Quality Control Laboratory Manual
Quality Control Laboratory Manual
Laboratory Tests
The purpose of this Laboratory Manual is to standardise & provide test methods
as per the requirement of Clients / Cilents Consultant. The manual is brief &
made user friendly. It also includes formats which can be incorporated to record
the results & thus in toto is a ready reckoner.
This laboratory manual was initiated by [Link] Joshi, Q.A / Q.C Manager
under the guidance of Mr. N.D. Sadri Management Representative (ISO
9001:2000) with ISO - Cell at H.O. The standard practices & methods of testing
& measurement will be updated by ISO Cell (H.O) from time to time based on the
feedbacks received from the Regional ISO Coordinators across the country so as
to be in tune with our Quality Policy & Objectives.
The update of this manual shall remain a continuous effort to bring Continual
Improvements into the Quality Management Systems of SPCL.
Note :
1) This document is property of Shapoorji Pallonji & [Link] and must be surrendered to the Document Controller / M.R. on
transfer or cessation of employment.
2) While every effort has been made to ensure the accuracy of the information presented in this Lab Manual, neither SPCL nor
its employees can accept responsibility for any loss or damage incurred in connection with the use of the contents.
ACKNOWLEDGEMENT
1. Mr. Hemant G. Joshi QA/QC Manager (Poona R.O)
2. Mr. N. D. Sadri Management Representative (ISO 9001:2000)
3. Mr. J. P. Rao Additional G.M (H.O)
4. Mr. Omkar S . Bendre Asst. Engineer Quality (ISO Cell)
5. Mr. Prashant P. Bhavsar Asst. Engineer Quality (ISO Cell)
INDEX
Page No.
I - General :
II - Procedures :
1. General 59
2. Calibration Plan 60
3. Procedure for Verification of Equipments 61 to 64
4. Calibration of Batching Plant 65 to 66
5. List of Abbreviations 67
6. Definitions 68 to 69
7. Ammendment 70
CHAPTER 1
GENERAL
SCOPE OF THE MANUAL :
This is a users manual for material testing and sampling at site. The scope of this
manual is pertaining to SPCL procedure Document No 1000 GP04 038 and which
includes data, procedures , formats as following :
1. Setting up of infra-structure required for testing various regular material as per the
list given in Table-1. Infra will comprise of :
a. Enclosed area for conducting the tests at desired conditions.
b. Equipments for the various tests as listed in table-2 .
c. Filing rack / cabinet for keeping the records and table /chair.
d. Curing tank for concrete cubes.
e. Trained QC engineer & /or Trained Lab technician shall be deputed for the
site.
2. Any other tests on same material or the material other than listed will have to be
done in external laboratory. The records of such tests will be maintained at the
laboratory. ( List Of Tests as per Table-1a )
3. Any approved samples, test pieces will be maintained at the laboratory.
4. Procedure for calibration of test equipments & validation of measuring
aids (GP 04 043 )
1
TABLE 1
2
TABLE 2
4
TABLE 3
List of Laboratory Equipments :
6
Table 4
7
TABLE 5
10
Acceptance Criteria Graph ' Zone Wise ' for Sand
Zone-I
Zone-II
Zone-III
Zone-IV
Upper limit
600 mcn %
ZONES passing
Lower Limit
ZONE - I GRADING
ZONE-I GRADING CURVE
Sieves % Passing
2.36 mm 60 95 80
60
1.18 mm 30 70
40
600 mcn 15 34 20
300 mcn 5 20 0
150 mcn 0 10
1.18 mm
2.36 mm
4.75 mm
150 mcn
300 mcn
600 mcn
10 mm
% Passing
Lower
SIEVES SIZES % Passing
Upper
ZONE - II GRADING
Sieves % Passing ZONE -II GRADING CURVE
Lower Limit Upper limit
10 mm 100 100 120
4.75 mm 90 100 100
% PASSING
2.36 mm 75 100 80
1.18 mm 55 90 60
600 mcn 35 59 40
300 mcn 8 30 20
150 mcn 0 10 0
1.18 mm
2.36 mm
4.75 mm
150 mcn
300 mcn
600 mcn
10 mm
% Passing
Lower
% Passing
SIEVE SIZES
Upper
11
ZONE - III GRADING
Sieves % Passing ZONE -III GRADING CURVE
Lower Limit Upper limit
10 mm 100 100 120
4.75 mm 90 100
100
2.36 mm 85 100
1.18 mm 75 100
% PASSING
80
600 mcn 60 79 60
300 mcn 12 40
150 mcn 0 10 40
20
0 % Passing
1.18 mm
2.36 mm
4.75 mm
150 mcn
300 mcn
600 mcn
10 mm
Lower
% Passing
Upper
SIEVE SIZES
ZONE - IV GRADING
Sieves % Passing
Lower Limit Upper limit ZONE -IV GRADING CURVE
10 mm 100 100
4.75 mm 95 100 120
2.36 mm 95 100 100
1.18 mm 90 100
% PASSING
80
600 mcn 80 100
60
300 mcn 15 50
40
150 mcn 0 15
20
% Passing
0
Lower
1.18 mm
2.36 mm
4.75 mm
150 mcn
300 mcn
600 mcn
10 mm
% Passing
Upper
SIEVE SIZES
GRADING OF AGGREGATES :
Seives used for Coarse Aggregate : 80mm, 40mm, 20mm, 10mm, 4.75mm.
Seives used for Fine Aggregate : 10mm, 4.75mm, 2.36mm, 1.18mm, 600micron, 150micron.
12
CHAPTER 2
PROCEDURES
CHAPTER 1
To have convenient working and storage of records and equipment area is required
more than 12 sq. m. Working platform of approx 3 m long and 700 mm wide will be
required. 2-15Amp / 2-5 Amp electric points other than regular lighting /fan points are
required.
Curing tank :
Size of Tank is depend upon number of cube sets taken at decided frequency. Cubes
to be arrange in stack of three and day wise. Tank should have separate
compartments for 7 days and 28 days cubes. Thus for daily avg 3 sets
( 18 cubes ) of cubes, tank will have plan dimensions 1250x900 for 7 day
compartment and 3000x1250 for 28 days compartment. Clear Depth of tank shall be
fixed one at 750 mm which includes free board. For any increase and decrease of
sampling size can be alter considering cube stacking [Link] tank should
be kept clean and free from dust particles & micro organisms growth. Water should be
changed every 7th [Link] tank should be covered with a lid.
13
14
CHAPTER 2
Certain work Culture and precautions are required to upkeep equipments and
samples :
1. Cube Moulds :
Shall be always used in whole set. ( 1 set of 6 nos of moulds along with
spanner )
Components of mould sets shall not be interchanged.
All bolts shall be checked for threading and shall be oiled from time to time after
cleaning.
Only fixed spanners shall be used for bolts.
Moulds shall be checked for dimensional correctness & daigonal check
everytime before use.
Moulds shall be thoroughly cleaned after the use and lightly oiled.
2. Slump Cone :
Shall be always ready in complete set including tamping rod and trowel.
Shall be cleaned and lightly oiled from inside after the use. Before use oil shall
be wiped out.
Cone shall be well fitted with base so as no leakage of slurry takes place.
3. Compression Testing machine :
Have authentic calibration report handy.
Always use designated oil in machine
Keep platens in clean condition.
CTM shall be properly fixed in position and shall be in level.
Keep adequate clear working area in front of CTM.
Check dial gauge pointer is on zero before testing.
Max. Loading on CTM shall be 85-90% of Rated Capacity.
4. Curing Tank :
Water in tank shall be clean and change at frequent intervals. The water shall
not be allowed to use for any other purpose.
Water shall always cover top of cube by at least 50-75 mm.
Water temperature must be controlled during winter.
15
5. Concrete Cubes :
Casting of cubes shall be done at well designated place and level / hard
platform.
Freshly cast cubes shall be away from any vibrations and shocks. They will be
covered by wet gunny bags immediately after casting.
Cubes shall be correctly mkd for number / location , mix, date etc.
Cubes shall be placed in tank in correct sequential manner so as to locate them
easily.
While handling cubes, utmost care to be taken not to damage edges / corners.
Always cast extra cubes to deal with serious situation.
6. Sieves :
Sieves shall be always kept in set in proper sequence and vertically arranged.
Fine sieves can get damaged due to incorrect use. Always clean sieves by
brush and remove stuck particle by forceps or needle. Do not bang on the
mesh.
Sieves shall be kept clean and dry.
7. Core Cutters :
Use Cutters in set of three.
Do not use cutter in coarse grain /gravelly soil.
8. Weighing Balance :
Keep balance in clean condition. De-dust it frequently.
Always cover electronic balance when not in use.
Balance shall be loaded to max 90% of rated capacity.
Balance shall be kept on level platform. Remove the pan when not in use.
Do not weigh with Fan on. Breeze affects the accurate weighing.
9. Samples :
All samples shall be kept at laboratory in designated area in proper pack ,
container.
All samples shall be tagged for name, sources, collection points and dated.
16
CHAPTER 3
18
CONCRETING IN HIGH TEMPERATURE REGIONS (IS : 7861-1)
Ice is added
Water Cement Ratio should not change with addition of Ice
Adjust Quantity of water accordingl to the volume of melting ice
Sample size for required test shall be made as per quartering method
described above.
Care to be taken that no fines are lost in the operation as soil properties mostly
depend on them for testing.
19
BRICKS ( As per IS : 5454 ) :
Sampling a lot which shall contain maximum 50000 bricks. In case a
consignment has bricks more than 50000 bricks of same classification, size
and manufactured under relatively similar conditions, it shall be divided into lots
of 50000 bricks or part thereof.
Sampling from the stack When it is necessary to take sample from the stack,
the stack shall be divided into number of real or imaginary sections and
required number of bricks shall be drawn from each section. For the purpose
bricks in the upper layers of the stack shall be removed to enable units to be
sampled from places within the stack.
Sample size For Visual / Dimensional Characteristics
Lot Size of bricks Sample size for Individual brick Sample size For group of
Check 20 bricks Check
2001 10000 20 40
10001 35000 32 60
35001- 50000 50 80
Sample size For Physical Characteristics
Samples shall be drawn for these tests from above sample lot.
20
CHAPTER 4
21
CHAPTER 5
Aim:
To Check, Inspect Conformity of RMC Concrete which is manufactured outside and
supplied at site.
Pre-requisites :
RMC supplier shall be given prior information by the site regarding following:
1. Grade of Concrete.
2. Minimum Cement or cementetious material contents. ( Client Approval required )
3. Slump required and tolerances in slump. (Guidelines IS : 4926. Client Approval
required)
4. W/C ratio.
5. Method of Concreting ( Manual, Bucket or Pumping )
6. Control of temperature if required shall be specified in case of Mass concreting.
7. Quantity of Concrete required Total, Phasewise, daywise.
8. Supplier shall know site condition , distance and shortest route to the site from his
plant
9. Decision shall be made between Supplier and Site regarding tests and method to
be adopted. ( Client Approval required )
10. Frequency and Acceptance criteria of each testing shall be decided before start. (
Client Approval required )
NAME OF PROJECT :
Name of Client :
Name of Consultant :
S Name Vide Time Time Grad Locat ID of Slum Temp of Random Date of
r of Delivery Mixer discharg e of ion of Cube p in fresh testing Testin
N Suppli Challan/ Left e Conc Use s mm Concret of g for 7
o er Date Mixin complet rete e recd. Aggrega days
. g ed te
Plant OK?
Yes / No
Date of Weight Area of Stren 7 days Strength 28 days Sign of Sign of Remarks
Testing of Cube gth at Avg at 28 Avg Contract Client /
for 28 Cubes Surface 7days Strength days in strength or Consulta
days in Kg cm2 in in kg/cm2 in nt
kg Kg/cm2 kg/cm2
/cm2
Remarks :
This format shall be used as Register. Preferably 7 days and 28days readings
shall be entered in different rows.
24
CHAPTER 6
Apparatus :
Cube moulds fitted tightly on base plate (size in mm 150x150x150) in required set (
One set comprises of 6 moulds.)
Smooth Tamping rod of size 16 mm dia and length of 600 mm with one rounded edge.
Trowels small and large.
Collection pan, scoop, measuring scale etc.
Flat working platform of adequate size.
Record :
Details of Cubes thus sampled shall be entered serially in Cube Register maintained
for testing compressive strength.
The number of cube samples cast shall also be entered in pour card with proper
traceability to cube register.
26
CHAPTER 7
27
Calculations:
Compressive Stress ( c ) in N / mm2 or Kg / cm2 as below :
Recording :
Record is generated as per the sample format given in chronological order.
28
FORMAT FOR CONCRETE CUBE REGISTER
NAME OF PROJECT :
Name of Client :
Name of Consultant :
Remarks :
This format shall be used as Register. Preferably 7 days and 28days readings
shall be entered in different rows.
29
CHAPTER 8
( As per SP-23 )
2 Std Dev shall first calculated for minimum 30 nos of results, n = No of results considered
4 Calculate value of ( Xi - Xbar ) for each result and Calculate square of ( Xi -Xbar )
30
Total Xi = Total Xn = (I)
Xbar n = 30
S.D. = (I)
30
UPDATING THE SD FOR SUBSEQUENT SETS
OF RESULTS
55
Total Xi = Total Xn = ( II )
Xbar n = 25
S.D. = ( II )
Total Xn = Xn( I ) + Xn ( II )
Total n = 29 + 24
31
CHAPTER 9
( Ref : A. M. Neville )
Aim : To determine Silt content in Sand by volumetric method field test.
Apparatus :
Measuring cylinder 250 ml
Common Salt.
Procedure :
Prepare 1% solution by mixing 10gms of common salt in 1litre of water.
Put this solution in measuring cylinder upto the mark of 50 ml.
Add Sand as received in the cylinder till its level reaches 100 ml.
Add Solution again so that the mixture reaches the level of 150 ml.
Cylinder top is now covered with the palm of hand and shake vigorously by
turning upside down.
Then allow it to stand undisturbed for 3 hours.
Take reading for top layer of Silt ( A ) and layer of Sand ( B ).
Calculations :
Silt content % Volumetric = (A / B ) x100
Reporting :
% Silt contain (Volumetric ) shall be reported in whole number.
Note : This method is approximate and conversion to weight basis ( which is
acceptance criteria ) is dependent on fineness of material. However 8% volumetric
content is treated as reliable. It was suggested that weight ratio is obtained by
multiplying volumetric ratio by for natural sand and for Crushed sand.
Accurate test when 8% limit of silt contain is exceeded can be done as per IS method
of Sedimentation if required.
Format to be Used :
It shall be recorded in Sieve Analysis for Fine aggregate. Alternatively separate
register for silt contents.
32
CHAPTER 10
Aim : To determine the properties of Fine aggregate for size and distribution by
calculating Fineness modulus and deciding Grading Zone.
Apparatus :
Drying Oven
IS Sieves 10 mm, 4.75mm, 2.36 mm, 1.18 mm, 600 micron, 300 micron, 150 mm,
pan.
Weigh scale to the accuracy of 1g.
Brush , Metal trays etc.
Procedure:
Sample of sand shall be collected as given earlier.
Sieves shall be cleaned and arrange in sequence in descending order. Pan
shall at the lower most end and Lid on top.
Take around 1 kg of sample and dry it in oven at temp of 100-110 deg C.
Dried sample shall be then weighed ( 1 kg preferably) and sieved successively
on sieves starting with 10mm and then through 150 micron.
Each sieve shall be shaken at least for two minutes on clean tray until no more
trace passes.
Motion shall be varied like back and forth, left to right, circular clockwise and
anti-clockwise and with frequent jarring.
Material shall not be forced through the mesh. Lumps in fines shall be broken
against the wall of sieve.
Sieves shall be brushed from underneath of mesh and pass on to the next.
On completion of sieving, material retained on each sieve is to be weigh
separately.
33
Calculations :
Fineness Modulus : Add values of Cumulative % Retained on each sieves and
divide by 100. (Normally accepted limit of FM is value between 2.2 to 3.2.
Higher value of FM indicates Coarser sand whereas lesser value indicates
Finer one. )
Grading Zone of Fine Aggregate Value is shown between I to IV. Where
zone- I is associates with Coarser Fine aggregate and Zone IV is Finer.
Zones are decided from values of 600 micron passing % in sieve analysis.
( Refer Table-4 of IS : 383 )
Zone I 15-34%, Zone-II 35-59 %, Zone-III- 60-79%, Zone-IV- 80-100%
Reporting:
The cumulative % by weight of the total sample passing each sieves, to the
nearest whole number.
Or
The % by weight of the total sample passing one sieve and retained on the next
smaller sieve to the nearest 1 decimal.
Calculate F.M. of the material and decide Grading Zone of material.
Format to be Used :
Format of Sieve Analysis of Fine Aggregate shall be used.
34
FORMAT FOR SIEVE ANALYSIS FOR FINE AGGREGATE
Name of Client :
Name Of Consultant :
Tested by : Checked by :
Date Date
35
CHAPTER 11
Aim : To determine the properties of Coarse aggregate for size and grading
distribution ( Nominal 20mm/12.5or10 mm metal).
Apparatus :
Drying Oven
IS Sieves 40 mm, 20 mm,16 mm, 12.5 mm, 10mm, pan. for Analysis of 20 mm
metal
IS Sieves 20 mm, 16 mm,12.5 mm, 10 mm, 4.75 mm ,2.36mm pan - for Analysis of
10/12.5 metal.
Weigh scale to the accuracy of 1g.
Brush , Metal trays etc.
Procedure:
Sample of aggregate shall be collected as given earlier.
Sieves shall be cleaned and arrange in sequence in descending order. Pan
shall at the lower most end and Lid on top.
Take around 5 kg of sample and dry it in oven at temp of 100-110 deg C.
Dried sample shall be then weighed ( 5 kg preferably) and sieved successively
on sieves starting with 40mm and then through 4.75mm( For 20 mm down
aggregate size ) and through 2.36 mm (For 12.5/10 mm down aggregate size) .
Each sieve shall be shaken at least for two minutes on clean tray until no more
trace passes.
Motion shall be varied like back and forth, left to right, circular clockwise and
anti-clockwise and with frequent jarring.
Material shall not be forced through the mesh. But for coarser than 20mm
particles, placing is permitted (passing particles through sieve opening
manually).
Sieves shall be brushed from underneath of mesh and pass on to the next.
On completion of sieving, material retained on each sieve is to be weigh
separately.
36
Reporting:
The cumulative % by weight of the total sample passing each sieves, to the
nearest whole number.
Or
The % by weight of the total sample passing one sieve and retained on the next
smaller sieve to the nearest 1 decimal.
Check for permissible limits for passing.
Format to be Used :
Format of Sieve Analysis for Coarse Aggregate shall be used.
37
FORMAT FOR SIEVE ANALYSIS FOR COARSE AGGREGATE
Name of Client :
Name of Consultant :
Water Absorption % : %
Date Date
38
CHAPTER 12
39
The contents of Pychnometer bottle shall be then emptied in the tray ensuring
all aggregate is transferred properly.
Pychnometer bottle shall be then rinsed and filled up with distilled water fully,
dried from outside as above and then weighed ( Weight C g )
The sample of aggregate as collected above shall be drained and decanted
through filter paper and retained material on filter paper shall be returned to the
sample.
The sample then shall be placed in oven at 100 to110 deg C for 24 +/- hrs.
During this period it shall be stirred occasionally to facilitate drying.
It shall be cooled in air-tight container and weighed ( Weight D g )
Such two tests shall be made
Calculations :
Specific Gravity = D/ A(BC)
Water Absorption = 100 ( A D ) / D
( % of Dry weight)
Reporting :
Individual and mean results shall be reported and grading of the aggregate shall be
stated.
Format to be Used :
Format of Determination of Specific Gravity shall be used.( For Sp. Gravity )
Format of Determination of Water Absorption of Coarse and Fine Aggregates
shall be used. ( Water Absorption)
40
FORMAT FOR DETERMINATION OF WATER ABSORPTION OF COARSE & FINE
AGGREGATE
( IS : 2386-III )
Name of Client :
Name Of Consultant :
Tested by : Checked by :
Date Date
41
FORMAT FOR DETERMINATION OF SPECIFIC GRAVITY
( IS 2386- III )
Name of Client :
Name of Consultant :
Sr Description Sample
I II
1. Weight of Saturated
Surface-dry sample, A in
g
2. Weight of Pychn. Bottle
+ Sample + Water , B in
g
3. Weight of Pychn. Bottle
+ Water, C in g
4. Weight of Oven Dried
Sample, D in g
5. Sp. Gravity = D / A ( B
C)
Tested By : Checked By :
Date Date
42
CHAPTER 13
Aim:
To determine the Flakiness of particles of Coarse Aggregate greater than 6.3 mm
size.
Apparatus :
Balance with accuracy of 0.1% of weight of sample
Flakiness Index Gauge
All other as per Sieve analysis.
Sample :
It shall be taken from retained material from Sieve analysis preferably and should
have at least 200 pieces of any fraction.
Procedure :
Each sample of 20 mm and 10mm shall be taken from retained fraction.
Each fraction shall be gauged in turn for thickness on metal gauge.
The total amount passing the gauge shall be weighed.
Report :
The flakiness Index is the total weight of the material passing the various
thickness gauges; expressed as a % of the weight of total sample gauged.
Format to be Used :
Format for Flakiness Index shall be used.
43
FORMAT FOR FLAKINESS INDEX OF COARSE AGGREGATE
Name of Client :
Name Of Consultant :
Tested by : Checked By :
Date Date
44
CHAPTER 14
Format to be Used :
Format for Elongation Index shall be used.
45
FORMAT FOR ELONGATION INDEX OF COARSE AGGREGATE
Name of Client :
Name Of Consultant :
Tested by : Checked By :
Date Date
46
CHAPTER 15
Aim:
To calculate aggregate Crushing value by testing aggregate passing 12.5 mm sieve
and retained on a 10 mm sieve. ( This is Alternative method to Aggregate Impact
Value.)
Apparatus:
15 cm dia steel cylinder with plunger and base plate
tamping rod 16 mm dia and 600 mm long with one end rounded.
Weighing balance of accuracy 1 g
I.S sieves 12.5 mm , 10 mm & 2.36 mm.
Drying Oven, CTM
Procedure :
Take sample of aggregates by sieving through 12.5mm and retained on 10mm.
The aggregate shall be tested in surface dry condition. If dried by heating, the
period of drying shall not exceed 4 hours and temp shall be 100-110 deg C.
Sample shall be cooled down to room temperature before testing. Take
approximately 6 kgs of sample.
The quantity of the sample shall be such that the depth of material in the
cylinder after tamping shall be 10cms.
Cylinder shall be filled up in 3 layers and each layer shall be tamped 25 times
with tamping rod and finally leveled off.
The weight of material comprising the test sample shall be determined. ( A ), g
The plunger shall be placed in position and the apparatus shall be then placed
between the platens of CTM.
Load shall be applied at uniform rate so that load of 40t is reached in 10
minutes.
The load shall be removed from the cylinder and sieved through 2.36 mm
sieve. The fraction passing sieve 2.36 mm shall be weighed to nearest 1g
(B,g )
Such two tests shall be taken.
47
Reporting :
Aggregate Crushing Value, % = ( B / A ) x100
The mean of the two results shall be reported to the nearest whole number.
Format to be Used :
Format for Aggregate Crushing value to be used.
48
FORMAT FOR AGGREGATE CRUSHING VALUE
Name of Client :
Name of Consultant :
Description Sample
I II
Weight of Oven Dried
Sample A , g
Weight of Sample
passing 2.36 mm
sieve after Loading ,
B , g
Aggregate Crushing
Value
= 100x B/A
Average
Acceptable Limit
Tested By : Checked By :
Date Date
49
CHAPTER 16
50
Calculations :
Compressive Strength, kg /cm2 = Max Load in Kg / Avg area of the bed faces of the
specimen, cm2
Report: Average of the results shall be reported.
Format to be Used :
Format for Testing of Common Burnt Clay Brick shall be used.
51
FORMAT FOR TESTING OF COMMON BURNT CLAY BRICKS
( IS : 3495-I )
Name of Client :
Name of Consultant :
A. Compressive Strength :
B. Water Absorption :
Sr Date of Frog I.D. Date of Wt of Wt of Water Sign.
receipt mark testing oven brick Absorpti
of Sketch dried immers on %
sample brick in ed for
g 24 hrs
in water
in g
Tested By : Checked By
Date Date
52
CHAPTER 17
Aim :
To determine Water Content in Soil Sample at Laboratory by Oven Method
Apparatus :
Container Any suitable non-corrodable air tight container. ( Remarks- These can
be 300ml aluminum or stainless steel boxes with lid )
Balance Having accuracy of 0.04% of the weight of soil taken for test. Remarks-
Balance of capacity 500 g and accuracy of 0.1g can be used when accurate
working is required. If normal weighing balance with 1g accuracy is used then
accuracy of water content will be around 0.2 to 0.5% only; depending on sample
size 500 to 200 g respectively.
Drying Oven Thermostatically controlled.
Soil Specimen :
It shall be true representative of soil mass. The size of specimen are
recommended for general laboratory use as below. However, the dryer the soil,
greater shall be size. Remarks : Preferably take 500g sample when weighing
accuracy is 1g.
Procedure:
Clean the container with lid, dry and weigh ( W1,g )
Take the required quantity of the soil specimen in container, crumble clods and
place loosely and weigh with the lid ( W2, g )
53
Keep filled container in an oven with the lid removed and maintain the
temperature at 110+/- 5 deg C. for maximum 24 hours.
Cool the container and record Final mass of container with lid and dried sample
( W3, g ).
Calculations :
% of Water Content = 100 x ( W2-W3 ) / ( W3- W1)
Report :
The water content % shall be expressed to two significant figures ( e.g.- 23, 2.3,
0.23 )
Note : Oven drying at 110 +/- 5 deg C does not result in reliable values for soil
containing Gypsum and any other mineral having water of hydration or significant
amount of organic matter. Reliable values can be obtained in an oven by drying at
temperature around 60-80 deg C.
Remarks: Traces of Gypsum / lime / Alum can be seen as white particles. That of
Organic matter will show black colour fibrous traces. Particles of Green / Bluish
Green can be minerals having water of hydration.
Aim :
To determine water content in soil specimen in the field.
Apparatus:
Container Any suitable Air tight container as given in Oven drying method.
Sand Bath : Suitable size and containing clean sand to a depth of 3 cms.
Stove, Spatula
Soil Specimen :
As given in Oven drying method.
54
Procedure :
Clean the container with lid, dry and weigh ( W1 , g )
Take the required quantity of the soil specimen in container, crumble the clods
and place loosely and weigh ( W2, g )
Add few pieces ( 3-4 small) of white paper if necessary. This the indicator for
over-heating. While heating the soil paper pieces shall not turn brown.
Place the container with lid removed on sand bath and heat sand bath on the
stove.
During heating sample shall be turned frequently and thoroughly to assist
evaporation. It shall be done carefully so as no soil mass is spilled over.
When drying is complete, remove the container and cool it down. Remove
pieces of papers.
Weigh the container with lid on. ( W3, g )
Calculations :
w % = 100x ( W2 - W3 ) / ( W3 W1 )
Report :
Same as Oven drying method to two significant figures ( e.g. 23, 2.3, 0.23 )
Format to be Used :
Format of Field Dry Density by Core cutter Method to be used.
55
CHAPTER 18
Aim : To determine the Field density of Fine grained soil by using Core-cutter. ( It
is less accurate than sand Replacement Method and recommended for well
compacted soils.
Apparatus :
Core cutter / Dolly / Rammer.
Balance of 1 g accuracy.
Pallet knife, Straight edge, Steel rule, Pick axe etc.
Soil sample :
Soil sample is termed as fine-grained if 90% by weight is passes through IS sieve
4.75 mm.
Procedure :
Internal Volume ( Vc, cm3 ) of core cutter shall be calculated by taking
dimensions to nearest to 0.25 mm ( By vernier).
Cutter shall be weighed to nearest g. ( Wc, g )
A small area, approximately 30 cms square of the soil layer to be tested shall
be exposed and leveled.
Cutter shall be placed vertically on soil with dolly on top.
Cutter shall be rammed down vertically into the soil layer until only about 15
mm of dolly protrudes above surface.
Care to be taken that cutter shall not rock sideways while hammering.
The cutter shall be dug out of surrounding soil by pick axe. Please take care so
as to have some protruding soil mass from the lower edge.
Soil from both the ends shall be trimmed flat to the ends of cutter.
The cutter containing soil mass shall be weighed to nearest g ( Ws, g )
The soil mass shall be removed from cutter and representative sample shall be
tested for water contents.
At least 3 tests are required to make average result.
56
Remarks Often problem encountered when soil mass is dry and cutter is not
properly filled up or looses soil while handling. In such case test is to be done
by sprinkling water and testing after suitable lapse of time. Core cutter shall be
removed, trimmed and kept in polythelene bag to take it to laboratory. It shall
be weighed with cutter and any loose soil mass collected in bag.
Calculations :
Bulk Density Yb of Wet Soil is as below:
Yb = ( Ws Wc ) / Vc , gms /cm3
Dry Density Yd is as below:
Yd = 100 Yb / ( 100 + w ) , gms /cm3 Where w = Water content %
Report :
Dry Density to be recorded to 2nd place of decimal in gms/cm3.
Water Content % to two significant figures ( e.g.- 23, 2.3, 0.23 )
Format to be Used :
Format of Field Density of Soil by Core Cutter Method shall be used.
57
FIELD DRY DENSITY OF SOIL
BY CORE CUTTER METHOD
( IS : 2720- XXIX )
Thickness of layer : mm
MDD of Soil : g/cm3 OMC % :
Acceptable Limit =
Tested By : Checked By :
Date Date
58
CHAPTER 3
CALIBRATION OF TEST
EQUIPMENTS
1- GENERAL
Scope :
The scope of this Calibration Plan is pertaining to SPCL procedure Document No
1000 GP04 043.
This Plan deals with Calibration & /or Verification of test equipments and measuring
equipments used in testing and production.
Requirements :
All test equipments in lab shall be in proper condition of use. They shall be verified at
some defined frequency to achieve correct results and consistent performance.
Measuring equipments and Test equipments are required to be calibrated to show that
these equipments give correct results within the tolerances specified by BIS. This shall
be done at defined frequency or as required.
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2 - CALIBRATION PLAN
60
3 - PROCEDURE FOR VERIFICATION OF EQUIPMENTS
(In House Test)
VERIFICATION OF CUBE MOULD
Aim : To check Cube Mould assembly for dimensional correct ness.
Apparatus : Platform flat and leveled, Set of spanners,Metallic scale,Vernier Caliper
Procedure :
Put Sr No on Cube moulds and base plates ( All plates )
Cube set assembly shall be kept on platform.
Check the joints which shall be tight and uniform. Thickness shall be hairline thick.
Check the bolts for tight fitting and cleanliness.
Remove the bolts and dis assemble the side plates and bottom plate.
Check for cleanliness and straightness with help of straight edge.
Re-fit the assembly and again and check for dimensional accuracy.
Check for diagonals for right angles in plan.
Remove bottom plate if attached and check diagonals between top and bottom.
Put cube assembly on base plate and check level of adjacent plates.
Tolerances ( IS : 516 ) :
Dimensional tolerances shall not be more than 150 + /- 0.2 mm.
Angular Tolerances shall be 90 deg + /- 0.5 deg. ( +/- 0.2 mm ).
Reports :Keep records of verifications of dimensions Date and Serial wise.
VERIFICATION OF SIEVES
Aim : To visually inspect the sieves for condition
Procedure :
Check the sieves are properly secure at frame and no gap is seen between frame and
sieve when pressed little on sieve center by palm.
Check the sieve wires /flats for straightness, ruptures etc.
Records : Rejected sieves shall be marked and then dispose suitably.
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VERIFICATION OF PAN BALANCE
Aim : To check the sensitivity of pan balance.
Apparatus : Weight of least count.
Procedure :
Check proper level of balance and cleanliness.
Keep the pan on balance and check for pointer.
Then apply slight pressure on pan and keep the balance in swing. Watch for any
abrupt stoppage of swing.
Then keep the least count weight lightly without shock in pan and check if it record
swing. Remove the weight lightly with forceps without shock and watch if pointer
returns back to original.
If it does not respond to the least count weight, use next higher weight and observe.
Conclusion : Weight to which balance responds and visually seen shall be the least
count of the balance.
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VERIFICATION OF COMPRESSION TESTING MACHINE OIL LEAKAGE
Aim : To check performance of loading. This can be tested while performing above
test also.
Apparatus :
Test Cube for higher grade than normally tested.
Procedure :
Test method is same as Cube Testing but cube is not to be loaded till crushing.
Place the cube in machine and load the cube till first crack appears on surface.
Stop the loading.
Watch the black needle whether remains in position. This needle may come back
slightly as cube is getting strained but then remains in position.
Conclusions :
If the needle traced back slowly it means there is leakage in system particularly Oil
seal inside cylinder. Or visible leakage in line connecting dial gauge and cylinder.
Report :
Report the load applied and observation and file in Calibration File.
Consult manufacturer for Repairs if required.
63
Slide the cube and center it correctly so that whole cube surface shall be in contact
with plain paper. Mark the cube edges on the paper by pen.
Slide one more plain paper ( Mark Top Side on the paper )on top surface of cube.
Put carbon paper on top of plain paper with carbon side touching plain paper. Mark
the cube edges on paper by pen after tightening platen on cube by jack.
Load the CTM partially say upto 25-30 kN. This should not break the cube.
Remove the load. Retrieve the cube and plain papers watch the carbon marks on the
[Link] the cube size marking with straight edge to show area of cube with
respect to carbon mark ( which will appear circular in shape).
Results :
Refer to the top side paper [Link] the diagonals of cube size and check if carbon
mark is concentric with center of cube dimensions. If this is not concentric then cubes
are getting loaded eccentrically and failures are occurring only on one side mostly.
Check the carbon marking on the paper with respect to size of cube. If this marking is
less than 75 mm in diameter, it means cube is getting loaded only as point load
thereby most of the cubes are getting cracks [Link] to the Bottom side
[Link] this side carbon marking will on more area than top side. Check the
consistency of shade of [Link] shall not be varying too much in shade or blank
spaces in between.
Conclusions:
If top markings are showing point or eccentric loading, it means top platen is bent (
Usually this occurs in 100t CTM as per our experience).If bottom marking have large
shade variance, bottom platen surface has [Link] the Manufacturer for
replacement or repairs of platens.
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4 - CALIBRATION OF BATCHING PLANT
(In House Test)
Aim : To calibrate the weighing mechanism of batch plant to conform within weighing
tolerances.
Apparatus :
Calibrated Weight blocks of various designations 50 / 20 kgs / 10 kgs ( As decided
and required ).
Procedure :
Clear the bucket of all loose and any sticking material shall be removed.
Set the reading at zero on display for no load.
Load the bucket with weights starting from 20 kg and increase at the increment of
50 kgs.
At start and each increment record the load on dial or display ( Loading Condition
).
Reach the total load upto 1.2 times the operating weight of material being used or
to the 0.9 times of capacity.
After this remove 50 kg load every time and record these decrement values as
above ( Unloading Condition )
Check the report for tolerances to + /- 3 %. If it is exceeding the same weighing
mechanism shall be adjusted suitably to give minimum errors.
Report :
Keep report of variance of actual weights and recorded weights. Give correction
factors to plant operator.
65
BATCHING PLANT CALIBRATION REPORT
SP Code No :
66
5 - LIST OF ABBREVIATION
Amp : Ampere
Avg : Average
C : Centigrade
C.C. : Cement Concrete
CA : Coarse Aggregate
cc : Cubic Centimeter
cl. : Clause
CM : Cement Mortar ( Proportion )
cm : Centimeter
cm2 : Square Centimeter
cm3 : - do
CTM : Compression Testing Machine
deg : Degree ( Temperature)
Dia : Diameter
DLBD : Dry Loose Bulk Density.
g : Gram
G.I. : Galvanized Iron
Hrs : Hours
IS : Indian Standard
ISI : Indian Standard Institution now BIS ( Bureau of Indian Standards )
Kg : Kilogram
kN : Kilo-Newton ( Weight measure. 1kN = 1000 N = 100 kg )
LL : Live Load
M.S. : Mild Steel
m3 : Cubic meter
Max : Maximum
mcn : Micron ( 1000 micron = 1 mm )
MDD : Maximum Dry Density
Min : Minimum
mm : Millimeter
mm2 : Square Millimeter
Mpa : Mega Pascal ( Unit of Stress/ Pressure )
MT : Metric Ton ( 1 MT = 1000 Kgs)
MTC : Manufacturers Test Certificate
N : Newton ( weight measure 10 N = 1 Kg approx )
No : Number
O.P.C : Ordinary Portland Cement
OMC : Optimum Moisture Content
Pg : Page
PPC : Portland Pozzolana Cement
PSC : Portland Slag Cement
Qty : Quantity
RMC : Ready Mix Concrete
S.D. : Standard Deviation
[Link]. : Specific Gravity
SPCL : m/s Shapoorji Pallonji & Co. Ltd.
Sr. : Serial
Std : Standard
UTS : Ultimate Tensile Stress
wt : Weight
67
6 - DEFINITIONS
Newton : It is measure of weight in S.I. ( International Standard ) Unit. 10 N = 1kg.
Approximately.
Mpa : It is unit of Stress or Pressure in S.I. ( International Standard ) Unit. Equivalent
to N/mm2.
Optimum Moisture Content ( OMC ) : Calculated in %. It is the moisture content in
soil at which soil can be compacted to maximum Dry Density under given applied
efforts ( Ramming with standard weight rammer through standard distance ).
Maximum Dry Density ( MDD ) : The maximum density to which soil can attain at
given parameters ( Like Moisture Content and efforts ). The value is calculated without
the weight of water content in specimen.
Gross Sample : Sample collected from stack of material which is representative and
it is further divided to make specimen for testing by specific method.
Liquid Limit ( LL ) : It is calculated in % for cohesive soils. It is the % of water at
which soil specimen flows under little effort applied. This gives undesirable conditions
of water content in cohesive soil mass.
Plastic Limit ( PL ) : It is calculated in % for cohesive soils. It is the % of water at
which soil specimen become plastic e.g. moldable / compactable. OMC of soil is
generally slightly less than PL.
Plasticity Index ( PI ) : It is numerical difference bet LL & PL ( LL- PL ). For highly
cohesive soils PI is high. For Non-cohesive soils PI is less. Highly cohesive soils
offers great resistance to compaction and Non-cohesive soils are unstable in moist
conditions.
Characteristic Strength ( of Concrete ) , Fck : This is the designated strength ( in
N/mm2 or kg /cm2 ) of cube cured for 28 days for given Grade of the concrete, below
which not more than 5% of the test results are expected to fall. This value shall not be
considered as accepted value of strength directly. Concrete strength acceptance
criteria is based on value of Fck.
Mean Target Strength (of Concrete ) : This value is targeted when designing the
mix of concrete under strict control at laboratory. Hence under site conditions lower
values will be attained without any compromise on acceptance criteria.
Lot of Brick : A collection of bricks of same class and size, manufactured under
relatively similar conditions of production.
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Batch of Cement : This is displayed on cement bags as a week number of the year.
It shows Week of production ( Whole year is divided in weeks and serial no of week is
given. E.g.- 4th week means 4th week of Jan. 9th week means 1st week of Mar ) along
with Month and year is also shown. The display is 9 / 03 or
W M Y
9 3 2003
0.2% Proof stress ( For steel ) - IS : 1608 : It is derived from graph force vs.
extension. Value of force is derived by drawing line at 0.2% of extension on graph and
running it parallel to the straight portion of graph. This line will intersect the graph and
value of force will be obtained. This force is divided by the original cross section area
of specimen and thus 0.2 % proof stress is arrived at.
Batch of Steel- IS 1786 : Any quantity of bars /wires of same size and grade whether
in coils or bundle presented for examination and test at one time.
Bundle of Steel IS 1786 : Two or more coils or a number of lengths properly bound
together.
Notes ( As mentioned in this manual ) : These are authentic notes / comments
given from references.
Remarks ( As mentioned in this manual ) : These are added extra as per normal
practices and observations. These can not be quoted as authentic one as no
proper back up can be available.
69
LABORATORY MANUAL AMENDMENT REQUEST FORM
From :
Document Code :
Dept./Site : ISO Cell, SP Centre
Document Title : To :
SIGNATURE OF ORIGINATOR
Review Notes :
P.S. The Amendment Request Form shall be approved Recommended Not Recommended
by the approving authority of the Document.
Document Issued On : By :
70
Cube casting involves verifying cube mould dimensions for tight assembly, arranging them in sets, and lightly oiling. Concrete is filled in three layers, each tamped 25 times with a rod. Extra concrete is struck off flush, and cubes are left undisturbed for at least 6 hours before marking. After setting, cubes are covered with wet bags until transferred to a curing tank 10-12 hours later. Curing involves arranging cubes sequentially in the tank without frequent handling .
The sieve analysis procedure involves drying a sample, weighing it, and successively sieving it through descending-sized sieves arranged with a pan at the bottom. The percentage by weight retained on each sieve is calculated to determine the size and grading distribution, which assesses if aggregates meet specified standards .
Water absorption is measured by comparing the weight of surface-dry sample to the oven-dried sample weight. The percentage water absorption is calculated as 100 x (A – D) / D. High water absorption can indicate porosity, affecting concrete strength and durability by influencing water-cement ratio and hydration .
In high temperature regions, ice is added to the concrete mix to manage temperature without changing the water-cement ratio, while the amount of water is adjusted to account for the melting ice . In low temperature regions, measures must be taken to control temperature during mixing and placement to ensure adequate curing and prevent freezing .
The quartering method involves taking the gross sample on a platform, mixing it, and forming it into a cone-shaped pile which is then flattened. The pile is divided into four quadrants, rejecting two diagonally opposite quarters. This process is repeated until the desired sample size is achieved for testing .
The fineness modulus is calculated by summing the cumulative percentages retained on each sieve of a sieve analysis and dividing by 100. Higher values indicate coarser sand, while lower values indicate finer sand. The normal range for FM is between 2.2 to 3.2, indicating acceptable aggregate gradation .
Concrete sampling from a mixer is conducted by taking at least three approximately equal samples that total 0.02 m3. Samples should be taken using a scoop, at times when 1/4, 1/2, and 3/4 of the concrete has been discharged. The samples need to be collected and remixed on a non-absorbent platform for testing .
Flakiness index measures the percentage of aggregates that are flaky, meaning their thickness is less than 0.6 of the nominal size. It is determined using a flakiness gauge and calculated by weighing pieces passing slots corresponding to each fraction size. High flakiness impacts workability and strength, thus should be minimized for quality concrete .
The specific gravity is determined by weighing the saturated surface-dry sample (A), the pycnometer with sample and water (B), and just the pycnometer with water (C). After weighing the oven-dried sample (D), specific gravity is calculated using the formula D / [A - (B - C)]. This provides a measure of aggregate density .
Consistent side cracking indicates centric loading; if cracks always occur centrally, it signifies point loading due to platen convexity. It is necessary to adjust loading procedures or equipment setup to ensure even loading surfaces to prevent incorrect failure modes .