slippage of
particles.

V600/ VACUUM SYSTEM

V800 Vacuum system designed for creating and Carbon Suitable (01)
maintaining vacuum in Bleacher B602. steel
*Note: Combined vacuum system is given for
both Bleaching & Deodorization section V800

T606 TANK (recovered oil)

Tank for collection of the recovered oil during Carbon Suitable 01
Pressure Leaf Filter cleaning cycle. Cylindrical steel
tank is complete with agitator and Motor. The
vessel is provided with coil for providing steam
Heating and nozzles for oil and vapor.

P606 PUMP (recovered oil)

Pump for feeding recovered oil slurry to Body: CS & Suitable 01
Bleacher B602. Internal:
Type: Centrifugal SS304
Complete with mechanical seal, base plate &
Motor.

Q/ST/231222/AA/231360/R0 15
Eq. Code Description MOC of Cap. Qty.
contact &Size
Parts

C606 CYCLONE
Cyclone vessel for separation of steam from Carbon Steel Suitable 01
Oil & slurry during cleaning operations of
filters.

MT604 MOISTURE TRAP

Moisture trap for entrapping moisture from Carbon Steel Suitable 01
Vacuum line. The vessel provided with
necessary connections.

DH632 DUMP HOPPER

Dump hopper for dumping bleaching earth Carbon Steel Suitable 01
sacks at ground level

LIST OF INSTRUMENTS

Sr. Instrument Description Qty.

No Code
1. PI 602 PRESSURE INDICATOR 1S
Pressure Indicator for Bleacher consisting of transmitter
and panel mounted indication.
2. TI 602 TEMPERATURE INDICATOR 1S
Temperature indicator consisting of Transmitter and panel
mounted indication.
3. LAH 606 LEVEL SWITCHES 2
LAL 606 Level switches for Low and High- level control of Cloudy
Oil Tank

Q/ST/231222/AA/231360/R0 16
 3.3 GLYCEROLYSIS CUM DEACIDIFICATION

Eq. Description MOC of Cap. Qty.

Code contact &Size
Parts

T801 TANK (De-aeration)

Tank for storage / de-aeration of feed oil from SS304 Suitable 01
bleaching section and feeding tank to
deodorization process.
Cylindrical tank with necessary nozzles for oil, sight
& light glass, designed for working under vacuum.

P801 PUMP (De-aerated oil)

Pump for pumping de-aerated oil from T801 to oil SS304 Suitable 01
heater in bottom tray of Deodorizer.
Type : Centrifugal
Complete with base plate, mechanical seal,
coupling and motor.

T1903 TANK
Tank for the storage of glycerin required for SS304 Suitable 01
Glycerolysis process, provided with necessary inlet
outlet nozzles, sight glass and measuring or
calibrated glass.

DEACIDIFICATION COLOUMN
Deodorizer Column comprise of Two Rated 01
Sections – Capacity
D802 1. TOP Section –STRIPPER
Stripper is cylindrical tower with dished end at top and SS304
bottom is mounted on the deodorizer vessel; it Packs SS316
comprises of structural packing bundles installed one
over the other vertically. At the top there is liquid
distributor for uniform distribution of oil.
D802A 2. LOWER Section – RETENTION VESSEL
Equipped with coils for Thermic Fluid and cooling SS304 Suitable
water, Sparge steam arrangement, Nozzles for
Temperature and pressure indication. Sight glass
and Manholes are also provided.
Design :- Thermic fluid Coils –
SS316 seamless Schedule10

Q/ST/231222/AA/231360/R0 17
 Eq. Description MOC of Cap. Qty.
Code contact &Size
Parts

P803 PUMP
Pump for circulating the oil in D802 and after SS304 Suitable 01
completion of Deodorization process the oil is
transferred to storage.
Type: Centrifugal
Complete with coupling and motor.

E806 CONDENSER SS304 Suitable 01

Condenser for condensing Glycerin

E805 HEAT EXCHANGER (Final Cooling)

Heat exchanger for final cooling of oil before SS304 Suitable 01
going to storage.
Type: Shell and tube

PF803 POLISHING FILTER

Polishing filters for polishing deodorized oil SS304 & Suitable 01
and entrapping foreign matter size 8 micron and Nylon
above
Cylindrical filter casing fitted internally with
multiple nylon filter bag with bag removal facility.
The bags are heat sealed for avoiding any
slippage of particles.

D804 SCRUBBER
Scrubber is designed for the separation of SS304 Suitable 01
distillate and volatiles from vapors coming out of
Deodorizer. The vapor scrubber is a cylindrical
column provided internally with structured
packing for vapor scrubbing. The scrubber is
equipped with manhole, sight glass and
distribution system for uniform distribution of
distillate on structured packing.
The scrubber is connected by vapor duct with
Deodorizer.

PUMP (Distillate circulation)

P804 Pump for circulation of scrubbed distillate from SS316 Suitable 01
scrubber D804 to heat exchanger E804 and
back to the scrubber
Type: Centrifugal,
Complete with base plate, mechanical seal, and
coupling and motor.

Q/ST/231222/AA/231360/R0 18
 Eq. Description MOC of Cap. Qty.
Code contact &Size
Parts

E804 HEAT EXCHANGER (Fatty acid cooling)

Heat exchanger is designed of suitable size to Plate: SS316 Suitable 01
cool fatty acids in circulation in D804. Distillate Gasket: NBR
for the high temperature volatile circulation.
Type: Plate

V800/V VACUUM SYSTEM

600 Vacuum system designed for creating and Condensers: Suitable 01
maintaining high vacuum in deacidification SS304
section. Rest Carbon
Note: Combined Vacuum System for both steel
Bleaching &

LIST OF INSTRUMENTS

Sr. Instrument Description Qty

No Code

1. PI802 PRESSURE INDICATOR 1S

Pressure indicator for the deodorization column. Transmitter
with indication at the panel.
2. TI 02 TEMPERATURE INDICATORS 1S
Temperature indicators dial type with SS pockets for the
connection to the Equipment
3. LAH 801 LEVEL SWITCHES 2
Level switches for Tank T801

Q/ST/231222/AA/231360/R0 19
3.4 TRANS-ESTERIFICATION

Eqpt. Description MOC of Cap. & Qty.

Code contact parts Size

P1801 PUMP
Pump for feed oil into the trans-esterification Carbon Steel & Suitable 01
process. SS304
Pumps complete with baseplate, coupling,
mechanical seal and FP motor.

T1850 TANK
Tank for the intermediate storage and feeding SS304 Suitable 01
the methanol into the process.

P1850 PUMP
Pump for charging methanol into the trans- Carbon Steel Suitable 01
esterification reactors.
Type: Centrifugal
Pumps is complete with baseplate, coupling,
mechanical seal and FP motor.

T1851 TANK
Tank for the intermediate storage and feeding SS304 Suitable 01
the catalyst solution in to the process.

P1851 PUMP
Pump for the metering the solution. LCP Suitable 01
Type; Plunger SS316
Pump is complete with base frame and FP
motor.

R1803 REACTOR
Reactor are equipped with agitator for SS304 Suitable 01
dispersing the catalyst and alcohol.
The vessel will be equipped with sight glass,
light glass, nozzles. Each reactor is provided
arrangement for sampling of the product.
The vessel is also equipped with mechanical
seal and variable speed drive.

Q/ST/231222/AA/231360/R0 20
Eqpt. Description MOC of Cap. & Qty.
Code contact parts Size

P1803 PUMP
Pump for re-circulation of mass in the reactor LCP Suitable 01
And transfer to further process. SS304
Type: Centrifugal
Pump is complete with baseplate, coupling,
mechanical seal and FP motor.

E1803 HEAT EXCHANGER

Heat exchanger for heating / cooling the SS304 Suitable 01
reaction mass by cooling water or steam.
Type: Shell and tube

T1812 TANK
Tank for the intermediate storage of Carbon Steel Suitable 01
separated glycerin from the reactors.

P1812 PUMP
Pump for transferring the separated glycerin. Carbon Steel Suitable 01
Type: Centrifugal & SS304
Pump is complete with baseplate, coupling,
mechanical seal and FP motor.

T1833 TANK
Tank for hot water required for washing of SS304 Suitable 01
FAME provided with all necessary nozzles.

P1833 PUMP
Pump for transferring soft hot water to FAME LCP Suitable 01
wash tank T1807 SS304
Type: Centrifugal
Pump is complete with baseplate, coupling,
mechanical seal and FP motor.

T1811 TANK
Tank to store citric acid solution to SS316 Suitable 01
neutralize the alkalinity of the FAME

T1807 TANK
Tank for treatment of FAME with citric acid Carbon Steel Suitable 01
and water washing

Q/ST/231222/AA/231360/R0 21
Eqpt. Description MOC of contact Cap. & Qty.
Code parts Size

P1807 PUMP
Pump for transfer of FAME circulation & CS Suitable 01
drying. & SS304
Type: Centrifugal
Pump is complete with baseplate, coupling,
mechanical seal and FP motor.

E1807 HEAT EXCHANGER

Heat exchanger to heat mass by steam. SS304 Suitable 01
Type: Shell and tube

D1808 DRYER
Dryer for removing residual moisture from Carbon Steel Suitable 01
the washed FAME. Provided with spray
nozzle assembly and necessary nozzles.

P1808 PUMP
Pump for the transfer of FAME to dryer CS & Suitable 01
Type: Centrifugal SS304
Pump is complete with baseplate, coupling,
mechanical seal and FP motor.

E1808 HEAT EXCHANGER Plates: SS316

Heat exchanger, to cool FAME to storage Gasket: NBR Suitable 01
temperature by cooling water.
Type: Plate

T1809 TANK
Tank for draining of washed soapy water. Carbon Steel Suitable 01

P1809 PUMP
Pump for conveying soapy water to further Carbon Steel Suitable 01
treatment.
Type: Centrifugal
Pump is complete with baseplate, coupling,
mechanical seal and FP motor.

EJ1800 EJECTOR
Ejector for the low suction pressure in the Carbon Steel Suitable 01
process.

Q/ST/231222/AA/231360/R0 22
 3.5 METHANOL RECTIFICATION

Eqpt. Description MOC of Cap. & Qty.

Code Contact Parts Size

E1823 HEAT EXCHANGER

Heat exchanger to condensed methanol SS304 Suitable 01
vapor.
Type: Shell and tube

T1855 TANK
Tank for the collection of wet methanol. Carbon Steel Suitable 01

P1855 PUMP
Pump for conveying wet methanol to CS & SS304 Suitable 01
rectification tower.
Type: Centrifugal
Pump is complete with baseplate, coupling,
mechanical seal and FP motor.

P1856 PUMP
Pump for circulation of wet methanol via heat CS & SS304 Suitable 01
exchanger E1857.
Type: Centrifugal
Pump is complete with baseplate, coupling,
mechanical seal and FP motor.

E1857 HEAT EXCHANGER

Heat exchanger to heat the circulating wet SS304 Suitable 01
methanol.
Type: Shell and tube

D1858 DISTILLATION COLUMN

Distillation column for the rectification of CS body & Suitable 01
wet methanol for purity. Cylindrical dish ends Packing’s in
provided with internal packing beds for SS304
rectification process.

E1859 HEAT EXCHANGER

Heat exchanger to condense methanol SS304 Suitable 01
vapors emerging from distillation column.
Type : Shell & tube

Q/ST/231222/AA/231360/R0 23
Eqpt. Description MOC of Cap. & Qty.
Code Contact Parts Size

T1859 TANK
Tank for receiving condensed methanol. Carbon Steel Suitable 01

E1861 HEAT EXCHANGER

Heat exchanger for condensing methanol SS304 Suitable 01
from the residual vapors from the receiving
tank T1859. Type: Shell and tube
Cooling media: water at 8 0C.

P1860 PUMP
Pump for conveying reflux to distillation tower CI Suitable 01
for purification & conveying rectified methanol.
Type: Centrifugal
Pump is complete with baseplate, coupling,
mechanical seal and FP motor.

Q/ST/231222/AA/231360/R0 24
 LIST OF INSTRUMENTS

Sr. Instrument Description QTY

No Code
1 LAH1803 LEVEL SWITCHES
LAH1807 High level switches for reactor R1803 & tank T1807, 05
LAH1808 T1808, T1855.
LAH1855
2 LI1850 LEVEL INDICATORS
LI1833 Level indicators for tankT1850, T1833, T1851 & T1855 for 04
LI1851 visualization of level externally.
LI1855
3 TIC1803 TEMPERATRUE CONTROLERS
TIC1807 Temperature Controllers for heating and cooling. Comprise 03
TIC1857 of temp. Transmitter with output to controller and flow
diverting control valve.
4 PI600 PRESSURE INDICATORS
Pressure indicators field mounted 1 Set
With connection details.

5 TI600 TEMP. INDICATORS

Temperature indicators field mounted with connection 1 Set
details.

Q/ST/231222/AA/231360/R0 25
 3.6 FAME DISTILLATION

Eqpt. Description MOC of Cap. & Qty.

Code Contact Parts Size

P2001 PUMP (FAME)

Pump for feeding crude FAME to CS & SS304 Suitable 01
distillation process.
Type of pump: Centrifugal
Pump is complete with casing, impeller,
base plate, mechanical seal, and coupling
and FP motor.

D2002 DISTILLATION TOWER

Distillation tower cylindrical and dished
end to distillate. Tower comprise of SS304 & Suitable 01
stripping zone and scrubbing zone. internal
Arrangement of re-boiler heating coils packing in
provided with hot thermic fluid circulation at SS316
bottom of the tower.
Provided with necessary nozzles like
product inlet, outlet. Vapor outlet, sight
glass, manhole, thermic fluid inlet outlet.

P2005 PUMP
Pump for conveying pitch through heat CS & SS304 Suitable 01
exchanger E2004.
Type of pump: Centrifugal
Pump complete with casing, impeller, base
plate, mechanical seal, and coupling and
FP motor.

P2007 PUMP
Pump to circulate and transfer condensed CS Suitable 01
methyl esters in scrubbing zone & &
conveying to storage. SS304
Type of pump: Centrifugal
Pump complete with casing, impeller, base
plate, mechanical seal, and coupling and
FP motor.

E2004 HEAT EXCHANGER (cooling)

Heat exchanger to cool pitch from the SS304 Suitable 01
tower prior sending to storage
Type: Shell and tube

Q/ST/231222/AA/231360/R0 26
 Eqipt. Description MOC of Cap. & Qty.
Code Contact Parts Size

E2008 HEAT EXCHANGER (cooling)

Heat exchanger to cool distilled FAME to SS304 Suitable 01
storage temperature.
Type: Shell and tube
E2003 HEAT EXCHANGER
Heat exchanger to heat the crude FAME Suitable 00
by thermic fluid. SS304
Type: Shell and tube
Note: Included at the bottom of the column
E2006A HEAT EXCHANGER
Heat exchanger to heat the crude FAME Suitable 01
by distilled FAME vapors. SS304
Type: Shell and tube
E2006B HEAT EXCHANGER
Heat exchanger to cool the FAME by Suitable 01
Cooling water. SS304
Type: Shell and tube

V2000 VACUUM SYSTEM Carbon steel Suitable 01

Vacuum system for the distillation section

Q/ST/231222/AA/231360/R0 27
LIST OF INSTRUMENTS
Sr. Instrument Description QTY
No Code

1. FI2000 FLOW INDICATOR

Flow indicator to indicate the flow of crude FAME. 01
2. FI2007 FLOW INDICATION
Flow indicator & Controller to indicate the flow of 01
FAME distillate.
2. TIC2003 TEMPERATRUE CONTROL
Temperature Controller for control of temperature. 01
Transmitter, controller and control valve
3. TI2008 TEMPERATURE INDICATOR
Temperature indicator at process stage to Indicate 01
process temp, provided with transmitter
4. LI2007 LEVEL INDICATOR
LI2003 Level Indicator for level indication at T2007 & E2003 02
5. PI2002 PRESSURE INDICATOR
Pressure Indicator for distillation column 01
6. PI2000 PRESSURE INDICATOR
Pressure indicators field mounted 1S
With connection details. (set)
7. TI2000 TEMPERATURE INDICATOR 1S
Temperature indicators field mounted with connection
details. (set)

Q/ST/231222/AA/231360/R0 28
 3.7 GLYCERIN TREATMENT

Eqpt. Description MOC of Cap. & Qty.

Code Contact parts Size

R1841 REACTION VESSEL

Reaction tank for reaction between crude CS & Suitable 01
glycerin and HCl acid. FRP coating
Cylindrical tank complete with necessary inlet
and outlet nozzles for glycerine & HCl addition,
level instruments.

P1841 PUMP (Circulation)

Pump for circulation of mass into the Reactor. Body CS with Suitable 01
Type: Centrifugal pump. PVDF lining for
Complete with casing, impeller, base plate, and LCP
mechanical seal and coupling and motor

T1846 TANK (HCL Acid)

Tank for buffer storage of HCl acid. CS & Suitable 01
Cylindrical tank complete with necessary inlet FRP coating
and outlet nozzles

P1846 PUMP (HCL Acid) Body CS with

Pump for transfer of HCL acid to Acidulation Teflon lining for Suitable 01
Reactor through inline mixer IM1845A. contact parts
Type: Metering Pump
Pump complete with casing, base plate,
mechanical seal, and coupling and motor.

IM1845A INLINE MIXER CS &

Inline mixer for mixing HCL acid, hot water FRP coating Suitable 01
with crude glycerine.

T1843 TANK (Acid Oil)

Tank for receiving Acid oil after settling in CS with FRP Suitable 01
reaction tank. lining
Cylindrical tank with conical bottom and is
complete with necessary inlet and outlet
nozzles.

Q/ST/231222/AA/231360/R0 29
 Eqpt. Description MOC of Capacity Qty.
Code Contact parts & Size

P1843 PUMP
Pump for pumping the acid oil from acid oil Body CS with Suitable 01
Tank T1843 storage. PVDF lining for
Type: Centrifugal contact parts
Pump complete with casing, impeller, base
plate, and mechanical seal and coupling and
motor.

T1842 TANK
Tank for receiving glycerin after settling in CS with FRP Suitable 01
reaction tank. lining
Cylindrical tank with conical bottom and is
complete with necessary inlet and outlet
nozzles.

T1844 TANK
Tank for receiving acidic water after washing in CS with FRP Suitable 01
reaction tank. lining
Cylindrical tank with conical bottom and is
complete with necessary inlet and outlet
nozzles.

P1844 PUMP
Pump to convey the acid water from acid water Body CS with Suitable 01
storage to ETP. PVDF lining for
Type: Centrifugal contact parts
Pump complete with casing, impeller, base
plate, and mechanical seal and coupling and
motor.

Q/ST/231222/AA/231360/R0 30
 LIST OF INSTRUMENTS

Sr. Instrument Description Qty.

No Code
1. LAH1841 LEVEL SWITCH
Level switch for the reactor tank R1841. 01
2. FI1833 FLOW INDICATOR
Flow Indicator for hot water 01
3. PI 01 PRESSURE INDICATORS 1S
Pressure Indicators with accessories
4. TI 21 TEMPERATURE INDICATORS 1S
Temp. Indicators with accessories

Q/ST/231222/AA/231360/R0 31
 3.8 CONTROL PANEL

Eq. Description MOC Cap. Or Qty.

Code Of Contact size
Parts
CPX00 CONTROL PANEL Housing Steel For 01
Control panel consisting of Motor Control Powder coated Equipment
Centre & Remote-Control for operation of Supply
electrical motor starters and instruments at
various points in the process plant sections.
The dustproof, prewired and ready to install
panel comprising of –
Bus bar
Incoming main switch
MCB, Power Contactors
Voltmeter, Ammeter
Energy meter
Earth Fault Relay
Overload Relay
Overload tripping and circuit breaking device
Star delta feeders for motors rating above
7.5kw
Interlocking for controls as per specifications
For manually operated plant mimic diagram
will be provided.

Q/ST/231222/AA/231360/R0 32
3.9 ERECTION MATERIAL

Eq. Description MOC of Qty.

Code Contact parts
ERECTION MATERIAL
EM1870 VALVES
Ball valves CS & SS 1S
Media: oil, process water, glycerin, methyl ester, & SS316
methanol, sodium methylate, citric acid
Globe valves (Piston) CS & 1S
Media: Steam, condensate etc. SS304
Butterfly valves; CI with 1S
Media: clean and contaminated Water Nitrile rubber
Non-return valves: SS304 & 1S
Media: acid & reagent and water CS
Actuators double acting type Al casting 1S

EM1871 PIPES AND PIPES FITTINGS

Pipes in straight length ERW CS 1S
Media: Oil, methyl alcohol, glycerin, water, sodium IS:1239
methoxide soln., methyl ester, pitch & steam
Pipes ERW SS304 & SS316 1S
Media: Methyl esters, Oil
Pipe fittings, flanges, bends, reducers, nut & bolts CS & SS304 1S
/SS316
Gasket material Non-Asbestos 1S

EM1872 ELECTRICAL MATERIAL

Power cables Armored Copper conductor Copper 1S
Instrument cables Un-armored Copper 1S
Earth Flexible cables Copper 1S
Cables trays in steel with powder coating Steel 1S

EM1873 INSULATION MATERIAL

LRB Mattress with chicken wire mesh LRB 1S
Aluminum sheets Aluminum 1S
Self-tapping screw and wiring material Steel 1S

Q/ST/231222/AA/231360/R0 33
3.10 Thermic Fluid Heater

Eqpt. Description MOC of Capacity Qty.

Code contact Or Size
parts

G860 THERMIC FLUID HEATER

Thermal Oil Heater for heating thermal oil for Carbon Suitable 01
heating vegetable oil in deodorization process. Steel
Fuel: LDO
Thermic Fluid Heater comprises of Skid mounted
heater
1 N Thermal Oil Circulation Pump with Motor
1 N Expansion cum de-aerator tank for thermal oil
Control panel and necessary controls

Thermal Oil heater will be common for both

Glycerolysis cum Deacidification Section and FAME
Distillation Section.

Note: Chimney & interconnecting ducts ate in

Purchaser’s scope.

Q/ST/231222/AA/231360/R0 34
 3.10 PRS, AIR COMPRESSOR, AIR RECEIVERS

Eqpt. Description MOC of Capacity Qty.

Code contact orSize
parts

PRS-1 PRESSURE REDUCING STATION

Pressure reducing station for reduction in CS Suitable 01
steam pressure from 12 bar g * to 3 Bar g Valves
(* The Purchaser shall confirm Pressure rating CS/SS304
atthe time of placement of order.)
Pressure reducing station comprises of
necessary pressure reducing valve, regulating
valves installed in pipeline along with
provisionfor pressure gauge mounting.

PRS-2 PRESSURE REDUCING STATION Suitable

Pressure Reducing Station – for reduction CS 01
insteam pressure from 12 bar g * to 9 Bar g Valves
(*The Purchaser shall confirm Pressure rating CS/SS304
atthe time of placement of order.)
Pressure reducing station comprises of
necessary pressure reducing valve, regulating
valves installed in pipeline along with
provisionfor pressure gauge mounting.

AC AIR COMPRESSOR
Air Compressor with receiver & built in dryer Carbon Suitable 01
Air compressor for providing necessary dry Steel
andclean instrument air required for various
instruments in Refinery.

AR AIR RECEIVER
Air receiver designed to supply continuous Carbon Suitable 01
airfor the Process instruments and equipment. Steel

Q/ST/231222/AA/231360/R0 35
 3.11 COOLING TOWERS WITH PUMPING

Eqpt. Description MOC of Capacity& Qty.

Code Contact parts Size

CT1 COOLING TOWER

(Contaminated)Cooling tower Wooden Suitable 01
induced draft type, Type: cross
flow
Inlet temp./ outlet temp : 38 0C / 32 0C

CT2 COOLING TOWER (clean)

Cooling tower induced draft FRP Suitable 01
type,Type: cross flow
Inlet temp./ outlet temp : 38 0C / 32 0C

P001 PUMP (Contaminated)

P002 Pumps for the conveying of the water Body: CI, Suitable 02
toProcess House. Pump is complete Internal: CI
with Base-plate, coupling and motor
One pump will be standby

P003 PUMP (Contaminated)

Pump for the conveying of the water from Body: CI, Suitable 01
thePond to cooling tower. Internal: CI
Pump is complete with base-plate, Coupling
and motor

P004 PUMP (Clean)

Pump for the conveying of the water from Body: CI, Suitable 01
the Cooling tower to process and back to Internal: CI
coolingtower. Pump is complete with base-
plate,
coupling and motor.

Q/ST/231222/AA/231360/R0 36
 SECTION 4 : SPECIFICATIONS IN GENERAL

4.1 SPECIFICATIONS OF EQUIPMENT

1. Interconnection of various equipment by Pipes & fittings is to be as per the Process

and Instrumentation diagram for the specific project after detailed engineering of
each section order the piping considered in this offer.

2. The scope of piping will be as per the points indicated separately in the battery limits
in this offer. The Seller and Purchaser jointly to reach logical decision shall discuss
any point, which is not clearly specified in scope,

3. The material of construction for pipelines is broadly followed as mentioned below

Section Tallow, Methanol Steam, Water, Phosphoric Fatty acid

UCO, Vacuum acid distillate
other Instrument air
Washing plant FRP NA Carbon Steel Not NA
for Acid oil applicable
Bleaching SS304 NA Carbon Steel SS304 NA
Glycerolysis SS304 NA Carbon Steel NA SS316
cum De-
acidification

Trans- Carbon Carbon Carbon Steel NA NA

esterification Steel Steel
Methanol recti. Carbon Carbon Carbon Steel NA NA
Steel Steel
FAME SS304 NA Carbon Steel NA NA
Distillation

4. The thickness of insulation for pipelines and equipment shall be considered as per
insulation schedule, which is based on heat insulation requirement.

5. The mentioned makes of equipment in this offer, are subjected to delivery schedule
and may vary in case not meeting the project deliveries. However, such change shall
be brought to the Purchaser’s notice before taking such decision.

6. All the pressure vessels will be according to ASME standard, div1, and will be
calculated, constructed, inspected and tested as per engineering procedures. Other
non-pressure equipment will be according to good engineering practices.

Q/ST/231222/AA/231360/R0 37
 4.2 SPECIFICATIONS OF UTILITIES

Sr. Description Unit Value

No
01 Steam
Dry saturated & free from foreign
Substances
For vacuum kg/cm2 9
For heating & sparging kg/cm2 3

02 Cooling water
0
Temperature C 32
Pressure kg/cm2 03
Hardness mg/liter 1.8 -
3.5
Chloride content mg/liter 50
pH content 7-8
Langelier saturation index -0.25 to
+0.25
Sulphate Ppm < 1000
Sodium bicarbonate Ppm < 200

03 Compressed air
Pressure kg/cm2 6
0
Dew point C -20

04 Power
Phases N 3
Frequency Hz 50
Volts V 400

The Specifications mentioned for utilities shall be confirmed by the Purchaser.

Q/ST/231222/AA/231360/R0 38
 4.3 MAKES OF STANDARD BOUGHT OUT

EQUIPMENTS

Sr. STANDARD BOUGHT EQUIPMENT MAKES OR BRAND

No.
1. Centrifugal pumps process Flowserve
2. Plate type heat exchangers Kelvion or danfoss
3. Centrifugal multistage pumps Grundfos / KSB
4. Centrifugal pumps for water KSB / Kirloskar
5. Positive displacement pumps Hydro-Prokav
6. Gear pumps Alfa pumps
7. Metering pumps Swelore engineering company
8. Electric motors TEFC Bharatbiajli or equivalent
9. Gear boxes Bonfiglioli / PBL / Roto
10. Cooling towers Paharpur cooling towers
11. Air compressors Atlas Copco
12. Variable speed drives Crompton / Delta or equivalent
13. Gasket material Uniklinger/ equivalent
14. Electrical cables Power or control Thermo Cables
15. Cable trays powder coated Vishwachaya
16. Aluminum sheets Hindalco
17. Hot insulation material Rockwool India limited
18. Thermal Oil Heater Isotex or equivalent
20 Vacuum System Mazda

INSTRUMENTS

Sr. No. INSTRUMENT MAKES OR BRAND

1. Flow indicators with transmitters Yokogawa / Kronhe or equivalent
2. Flow indicators Fitzer or equivalent
3. Level transmitters - Capacitance Type Sapcon / Precision
4. Level switches Sapcon / Waree
5. Pressure transmitters Waree / Wika
6. Pressure gauges Forbes Marshall
7. Temperature gauges - Dial type Forbes Marshall
8. Temperature transmitters Precision
9. Control valves Forbes Marshall / Dembla
10. Pressure switches Waree / Indfoss

Note – Above makes are w.r.t the equipment mentioned in Section 3 and subject to change
depending on availability.

Q/ST/231222/AA/231360/R0 39
 SECTION 5 : GUARANTEES
5.1 WARRANTY OF EQUIPMENT
Seller provides warranty on the supplied equipment towards mechanical, workmanship & other
standard bought out supplied equipment for a period of (18) eighteen months after delivery or (12)
twelve months after commissioning whichever comes first, subjected to operation / handling of
equipment by the Purchaser as per Seller’s instructions. This warranty however is not applicable for
normal wear and tear of any supplies.
Within the warranty period as specified above, upon notification and confirmation of defective part(s)
or equipment, Seller shall provide a free replacement on one for one exchange basis. However, the
cost incurred for performing the replacement work including the service of the skilled and unskilled
labor is not within Seller’s scope.

5.1 GUARANTESS FOR PROCESS

All the figures herewith apply simultaneously with +/- 5 % tolerance provided that the plant is operated
with the same feed-stock continuously for at least 24 hours under normal operating condition. The
methods of the determination of the guarantees shall be worked out between the Seller and the
Purchaser before commercial production during the commissioning of the plant. The criteria shall be
discussed for the process parameters.

A. FEED CAPACITY: 20 TPD BIODIESEL PLANT on 24 hour running basis

GLYCERIN TREATMENT SECTION: 3TPD

MODE OF OPERATION: BATCH

B. FEED SPECIFICATIONS:

Parameter Unit Used Cooking Animal Palm PFAD Acid oil

oil/crude tallow stearin SBO/SFO
Jatropha or
crude
vegetable oil
Moisture and % 5-8 1 0.2 0.03 0.2
insoluble
impurities
Colour Y+5R 45 40 6R Dark Dark
1” cell Yellow brown
Saponification N 192-215 192- 192 -205 204- -
value 202 210
IV Wije’s 100-102 30-56 30-34 45-56 -
Acid value 10 0.2 203 100-120
Unsap, matter % 0.5-0.8 1 0.3-0.9 0.5
Titre -- 40-51 NA 45-48
Phosphatide - - - - 0.5
Content

Q/ST/231222/AA/231360/R0 40
5.3 TYPICAL PRODUCT SPECIFICATIONS

a. BIODIESEL (FATTY ACID METHYL ESTTER)

Sr. Parameter Testing Unit Crude FAME Distilled FAME

No. Temp. Specification (Depends on feed
value quality)
1. Color Dark brown Colorless liquid
2. Density 150 C kg / m3 860 – 900 860 - 900
3. Viscosity 400 C mm2/s. 3.5 – 6.0 3.5 – 5.0
0
4. Flash point - C > 120 >120
5. Methanol content - % < 0.2 <0.1
6. Moisture - % < 0.05 <0.05
7. Sulphur - Ppm < 10 <10
8. Free Glycerin - % < 0.02 -
content
9. Total Glycerin - % < 0.25 -
content
10. Phosphorous - ppm <5 <5
content
11. Glyceride’s content - % < 1.2 -
(mono, di & tri)
12. Acid value - % < 0.5 <0.5
13. Contaminants - ppm < 24 -
14. Ester content - % 96.5 > 98
15. Cetane number - - > 51 >51

*Note: Above parameters of Distilled FAME comply BIS, ASTM OR EN specification

b. CRUDE GLYCERIN

Sr. No. Parameter Unit Crude FAME

Specification
value
1 Glycerin purity % 80 ±2%
3 Density kg / m3 1.2
4 Color NA Dark brown

c. RESIDUE/PITCH (FROM FAME DISTILATION)

Sr. No. Parameter Unit RESIDUE/PITCH

3 Density kg / m3 1.2
4 Color NA Dark brown

Q/ST/231222/AA/231360/R0 41
5.4 UTILITIES & CHEMICALS CONSUMPTIONS
Seller offers below consumption of utilities and chemicals during steady state operation of the plant
per metric ton of feedstock processed. The variation during measurement shall be +/- 10% and the
utilities to be measured for the sections offered by Seller. Methods for the determination of
Performance shall be worked out jointly between Seller and Purchaser.

1. PRETREATMENT OF FEEDSTOCK

Sr. Parameter Unit Was Bleac Glycerol Trans- FAME Rectifi

No. h. hing ysis cum Ester.+Meth Dist. & Of
De-acid. anol MeOH
Recti.+GT
A. UTILITIES
0C
1. Feed Oil / product 35 35 60 40 50 50
temperature
2. Steam consumption
Steam for heating Kg/T - 32 180 - 250

Live steam Kg/T 5 - - - -

Steam for vacuum Kg/T 155 230 -
Steam for filter Kg/T - 12 - - -
blowing
Energy G860 Kg/T - - 55000 - 70000 -
3. Installed power in KW 5 16 10 27 14 7
process house
(indicative)
4. Contaminated water M3/hr 31 - 41 -
in circulation
5. Clean water in M3/hr. - - 7 15 48 6
circulation
6. Process soft / RO M3/T 0.1 - 0.148 -
water
Chilled water in M3/T - - - - - 3
circulation
7. Air at 6 bar
for instruments nM3/ 2 2 2 2 2 2
hr
For filters nM3/ 1– - - - -
min 1.4

Q/ST/231222/AA/231360/R0 42
BIODIESEL PRODUCTION

Sr. Parameter Unit Wash. Bleac Glycer Trans- FAME Rect. Glyc Total
No. h. olysis Ester. Dist. & Of Treat Cons.
De- MeOH
acid.

CHEMICALS
1. Phosphoric Kg/ - 0.5 - - - - - 0.5
acid MT
2. Activated Kg / - 10 - - - - - 10
Bleaching MT
Earth
3. Methanol Kg / - - - 130 - - - 130
MT
4. Catalyst Kg / - - - 8 - - - 8
(Sodium MT
methoxide –
100%)
5. Citric acid dry Kg/ - - - 0.7 - - - 0.7
MT
6. Refined Kg/ - - 110 - - - - 110
Glycerin (on MT
100% FFA
Basis)
7. Hydrochloric Kg/ - - - - - - <47 47
acid by weigh T
of heavy phase

Q/ST/231222/AA/231360/R0 43
 SECTION 6 : TECHNICAL SERVICES
6.1 DOCUMENTATION

Seller shall provide two sets of the following documents in English as per schedule
mentioned below-
Proposed Equipment GA Layout Three weeks from the receipt of order along
with full advance
Foundation Drawings Three weeks from the receipt of approved
Equipment GA Layout from the Purchaser
Motor list, major equipment list and Utilities Four weeks from the receipt of order along
list with full advance
Process and instrumentation drawings Shall be discussed and mutually frozen by
Seller within Six weeks from the receipt of
order with full advance.
Electrical and instrument installation drawing Shall be discussed and mutually frozen by
Seller within Six weeks from the receipt of
order with full advance.
Operating instructions & Maintenance Two weeks prior to start-up of
Manual Pre-commissioning activity.

6.2 SPECIALIST SERVICES

Seller shall provide services for the installation and piping of the equipment of the plant. Seller shall
also provide services for the commissioning on completion of the installation, piping and testing as
per the seller’s specification.
6.3 ADDITIONAL DOCUMENTATION
1) Key site layout of the plant
2) Equipment layout drawing of process house indicating the load detail & individual equipment
mounting and water filled load.
3) Steel structural details:
Details bill of material of all the columns, beans layout, trusses, louvers and purling staircases
chequrred plates is to be furnished by Seller to Purchaser.
DVC will furnish all the details of steel to be purchased by Purchaser. AC sheeting and side sheeting
is to be completed by Purchaser.
4) DVC will furnish foundation details of the following:
(i) Foundation of the footing of the columns
(ii) Distillation column foundation i.e. ring beam at 2.5
(iii) Foundations of cooling towers and cooling tower basin drawing.
(iv) Foundations of the pumps outside the process house Cooling water conveying, conveying or oil
transfer.
5) Process and instrumentation diagram of all process system
6) Operating procedures, method for the analysis like cooling water conveying, and feedstock

Q/ST/231222/AA/231360/R0 44
6.4 SERVICES FOR INSTALLATION & COMISSIOING

A. SELLER’S SCOPE

1. Provide skilled personnel to carry out installation of equipment and erection material
supplied by seller at the Project site for the activities described below.
2. Undertake erection in areas of mechanical & piping and of equipment & accessories
supplied by Seller as mentioned in this proposal.
3. Undertake final alignment of all equipment and pressure testing of all pipe lines after erection.
4. To carry out insulation and cladding of equipment, tanks and piping inside the plant.
5. Undertake electrical cabling work and instrument & control panel installation.
6. Carry out mechanical runs of all the plant, machinery and equipment.
7. Provide welding machine, cutting set and consumables like welding rod, gas, etc.
8. Provide skilled & unskilled man-power support for the erection, piping & commissioning activities

Note: Estimated Period: 12 Weeks

B. PURCHASER’S SCOPE

1. Carry out of complete civil and supply, including site grading and preparation, factory and utilities
buildings, equipment and machinery foundations, rack foundation within plant
Battery limits.
2. Carry out of casting of foundations and grouting of base plates of equipment.
3. The equipment will be installed on the foundations, aligned and foundation bolts inserted by us
before the same are released to you for grouting and finishing.
4. Provide lifting equipment like chain block, crane, etc.
5. Carry out building lighting and earthing network.
6. Supply of uninterrupted facilities like power, steam and water at specified points.
7. Provide site office with facilities to keep and safeguard all engineering documents as well as
special tools belonging to us.
8. Free issue of all machinery, equipment, components and accessories kept by Purchaser to
Seller as and when required to carry out erection.
9. Provide Personal Protection Equipment like Helmet, safety glasses, belt, etc.
10. Obtain all necessary licenses, permissions, and sanctions such as approvals by Factory
inspectorate, Boiler inspectorate, explosive authorities, electrical inspectorate, pollution
authority and other statutory authorities.
11. The safety and fire-fighting facilities at project site.
Food, Accommodation, Local Conveyance to all the personnel of Seller and Seller’s Sub-
contractor.

Q/ST/231222/AA/231360/R0 45
SECTION 7: BATTERY LIMITS AND EXCLUSIONS
7.1 BATTERY LIMITS OF PROCESS

A: PRE-TREAMENT

FOR ACID OIL:

Acid oil is to be provided by the Purchaser at the Pump P301.

WASHED OIL:
Washed oil line is to be terminated at the outlet of the Tank T303 by Seller.

UCO/ TALLOW:
UCO / Tallow line is to be provided by the Purchaser at the strainer F601 near suction of the
pump P601.

BLEACHING EARTH:
Bleaching earth as per specifications of Seller is to be provided by the Purchaser at the tank
DH632 of bleaching plant.

SPENT EARTH:
Spent earth is to be left at the ground floor via chute below PLF601 & PLF602. Purchaser to
make arrangement for further disposal.

DEACIDIFIED OIL:
De-acidified oil line is to be terminated by Seller at the outlet of the Heat Exchanger E805.
Purchaser to make arrangement of storing de-acidified oil.

FATTY ACID DISTLLATE:

Fatty acid distillate line is to be left by Seller at the outlet of FV804.

B. BIODIESEL PRODUCTION

PRETREATED OIL:
Pretreated oil line is to be provided by the Purchaser at the suction of pump P1801

SODIUM METHYLATE SOLUTION:

Sodium methylate solution is to be provided by the Purchaser at the tank T1851.

METHYL ALCOHOL:
Methyl alcohol is to be provided by the Purchaser at the tank T1850.

CITRIC ACID:
Citric acid solution is to be provided by the Purchaser at the tank T1811.

GLYCERIN:
Crude Glycerin line is to be terminated by Seller at the outlet of heat exchanger E1814.

Q/ST/231222/AA/231360/R0 46
 PROCESS WATER:
Process Water is to be provided by purchaser at inlet of tank T333.

FAME:
FAME line is to be terminated by Seller at the outlet of the heat exchanger E2006.

PITCH (FROM FAME DISTILLATION):

Pitch line is terminated by seller at the outlet of heat exchanger E2004

WASH WATER:
Wash water line is to be left by Seller at the outlet of pumps P307 & P1825A. Purchaser to carry
the same for further treatment.

7.2 BATTERY LIMITS OF UTILITIES

CLEAN & CONTAMINATED COOLING WATER LINE:

Contaminated water line for make-up, foundations & pond is provided by Purchaser. Cooling tower
and cooling water conveying pump and piping is in seller’s scope.
(*Note: Cooling Tower must be located within 10 meters from the process house)

STEAM:
Steam line as per Seller’s specification is to be made available by the Purchaser at the inlet of
Pressure Reducing Stations in Process House.
*Note: Steam Boiler, Boiler Feed water & condensate water and its piping in in Purchaser’s scope.

INSTRUMENT AIR:
Instrument air as per Seller’s specification within the Process House, is to be provided by Seller.
(Compressor & receiver in Seller’s scope)
POWER:
Power cable along with the earthing shall be connected by the Purchaser at the main isolator of the
common control panel supplied by the Seller.

FLUE GAS EXHAUST:

Flue gas exhaust from high temperature media generation unit is to be connected by Purchaser by
suitable duct. Ducting and Chimney is Purchaser’s scope.

EARTHING SYSTEM
Earthing cable and instrument earthing is to be provided by Purchaser up to the electrical & Control
Panel.

Q/ST/231222/AA/231360/R0 47
6.4 KEY EXCLUSIONS:

1. Civil, Steel structure and its erection

2. Interconnections & piping of storage tanks and up to the battery limits
3. Equipment and piping support material along with piping rack & structure Or bridge
4. Bulk storage tanks for the products, by-products
5. Bulk storage for chemicals and consumables.
6. Un-interrupted power supply for PC, AC room, table and chair
7. Interconnection of hot well and cooling tower basin (Civil)
8. Plant lighting
9. Hotwel
10. Effluent treatment plant
11. Chilling Unit
12. Transformer, power distribution and cables up to the control panel
13. Steam boiler and distribution up to process house & tank farm
14. Safety & Firefighting equipment.

Q/ST/231222/AA/231360/R0 48
 6.5 EXCLUSIONS FROM THE SCOPE OF SELLER

Sr. Description of Exclusion

No.
1. Civil work of any nature ,buildings, steel structural design, material supply and
installation, pipe supports within and outside refinery, bulk storage facilities with
necessary interconnecting piping and electrical, excavations, concrete work masonry,
anchorage , AC sheeting, foundations, hot well for barometric water, clean and
contaminated cooling towers ,pumps ,piping with its civil work like basins, foundations
etc., equipment as well as plant lighting facilities like air conditioning, ventilation
,sanitary and potable water, waste water drainage, firefighting system are excluded
from the scope of Seller.
2. All technical personnel like process specialists, maintenance engineers, plant
operators, laboratory chemists, unskilled labor required for the starting up of plant are
excluded from the Seller’s scope however the operational support shall be extended
by the Seller after commissioning on paid basis.
3. All piping outside the specified & explicitly mentioned under Section 7- Battery Limits
and Exclusion of this proposal, is excluded from the scope of the Seller.
4. Steam generation equipment (boiler) & distribution, storages tanks of tank yard, &
filling section are excluded from the scope of supply of the Seller.
5. Electricity measurement (CTPT), HT panel, Transformer, LTDB and power distribution
LT cables , cable trenches are excluded from the scope of the Seller
6. Effluent Treatment Plant, liaison services, and disposal of effluents are excluded from
the scope of the Seller.
7. Laboratory for the analysis of process parameters, laboratory equipment, chemicals
are excluded from the scope of the Seller.
8. First charge for lubricants, gear or hydraulic oil, wherever applicable is excluded from
the scope of Seller.
9. Necessary spare-parts (excluding wear parts) required during commissioning are
excluded from the scope of the Seller and will be supplied at chargeable basis.
10. Painting of equipment at site is excluded from the scope of the Seller.
11. All kind of liaison and approvals, sanctions from Government or Semi government
authorities required for project related activities are excluded from the scope of
supply of the Seller.
12. Unloading of material at project site are excluded from the scope of supply of Seller
and the cost for the same is to be borne by the Purchaser.
13. Any other point not covered in above exclusions and not covered under the scope of
supply is excluded from the scope of the Seller.

Q/ST/231222/AA/231360/R0 49
 SECTION 7: COMMERCIAL
6.1 PRICE SUMMARY

Sr. No. Description Price In INR

A EQUIPMENT SUPPLY
3.1 Washing
3.2 Bleaching
3.3 Glycerolysis cum De-acidification
3.4 Transesterification
3.5 Methanol Rectification
3.6 FAME Distillation
3.7 Crude Glycerin Treatment
3.8 Control panel
3.9 Erection material
B UTILITIES
3.10 Thermic Fluid Heater
3.11 PRS, Air Compressor, Air Receiver
3.12 Cooling Towers with Pumping
4,95,00,000
B SUPERVISORY SERVICES
Services for Installation & Commissioning 25,00,000

A. PRICE BASIS
• The above-mentioned prices are EX-WORKS, JEJURI or SUB-SUPPLIERS.
• The charges towards packing & forwarding are included in price.
• GST, transportation and transit insurance are excluded and to Purchaser’s account.
• The above prices are in reference to Seller’s equipment and plant design parameters, any
deviation in later stage of the project will be at additional price settled mutually.
• The charges towards third party inspection will be extra and to be borne by Purchaser.
• Facility for internet, email and telephonic communication for Seller’s personnel at Site to be
provided by Purchaser
• Purchaser shall complete all site activities before arrival of installation & commissioning
engineer / team at site.
• All Travel and stay expenses including return tickets, airport transfer, local conveyance,
accommodation, food, laundry, etc. for Seller’s personnel or Seller’s subcontractors, to be
provided by Purchaser.
• Medical facility in case of emergency to be provided by Purchaser.
• During installation any failure of the machines, purchaser has to provide support and if possible,
arrange the same locally for which charges has to be paid by seller.

B. STATUTORY VARIATION
The above prices quoted are based on the prevailing rate of the tax and duties. Any Additional
cost due to variation in rates or structure of tax and duties, new implementation of taxes and
duties shall be borne by the Purchaser.

Q/ST/231222/AA/231360/R0 50
C. TERMS OF PAYMENT

For Supply
40% Advance to be credited to Seller’s account on the date of the purchase order by Purchaser.
Balance along with all applicable taxes, duties, levies and charges against Proforma Invoice
before dispatch

For Services
40 % advance along with order and balance 60% against progressive bills including all
applicable duties, taxes and any other levies.
For delay beyond the agreed period, for reasons not attributed to the Seller, services will be
charged additionally @ 15,000 INR/man-day.

D. SELLER’S BANK DETAILS

Bank: SVC COOPERATIVE BANK LTD
AUNDH, PUNE
Name of Account Holder’s: DVC PROCESS TECHNOLOGISTS
Account No: 110319940000020
Type of Account Current
GST NO 27ADAPC8592L1Z7
IFSC Code SVCB0000103

E. VALIDITY
Our proposal is valid for your acceptance till one month from the date of this proposal and is
subject to our confirmation thereafter.

F. DELIVERY
For supply of equipment: The goods shall be ready for dispatch in 20 weeks on Ex-Works
Basis from the receipt of confirmed Purchase Order on Seller along with advance payment.
The Partial shipment of material shall be allowed considering the exhaustive scope of supply.

G. INSPECTION
The Purchaser is free to carry out inspection at Seller’s works OR workshops of sub-suppliers
of seller on advance notice of minimum 5 days prior to inspection. The cost towards lodging,
boarding and conveyance required for inspection shall be borne by the Purchaser. All third party
inspection cost to be borne by Purchaser.

H. CANCELLATION
In case of cancellation of the order the Purchaser is liable to compensate for the cost incurred
on work carried till the date of the cancellation by Seller.

Q/ST/231222/AA/231360/R0 51
I. FORCE DE MAJEURE
Force majeure shall mean any circumstances beyond the reasonable control of the Seller
which prevent or impede the due the performance of the Agreement including but not limited
to war or hostilities or war like conditions such as acts of God, Riot or civil commotion, epidemic,
famine, earthquake or flood, fire or other natural physical disaster or denial of use of any railway
port or airport or shipping services or other means of transport or strike lockout or other industrial
action.
Federal, State, local Municipal legislation, Ruling or Ordinance, notice order or any situation
affecting the Agreement. The mere shortage of labor or materials or utilities will not constitute
force majeure unless caused by circumstances which are themselves force majeure. The Seller
shall not be held responsible for any loss or damages caused by such reasons.

J. TRANSPORTATION & INSURANCE

Transportation of all the equipment to be supplied shall be arranged by Purchaser from location
of delivery to designated project site. The charges for loading, transportation and unloading at
site shall be paid by Purchaser, extra at actual.
Insurance charges for the transit and storage at site till commissioning period will be arranged
by Purchaser. The Purchaser shall open the policy and shall inform to us prior to dispatch of
the equipment from our works/suppliers.

K. EXCESS MATERIAL
The erection material, wrong supplies due to mistakes & tools tackles after completion of the
work will be property of the DVC. Purchaser shall allow DVC’s representative to take back such
material to DVC’s workshop.

L. JURISDICTION
All disputes and differences arising out of or connected with this transaction failing amicable
settlement shall be referred to jurisdiction of courts of Pune or the place is to be decided jointly
if such disputes occur.

M. THE GENERAL TERMS & CONDITION OF SALE

The attached document for General Terms and Conditions form the part of this quotation

FOR
DVC PROCESS TECHNOLOGISTS

ATUL AMGAONKAR KIRAN PALKAR

Q/ST/231222/AA/231360/R0 52